One-pot three component synthesis of 5-allyl-1,2,3-triazoles using copper(I) acetylides

Reddy Parigi Raghavendar; Cui Lianji; Ryu Jae-Sang

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One-pot three component synthesis of 5-allyl-1,2,3-triazoles using copper(I) acetylides

机译：使用铜（I）乙酰酯的5-烯丙基-1,2,3-三唑的单壶三组分合成

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One-pot three-component reactions using copper(I) acetylide, azide, allyl iodide, and NaOH have been developed. The reactions proceed smoothly at room temperature to afford 5-allyl-1,2,3-triazoles, which can be further transformed into a variety of 1,2,3-triazole-fused bi-/tricyclic scaffolds. This method offers the most efficient, convenient, and practical route towards useful polycyclic scaffolds in moderate to excellent yields.

机译：已经开发了使用铜（I）乙炔，叠氮，烯丙基碘化物和NaOH的一锅三组分反应。反应在室温下平滑地进行，得到5-烯丙基-1,2,3-三唑，可以进一步转化为各种1,2,3-三唑稠合的双/三环支架。该方法提供了适用于中等至优异产量的有用多环支架的最有效，方便，实用的途径。

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来源
《RSC Advances》 |2018年第5期|共9页
作者
Reddy Parigi Raghavendar; Cui Lianji; Ryu Jae-Sang;
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Ewha Womans Univ Coll Pharm 52 Ewhayeodae Gil Seoul 03760 South Korea;

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正文语种 eng
中图分类化学;
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1. One-pot three component synthesis of 5-allyl-1,2,3-triazoles using copper(I) acetylides [J] . Reddy Parigi Raghavendar, Cui Lianji, Ryu Jae-Sang RSC Advances . 2018,第5期

机译：使用铜（I）乙酰酯的5-烯丙基-1,2,3-三唑的单壶三组分合成
2. A Copper(I)-Mediated Tandem Three-Component Synthesis of 5-Allyl-1,2,3-triazoles [J] . Song Yoona, Lee Soyun, Dutta Palash, Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2020,第5期

机译：铜（I）介导的串联三分组合合成5-烯丙基-1,2,3-三唑
3. Practical one-pot synthesis of 5-alkynyl-1,2,3-triazoles via heterogeneous copper(I)-catalyzed tandem three-component click/alkynylation reaction [J] . Applied Organometallic Chemistry . 2020,第1期

机译：通过异质铜（I）的5-炔基-1,2,3-三唑合成的实用单壶合成 - 催化串联三分组分咔哒/醇烷基化反应
4. Copper(II) Triflate as a Double Catalyst for the One-Pot Click Synthesis of 1,4-Disubstituted 1,2,3-Triazoles from Benzylic Acetates [C] . Eiji Shimizu, Satoshi Kikuchi, Shin-ichi Fnkuzawa Symposium on Organometallic Chemistry . 2007

机译：铜（II）作为单罐的双催化剂，单击1,4-二取代的1,2,3-三唑的双催化剂，从苄基乙酸盐中键合
5. Development of a new tridentate pincer phosphine N-heterocyclic carbene ligand, &, Development of copper II catalyzed three component tandem synthesis of isoindolinone derivatives [D] . Sun, Leon Xuetong 2011

机译：新型三齿钳制膦N-杂环卡宾配体的开发，＆铜II催化异吲哚啉酮衍生物的三组分串联合成
6. Copper(I)-Catalyzed Cycloaddition of Bismuth(III) Acetylides with Organic Azides: Synthesis of Stable Triazole Anion Equivalents [O] . Brady T. Worrell, Dr. Shelby P. Ellery, Prof. Valery V. Fokin -1

机译：铜（I）催化的铋（III）与有机叠氮化物的环加成反应：稳定的三唑阴离子当量的合成
7. One-Pot, Three-Component Synthesis of 1-(2-Hydroxyethyl)-1H-1,2,3-triazole Derivatives by Copper-Catalyzed 1,3-Dipolar Cycloaddition of 2-Azido Alcohols and Terminal Alkynes under Mild Conditions in Water [O] . Hashem Sharghi, Mona Hosseini-Sarvari, Fatemeh Moeini, 2010

机译：通过铜催化的1,3-偶极醇环加入的2-α醇醇和末端炔烃在水中的温和条件下的1-（2-羟乙基）-1H-1,2,3-三唑衍生物的一锅。

One-pot three component synthesis of 5-allyl-1,2,3-triazoles using copper(I) acetylides

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