Cu-catalyzed cyclization to construct indoles fromN-(ortho-chloromethyl)aryl carbamates and terminal alkynesviaa one-pot reaction

Shi Yang; Wang Gangqiang; Wang Hang; Deng Bin; Gao Tao; Wang Jian; Guo Haibing; Wu Minghu; Sun Shaofa

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Cu-catalyzed cyclization to construct indoles fromN-(ortho-chloromethyl)aryl carbamates and terminal alkynesviaa one-pot reaction

机译：Cu催化的环化构建吲哚N-（邻氯甲基）芳基氨基甲酸酯和末端炔烃一锅反应

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摘要

In this reaction, a new strategy for the synthesis of indoles fromN-(ortho-chloromethyl)aryl carbamates and terminal alkynesviaCu-catalyzed coupling-cyclization has been developed. The reactions proceeded smoothly under mild conditions with a wide functional group tolerance.

机译：在该反应中，已经开发出来自Nn-（邻氯甲基）芳基氨基甲酸酯和末端炔烃催化偶联环化的新策略。反应在温和条件下平稳地进行，具有宽的官能团耐受性。

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来源
《New Journal of Chemistry》 |2020年第34期|共4页
作者
Shi Yang; Wang Gangqiang; Wang Hang; Deng Bin; Gao Tao; Wang Jian; Guo Haibing; Wu Minghu; Sun Shaofa;
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作者单位

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

Hubei Univ Sci &

Technol Sch Nucl Technol &

Chem &

Biol Nonpower Nucl Technol Collaborat Innovat Ctr Hubei Key Lab Radiat Chem &

Funct Mat Xianning 437100 Peoples R China;

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正文语种 eng
中图分类化学;
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1. Cu-catalyzed cyclization to construct indoles fromN-(ortho-chloromethyl)aryl carbamates and terminal alkynesviaa one-pot reaction [J] . Shi Yang, Wang Gangqiang, Wang Hang, New Journal of Chemistry . 2020,第34期

机译：Cu催化的环化构建吲哚N-（邻氯甲基）芳基氨基甲酸酯和末端炔烃一锅反应
2. Synthesis of Indoles through Highly Efficient Cascade Reactions of Sulfur Ylides and N-(ortho-Chloromethyl)aryl Amides [J] . Qing-Qing Yang, Cong Xiao, Liang-Qiu Lu Angewandte Chemie . 2012,第36期

机译：通过硫叶立德和N-（邻氯甲基）芳基酰胺的高效级联反应合成吲哚
3. Synthesis of 5-Aryl-5H-pyrido[2',1':2,3]imidazo[4,5-b]indoles by Domino Pd- and Cu-Catalyzed C-N Coupling Reactions [J] . Tran Quang Hung, Nguyen Minh Quan, Hoang Van Dong, Synlett . 2019,第3期

机译：通过Domino PD-和Cu催化的C-N偶联反应合成5-芳基-5H-吡啶[2'，1'，1'，1'，1'，1'，1'，1'，1'，1'，1'，1'，1'，吲哚
4. One-Pot Syntheses of 2,3-Dihydrothiopyran-4-one Derivatives by Pd/Cu-Catalyzed Reactions of α,β-Unsaturated Thioesters with Propargyl Alcohols [C] . Yasunori Minami, Hitoshi Kuniyasu, Nobuaki Kambe Symposium on Organometallic Chemistry . 2008

机译：通过Pd / Cu催化的α，β-不饱和硫代酯与丙醇醇的Pd / Cu催化反应合成2,3-二羟基吡喃吡喃-4-衍生物
5. The directed ortho metalation reaction of aryl O-carbamates on solid support. [D] . Milburn, Claire Louise Maud Jackson. 2001

机译：芳基氨基甲酸酯在固体载体上的定向原位金属化反应。
6. General and Efficient Cu-Catalyzed Three Component Coupling Reaction Toward Imidazoheterocycles: One-Pot Synthesis of Alpidem and Zolpidem [O] . Natalia Chernyak, Vladimir Gevorgyan -1

机译：通用和高效的铜催化的三组分偶联反应走向Imidazoheterocycles：阿吡坦唑吡坦和的一锅法合成
7. Chemo- and Stereodivergent Preparation of Terminal Epoxides and Bromohydrins through One-Pot Biocatalysed Reactions: Access to Enantiopure Five- and Six-Membered N-Heterocycles [O] . Bisogno Forconesi, Fabricio Román, Cuetos Fernández, Aníbal, Orden, Alejandro Agustín, 2010

机译：通过一锅生物催化反应化学和立体发散制备末端环氧化物和溴代醇的方法：获得对映纯的五元和六元N-杂环
8. Synthesis of Metallacycles by 1,3-Dipolar Cycloaddition Reactions Between Low-Valent Metal Carbonyls and Aryl Nitrile N-Oxides. [R] . Chetcuti, P. A., Walker, J. A., Knobler, C. B., 1988

机译：低价金属羰基化合物与芳基腈N-氧化物之间1,3-偶极环加成反应合成金属环。

Cu-catalyzed cyclization to construct indoles fromN-(ortho-chloromethyl)aryl carbamates and terminal alkynesviaa one-pot reaction

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