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Application of natural deep eutectic solvents to extract ferulic acid from Ligusticum chuanxiong Hort with microwave assistance

机译:自然深共晶溶剂在微波辅助中提取韧带川芎萃取阿魏酸的应用

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摘要

In this study, a method using natural deep eutectic solvents (NADES) combined with microwave-assistance extraction (MAE) was researched for the first time to establish an environmentally-friendly method for extracting ferulic acid from Ligusticum chuanxiong Hort. 20 kinds of NADES were initially screened, then response surface methodology was performed to optimize the NADES-MAE extraction of ferulic acid in L. c on the basis of the results of single-factor experiments. The results demonstrated that NADES could provide better extraction yields of ferulic acid than conventional solvents, and the combination of choline chloride and 1,2-propanediol was the most effective. The optimal conditions were an extraction time of 20 min, an extraction temperature of 68 degrees C, and a solvent-to-solid ratio of 30 : 1 mL g(-1). Under these conditions, the extraction yield of ferulic acid with NADES-MAE (2.32 mg g(-1)) was higher than that using traditional extraction methods. This research demonstrates that this approach, which adopts NADES as a green solvent and MAE as an assistant extraction technique, could be an excellent choice to design an environmentally-friendly method for extracting phenolic compounds in various materials.
机译:在该研究中,首次研究了使用天然深层共晶溶剂(NADE)与微波辅助提取(MAE)结合微波辅助萃取(MAE)的方法,以建立一种从LiGustercum Chuanxiong Hort中提取阿魏酸的环保方法。最初筛选了20种NADE,然后在单因素实验的结果的基础上进行响应表面方法,以优化L.C中的NADE-MAE提取。结果表明,NADES可以提供​​比常规溶剂的更好的萃取产率,并且氯化胆碱和1,2-丙二醇的组合是最有效的。最佳条件是20分钟的提取时间,提取温度为68℃,溶剂至固体比为30:1mL g(-1)。在这些条件下,含有NADES-MAE的阿魏酸的提取产率(2.32mg(-1))高于使用传统提取方法的萃取。该研究表明,这种方法采用NADE作为绿色溶剂和MAE作为助理提取技术,可能是设计一种用于在各种材料中提取酚类化合物的环保方法的绝佳选择。

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  • 来源
    《RSC Advances》 |2019年第39期|共8页
  • 作者单位

    Sichuan Agr Univ Coll Sci Yaan 625014 Sichuan Peoples R China;

    Sichuan Agr Univ Coll Sci Yaan 625014 Sichuan Peoples R China;

    Sichuan Agr Univ Coll Sci Yaan 625014 Sichuan Peoples R China;

    Sichuan Agr Univ Coll Sci Yaan 625014 Sichuan Peoples R China;

    Sichuan Agr Univ Coll Sci Yaan 625014 Sichuan Peoples R China;

    Sichuan Agr Univ Coll Sci Yaan 625014 Sichuan Peoples R China;

    Sichuan Agr Univ Coll Sci Yaan 625014 Sichuan Peoples R China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 化学;
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