Hydrothermal synthesis of MnCO_3 nanorods and their thermal transformation into Mn_2O_3 and Mn_3O_4 nanorods with single crystalline structure

Xiaoping Shen; Zhenyuan Ji; Huajuan Miao

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Hydrothermal synthesis of MnCO_3 nanorods and their thermal transformation into Mn_2O_3 and Mn_3O_4 nanorods with single crystalline structure

机译：MnCO_3纳米棒的水热合成及其热转化为单晶结构的Mn_2O_3和Mn_3O_4纳米棒

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摘要

MnCO_3 nanorods with diameters of 50-150 nm and lengths of about 1-2 ìm have been prepared for the first time by a facile hydrothermal method. Mn_2O_3 and Mn_3O_4 nanorods were obtained via the heat-treatment of the MnCO_3 nanorods in air and nitrogen atmosphere, respectively. The morphology and structure of the as-synthesized MnCO_3, Mn_2O_3 and Mn_3O_4 nanorods were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and selected area electron diffraction.

机译：MnCO_3纳米棒的直径为50-150 nm，长度约为1-2μm，是通过一种简便的水热方法首次制备的。 Mn_2O_3和Mn_3O_4纳米棒分别通过在空气和氮气气氛中对MnCO_3纳米棒进行热处理而获得。通过X射线衍射，扫描电子显微镜，透射电子显微镜和选择区域电子衍射对合成后的MnCO_3，Mn_2O_3和Mn_3O_4纳米棒的形貌和结构进行表征。

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《Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics》 |2011年第18期|共5页
作者
Xiaoping Shen; Zhenyuan Ji; Huajuan Miao;
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正文语种 eng
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Nanorods; Manganese oxide; Manganese carbonate; Synthesis; Lithium ion batteries;

机译：纳米棒氧化锰碳酸锰合成锂离子电池;

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1. Hydrothermal synthesis of MnCO_3 nanorods and their thermal transformation into Mn_2O_3 and Mn_3O_4 nanorods with single crystalline structure [J] . Xiaoping Shen, Zhenyuan Ji, Huajuan Miao Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics . 2011,第18期

机译：MnCO_3纳米棒的水热合成及其热转化为单晶结构的Mn_2O_3和Mn_3O_4纳米棒
2. Hydrothermal synthesis, characterizations and photoluminescence study of single crystalline hexagonal ZnO nanorods with three dimensional flowerlike microstructures [J] . Rohidas B. Kale, Yung-Jung Hsu, Yi-Feng Lin, Superlattices and microstructures . 2014,第may期

机译：具有三维花状微结构的单晶六角形ZnO纳米棒的水热合成，表征和光致发光研究
3. Synthesis, microstructure, magnetic properties and Raman scattering of single-crystalline BiFeO3 nanorods prepared by hydrothermal technique [J] . Optoelectronics and Advanced Materials-Rapid Communications . 2012,第2012期

机译：水热法制备BiFeO3单晶纳米棒的合成，微观结构，磁性和拉曼散射
4. Solution-phase synthesis of single-crystalline Mn_3O_4 nanorods with paramagnetic properties [C] . Yange Zhang, Pinjiang Li, Xiaoyun Zheng, International Conference on Manufacturing Science and Engineering . 2012

机译：具有顺磁性性质的单晶Mn_3O_4纳米棒的溶液相合成
5. Synthesis, characterization, and photocatalytic activities of Cobalt(II)-Titanium dioxide nanorods, and electrophoretic deposition of Titanium dioxide nanoparticle/nanorod composite films for self-cleaning applications. [D] . Kang, Wonjun. 2013

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6. Hydrothermal Synthesis and Biocompatibility Study of Highly Crystalline Carbonated Hydroxyapatite Nanorods [O] . Caibao Xue, Yingzhi Chen, Yongzhuo Huang, 2015

机译：高结晶碳酸化羟基磷灰石纳米棒的水热合成及生物相容性研究
7. Hydrothermal Synthesis of Single-Crystalline Anatase TiO2 Nanorods with Nanotubes as the Precursor [O] . -1

机译：用纳米管作为前体的单晶锐钛矿TiO2纳米棒的水热合成

Hydrothermal synthesis of MnCO_3 nanorods and their thermal transformation into Mn_2O_3 and Mn_3O_4 nanorods with single crystalline structure

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