Heteroleptic manganese compounds as potential precursors for manganese based thin films and nanomaterials

Lee Sunju; Lee Ga Yeon; Kim Chang Gyoun; Chung Taek-Mo; Park Bo Keun

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Heteroleptic manganese compounds as potential precursors for manganese based thin films and nanomaterials

机译：异致锰化合物作为锰基薄膜和纳米材料的潜在前体

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Heteroleptic manganese compounds, [Mn(tmhd)(TMEDA)Cl](2)(1), [Mn(tmhd)(dmamp)](2)(2), Mn-2(tmhd)(2)(edpa)(2)(mu-THF) (3), [Mn(dmampea)(NEt2)](2)(4), and Mn(dmampea)(Pr-i-MeAMD) (5), were synthesized and characterized. Compound5was a volatile liquid. Structural analysis revealed that1-4were dimers. Compounds1and3,2, and4had distorted octahedral, distorted trigonal-bipyramidal, and distorted tetrahedral geometries around the Mn centers, respectively. Based on thermogravimetric analysis, the residues of2and3were expected to be MnO and Mn3O4, respectively. According to thermogravimetric analysis,4showed a higher residual value, whereas5exhibited a lower value than those expected for manganese nitrides.

机译：异致锰化合物，[Mn（TMHD）（TMEDA）（TME）（2）（2）（1），[Mn（TMHD）（Dmamp）]（2）（2），Mn-2（TMHD）（2）（EDPA）（ 2）（MU-THF）（3），[Mn（DMAMPEA）（NET2）]（2）（4）和Mn（DMAMPEA）（PR-I-MEAMD）（5）被合成并表征。化合物5瓦斯挥发性液体。结构分析显示1-4次级别。化合物1和3,2，AND4横向反落，分别扭曲了八面体，扭曲的三角形 - 双吡酰胺，以及Mn中心周围的扭曲四面体几何形状。基于热重分析，分别预期的2和3次预期为MNO和MN3O4的残留物。根据热重分析，4表示较高的剩余值，而少于锰氮化物的值较低。

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《RSC Advances》 |2020年第50期|共9页
作者
Lee Sunju; Lee Ga Yeon; Kim Chang Gyoun; Chung Taek-Mo; Park Bo Keun;
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Korea Res Inst Chem Technol KRICT Thin Film Mat Res Ctr 141 Gajeong Ro Daejeon 34114 South Korea;

Korea Res Inst Chem Technol KRICT Thin Film Mat Res Ctr 141 Gajeong Ro Daejeon 34114 South Korea;

Korea Res Inst Chem Technol KRICT Thin Film Mat Res Ctr 141 Gajeong Ro Daejeon 34114 South Korea;

Korea Res Inst Chem Technol KRICT Thin Film Mat Res Ctr 141 Gajeong Ro Daejeon 34114 South Korea;

Korea Res Inst Chem Technol KRICT Thin Film Mat Res Ctr 141 Gajeong Ro Daejeon 34114 South Korea;

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中图分类化学;
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1. Heteroleptic manganese compounds as potential precursors for manganese based thin films and nanomaterials [J] . Lee Sunju, Lee Ga Yeon, Kim Chang Gyoun, RSC Advances . 2020,第50期

机译：异致锰化合物作为锰基薄膜和纳米材料的潜在前体
2. Manganese half-sandwich complexes as metal-organic chemical vapor deposition precursors for manganese-based thin films [J] . Assim K., Jeschke J., Jakob A., Thin Solid Films . 2016,第nova30期

机译：锰半三明治配合物，作为锰基薄膜的金属有机化学气相沉积前体
3. Water Oxidation Catalysis by Nanoparticulate Manganese Oxide Thin Films: Probing the Effect of the Manganese Precursors [J] . Archana Singh, Rosalie K. Hocking, Shery L.-Y. Chang Chemistry of Materials: A Publication of the American Chemistry Society . 2013,第7期

机译：纳米氧化锰薄膜的水氧化催化：探究锰前体的影响。
4. Carbon Nanotube/Manganese Oxide Thin Film Composites-based Counter Electrode for Dye-Sensitized Solar Cell [C] . NATHAKREAT Ketama, WIRAT Jarernboon, WINADDA Wongwiriyapan International Conference on Applied Physics and Material Applications . 2016

机译：用于染料敏化太阳能电池的基于碳纳米管/锰氧化物薄膜复合材料的基电极
5. Thin film Heusler compounds manganese nickel gallium. [D] . Jenkins, Catherine Ann. 2009

机译：薄膜Heusler复合锰镍镓。
6. New Heteroleptic Cobalt Precursors for Depositionof Cobalt-Based Thin Films [O] . SeongHo Han, Sheby Mary George, Ga Yeon Lee, 2017

机译：用于沉积的新型异钴钴前体钴基薄膜的制备
7. New Heteroleptic Cobalt Precursors for Deposition of Cobalt-Based Thin Films [O] . Han, Seung Ho, George, Sheby Mary, Lee, Ga Yeon, 2017

机译：用于沉积钴基薄膜的新型异钴钴前体
8. Manganese Concentrations in Air Resulting from the Possible Use of Manganese Compounds as a Diesel Fuel Additive and Health Effect Aspects of Manganese [R] . Kuhler, M. , Kraft, J. , Hertel, R. F. 1984

机译：可能使用锰化合物作为柴油添加剂和锰的健康影响因素导致的空气中的锰浓度

Heteroleptic manganese compounds as potential precursors for manganese based thin films and nanomaterials

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