A novel 3D Cd(ii) coordination polymer generated via in situ ligand synthesis involving C-O ester bond formation

Wang Ji-Jiang; Cao Zhuang; Wang Xiao; Tang Long; Hou Xiang-Yang; Ju Ping; Ren Yi-Xia; Chen Xiao-Li; Zhang Yu-Qi

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A novel 3D Cd(ii) coordination polymer generated via in situ ligand synthesis involving C-O ester bond formation

机译：通过涉及C-O酯键形成的原位配体合成产生的新型3D CD（II）配位聚合物

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A novel 3D Cd(ii) coordination polymer {[Cd(ddpa)(2,2-bpy)]H2O}(n) (1) (H(2)ddpa = 5,10-dioxo-5,10-dihydro-4,9-dioxapyrene-2,7-dicarboxylic acid, 2,2-bpy = 2,2-bipyridine) is hydrothermally synthesized in situ, and the influencing factors and mechanism for the in situ reaction are briefly discussed. The synthesis of 1 requires the formation of a new C-O ester bond. This current study confirms that metal ions and N-donor ligands play important roles in the domination of the in situ ligand from 6,6-dinitro-2,2,4,4-biphenyltetracarboxylic acid (H(4)dbta). Furthermore, the structure, thermal stability and photoluminescent property of 1 are also investigated.

机译：新型3D CD（II）配位聚合物{[CD（DDPA）（2,2-BPY）] H2O}（N）（1）（H（2）DDPA = 5,10-二氧氧-5,10-二氢 - 4,9-二氧己酮-2,7-二羧酸，2,2-BPY = 2,2-硼烷烃在原位中合成，并简要讨论了原位反应的影响因素和机制。合成1需要形成新的C-O酯键。本前研究证实，金属离子和N-供体配体在原位配体的统治中起重要作用，从6,6-二硝基-2,2,2,2,2,2,4-联苯基羧酸（H（4）DBTA）。此外，还研究了1的结构，热稳定性和光致发光性。

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来源
《RSC Advances》 |2019年第1期|共6页
作者
Wang Ji-Jiang; Cao Zhuang; Wang Xiao; Tang Long; Hou Xiang-Yang; Ju Ping; Ren Yi-Xia; Chen Xiao-Li; Zhang Yu-Qi;
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Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

Yanan Univ Coll Chem &

Chem Engn Shaanxi Key Lab Chem React Engn Key Lab New Energy &

New Funct Mat Yanan 716000 Peoples R China;

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1. A novel 3D Cd(ii) coordination polymer generated via in situ ligand synthesis involving C-O ester bond formation [J] . Wang Ji-Jiang, Cao Zhuang, Wang Xiao, RSC Advances . 2019,第1期

机译：通过涉及C-O酯键形成的原位配体合成产生的新型3D CD（II）配位聚合物
2. A two-dimensional zinc(II) coordination polymer created via in situ ligand synthesis involving C-N bond formation [J] . Acta crystallographica. Section C, Structural chemistry. . 2015,第2期

机译：通过涉及C-N键形成的原位配体合成产生的二维锌（II）配位聚合物
3. A 3D porous indium(III) coordination polymer involving in-situ ligand synthesis [J] . Han ZB, Song YJ, Ji JW, Journal of Solid State Chemistry . 2009,第11期

机译：涉及原位配体合成的3D多孔铟（III）配位聚合物
4. Synthesis and Crystal Structure of a Novel 3D Sm(III) Coordination Polymer with Mixed Ligands [C] . Shu-ju Wang, Yan-wen Tian, Li-xin You, International Conference on Advanced Engineering Materials and Technology . 2013

机译：用混合配体的新型3D SM（III）配位聚合物的合成与晶体结构
5. I. The synthesis and coordination chemistry of novel 1,1,1-tris(aminomethyl)ethane (TAME) derived ligands and their use as size selective fluorescent zinc(II) sensors. II. The synthesis of strongly and weakly binding ligands with nitrogen, oxygen, and sulfur-donor groups to be used as receptors in fluorescent ratiometric indicators for transition metal ions. [D] . Kennedy, Daniel Patrick. 2007

机译：I.新型1,1,1-三（氨基甲基）乙烷（TAME）衍生的配体的合成和配位化学及其作为尺寸选择荧光锌（II）传感器的用途。二。具有氮，氧和硫供体基团的强结合和弱结合配体的合成，将用作过渡金属离子的荧光比率指示剂中的受体。
6. ‘Metal Complexes as Ligands’ for the Synthesis of Coordination Polymers: A MnIII Monomer as a Building Block for the Preparation of an Unprecedented 1-D {MnIIMnIII}n Linear Chain [O] . Konstantinos N. Pantelis, Georgios Karotsis, Christos Lampropoulos, 2020

机译：用于配位聚合物合成的金属配体配体：MnIII单体作为构建空前的1-D {MnIIMnIII} n线性链的基础
7. Two Coordination Polymers Created via In Situ Ligand Synthesis Involving C-N and C-C Bond Formation [O] . -1

机译：通过原位配体合成产生的两种配位聚合物，涉及C-N和C-C键形成

A novel 3D Cd(ii) coordination polymer generated via in situ ligand synthesis involving C-O ester bond formation

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