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Estimation of the pore diameter of organosilane-modified silica based on the fusion temperature of ice

机译:基于冰的熔化温度估算有机硅烷改性二氧化硅的孔径

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摘要

Differential scanning calorimetry (DSC) measurements were performed for water confined within mesoporous silica substrates of TMPS-4 and TMPS-4M (TMPS-4 modified with 3-aminopropyltriethoxysilane) with highly ordered cylindrical channels. The pore diameter of TMPS-4M estimated by the DSC measurements corresponds to the results obtained by nitrogen adsorption measurements.
机译:进行差示扫描量热法(DSC)测量,测定水封存在TMPS-4和TMPS-4M(经3-氨基丙基三乙氧基硅烷修饰的TMPS-4)的介孔二氧化硅基质中,该基质具有高度规则的圆柱状通道。通过DSC测量估计的TMPS-4M的孔径对应于通过氮吸附测量获得的结果。

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