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首页> 外文期刊>Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics >Ba(Ti_(1-x)Sn_x)O_3 (x = 0.13) nanomaterials produced by low-temperature aqueous synthesis
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Ba(Ti_(1-x)Sn_x)O_3 (x = 0.13) nanomaterials produced by low-temperature aqueous synthesis

机译:低温水合成法制备Ba(Ti_(1-x)Sn_x)O_3(x = 0.13)纳米材料

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摘要

BaTi_(0.87)Sn_(0.13)O_3 (BTS_(13)) nanopowder was prepared by low-temperature aqueous synthesis (LTAS) method. The evolution of the structure and microstructure of the precursor precipitate, heated at temperatures up to 1000°C was studied by TGA, FT-IR, SEM and XRD techniques. The dried precipitate showed a microstructure consisting of nano-sized grains (~40 nm) with great tendency to agglomeration. BaTi_(0.87)Sn_(0.13)O_3 single phase was obtained at 800 °C. The ceramics prepared from as-obtained BTS_(13) powders (60-70 nm) show good dielectric and ferroelectric characteristics.
机译:通过低温水合成法制备了BaTi_(0.87)Sn_(0.13)O_3(BTS_(13))纳米粉。通过TGA,FT-IR,SEM和XRD技术研究了在高达1000°C的温度下加热的前驱体沉淀物的结构和微观结构的演变。干燥的沉淀物显示出由纳米颗粒(〜40 nm)组成的微观结构,具有很大的团聚趋势。在800℃下获得BaTi_(0.87)Sn_(0.13)O_3 单相。由获得的BTS_(13)粉末(60-70 nm)制备的陶瓷具有良好的介电和铁电特性。

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