Screening of multiclass pesticide residues in maca andMoringa oleiferaby a modified QuEChERS sample preparation procedure and UPLC-ESI-MS/MS analysis

Zhu Yanqin; Du Ping; Yang Jun; Yin Qinhong; Yang Yaling

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Screening of multiclass pesticide residues in maca andMoringa oleiferaby a modified QuEChERS sample preparation procedure and UPLC-ESI-MS/MS analysis

机译：Maca和Macoringa Oleiferaby在Maca和Moleiferaby中的多烷类农药残留筛选改性Quechers样品制备程序和UPLC-ESI-MS / MS分析

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In the present study, a modified QuEChERS (quick, easy, cheap, effective, rugged, and safe) method was proposed for the simultaneous analysis of 75 pesticides in maca andMoringa oleiferawith ultra-performance liquid chromatography-electrospray ionization-tandem mass spectrometry (UPLC-ESI-MS/MS). The developed method was validated in accordance with linearity, linear range, limit of detection, limit of quantification, accuracy, precision, and matrix effect. Each analyte had good linearity (R-2> 0.99) in the corresponding concentration range. The method LOD and LOQ values of all the analytes ranged from 0.01 mu g kg(-1)to 303.35 mu g kg(-1)and 0.03 mu g kg(-1)to 1011.15 mu g kg(-1), respectively. The recoveries (n= 6) of the analyzed pesticides were in the range of 75.92-113.43%. The RSDs of precision were between 0.60% and 7.36%. All matrix effect values ranged from 81.79% to 118.71% and 80.36% to 119.64% in maca andMoringa oleifera, respectively. The analysis of 103 samples showed the presence of isofenphos-methyl in some of them. The method had a good application prospect and could be used as a general approach for the quantitative determination of pesticide residues in food.

机译：在本研究中，提出了一种改进的QueChers（快速，容易，廉价，有效，坚固耐用，安全的）方法，用于同时分析Maca和Macoringa Oleiferawith超级性能液相色谱 - 电喷雾电离 - 串联质谱（UPLC -esi-ms / ms）。根据线性，线性范围，检测限，定量限制，准确，精度和矩阵效应，验证开发方法。每个分析物在相应的浓度范围内具有良好的线性度（R-2> 0.99）。所有分析物的方法LOD和LOQ值的范围为0.01μgkg（-1）至303.35μgkg（-1）和0.03μgkg（-1）至1011.15μgkg（-1）。分析的农药的回收率（n = 6）在75.92-113.43％的范围内。精度的RSD在0.60％和7.36％之间。所有基质效应值分别为81.79％至118.71％和80.36％，分别在Maca和Macoringa Oleifera的80.36％至119.64％。对103个样品的分析显示出在其中一些中的异氟苯甲酸甲基。该方法具有良好的应用前景，可用作量化食物中农药残留量的一般方法。

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《RSC Advances》 |2020年第60期|共14页
作者
Zhu Yanqin; Du Ping; Yang Jun; Yin Qinhong; Yang Yaling;
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作者单位

Kunming Univ Sci &

Technol Res Ctr Anal &

Measurement Kunming 650093 Yunnan Peoples R China;

Kunming Univ Sci &

Technol Res Ctr Anal &

Measurement Kunming 650093 Yunnan Peoples R China;

Kunming Univ Sci &

Technol Res Ctr Anal &

Measurement Kunming 650093 Yunnan Peoples R China;

Yunnan Police Coll Fac Narcot Control Kunming 650223 Yunnan Peoples R China;

Kunming Univ Sci &

Technol Fac Life Sci &

Technol Kunming 650500 Yunnan Peoples R China;

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正文语种 eng
中图分类化学;
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1. Screening of multiclass pesticide residues in maca andMoringa oleiferaby a modified QuEChERS sample preparation procedure and UPLC-ESI-MS/MS analysis [J] . Zhu Yanqin, Du Ping, Yang Jun, RSC Advances . 2020,第60期

机译：Maca和Macoringa Oleiferaby在Maca和Moleiferaby中的多烷类农药残留筛选改性Quechers样品制备程序和UPLC-ESI-MS / MS分析
2. Validation of a modified QuEChERS method to determine multiclass multipesticide residues in apple, banana and guava using GC–MS and LC–MS/MS and its application in real sample analysis [J] . Swagata Mandal, Rajlakshmi Poi, Inul Ansary, SN Applied Sciences . 2020,第2期

机译：使用GC-MS和LC-MS / MS验证改良的QuEChERS方法以确定苹果，香蕉和番石榴中多种农药残留的方法及其在实际样品分析中的应用
3. Identification and characterization of matrix components in spinach during QuEChERS sample preparation for pesticide residue analysis by LC-ESI-MS/MS, GC-MS and UPLC-DAD [J] . Islam Abul Kasem Mohammad Mydul, Hong Su-Myeong, Lee Hyo-Sub, Journal of Food Science and Technology . 2018,第10期

机译：QueChers样品制剂在QueChers样品制剂中鉴别和表征菠菜在昆虫渣水合物，GC-MS和UPLC-DAD分析
4. Simultaneous Determination of Four Herbicide and Pesticide Residues in Chinese Green Tea Using QuEChERS Purification Procedure and UPLC-MS/MS Analysis [C] . Sufang Wang, Shoujie Zhang, Chunhong Dong International Conference on Chemical, Material and Metallurgical Engineering . 2013

机译：用Quechers纯化程序和UPLC-MS / MS分析同时测定中国绿茶中四种除草剂和农药残留物
5. Soil pesticide residue degradation and soil sample management procedures for environmental forensics [D] . Saxton, George N., Jr. 2004

机译：土壤农药残留降解和环境法证的土壤样品管理程序
6. Identification and characterization of matrix components in spinach during QuEChERS sample preparation for pesticide residue analysis by LC–ESI–MS/MS GC–MS and UPLC-DAD [O] . Abul Kasem Mohammad Mydul Islam, Su-Myeong Hong, Hyo-Sub Lee, 2018

机译：用LC–ESI–MS / MSGC–MS和UPLC-DAD对QuEChERS样品进行农药残留分析的菠菜中基质成分的鉴定和表征
7. Validation of a modified QuEChERS method to determine multiclass multipesticide residues in apple, banana and guava using GC–MS and LC–MS/MS and its application in real sample analysis [O] . Swagata Mandal, Rajlakshmi Poi, Inul Ansary, 2020

机译：使用GC-MS和LC-MS / MS的苹果，香蕉和番石榴中多种多组多农素残留的修改QueChers方法及其在真实样本分析中的应用

Screening of multiclass pesticide residues in maca andMoringa oleiferaby a modified QuEChERS sample preparation procedure and UPLC-ESI-MS/MS analysis

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