Oxone-sodium nitrite mediated N-nitrosamines formation under mild conditions from secondary amines

Pinki Gaur; Shaibal Banerjee

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Oxone-sodium nitrite mediated N-nitrosamines formation under mild conditions from secondary amines

机译：氧源亚硝酸钠介导的仲胺根据温和条件下的N-亚硝胺形成

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摘要

Herein, we report an efficient synthesis of N-nitrosamines from cyclic, aliphatic, benzylic, and aromatic secondary amines via a novel straightforward, efficient, and mild chemical process using sodium nitrite and Oxone in methanol as a solvent at 0-5 °C. The demonstrated methodology accounts well for the parameters like costeffective, short reaction time, clean and safe handling along with good to excellent yields.

机译：在此，我们通过使用亚硝酸钠和在甲醇中的甲醇为0-5℃的溶剂，通过新的简单，高效和温和的化学方法报告来自环状，脂族，苄基和芳族仲胺的N-亚硝胺和芳族化学方法的高效合成。显示的方法账户良好的参数，如性价比，反应时间短，清洁和安全处理以及良好的优良产量。

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来源
《Synthetic Communications》 |2019年第20期|共10页
作者
Pinki Gaur; Shaibal Banerjee;
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作者单位

Department of Applied Chemistry Organic Synthesis Laboratory Defence Institute of Advanced Technology (DU) Girinagar Pune India;

Department of Applied Chemistry Organic Synthesis Laboratory Defence Institute of Advanced Technology (DU) Girinagar Pune India;

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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
N-nitrosamines; Oxone; secondary amines; sodium nitrite;

机译：N-硝基胺;赭石;仲胺;亚硝酸钠;

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专利

1. Oxone-sodium nitrite mediated N-nitrosamines formation under mild conditions from secondary amines [J] . Pinki Gaur, Shaibal Banerjee Synthetic Communications . 2019,第17a20期

机译：氧源亚硝酸钠介导的仲胺根据温和条件下的N-亚硝胺形成
2. Effects of plant polyphenols and alpha-tocopherol on lipid oxidation, residual nitrites, biogenic amines, and N-nitrosamines formation during ripening and storage of dry-cured bacon [J] . Wang Yongli, Li Feng, Zhuang Hong, LWT-Food Science & Technology . 2015,第1期

机译：植物多酚和α-生育酚对干腌培根成熟和储存期间脂质氧化，残留亚硝酸盐，生物胺和N-亚硝胺形成的影响
3. Formation of N-nitrosamines and N-nitramines by the reaction of secondary amines with peroxynitrite and other reactive nitrogen species: comparison with nitrotyrosine formation. [J] . Masuda M, Mower HF, Pignatelli B, Chemical research in toxicology . 2000,第4期

机译：通过仲胺与过氧亚硝酸盐和其他活性氮物质的反应形成N-亚硝胺和N-硝胺：与亚硝基酪氨酸形成的比较。
4. THE HAZARD OF N-NITROSAMINES FORMATION DURING SHORT CHAIN SECONDARY AMINES (DMA, MEA AND DEA) REACTIONS WITH CATALYZED AND NON-CATALYZED HYDROGEN PEROXIDE [C] . P. ANDRZEJEWSKI, N. KULlK International Conference on Environmental Science and Technology . 2007

机译：催化和非催化过氧化氢的短链中仲胺（DMA，MEA和DEA）反应期间N-硝基胺形成的危害
5. Development of a rapid screening procedure for the detection of nitrite, nitrate, and total N-nitrosamine in environmental and physiological samples. [D] . Katz, Mitchell Franklin. 1995

机译：快速检测程序的开发，用于检测环境和生理样品中的亚硝酸盐，硝酸盐和总N-亚硝胺。
6. Formation of N-nitrosamines from seconday animes and nitrite by resting cells of Escherichia coli B. [O] . N Kunisaki, M Hayashi 1979

机译：大肠杆菌B的静止细胞由仲胺和亚硝酸盐形成N-亚硝胺。
7. Conversion of furfural to tetrahydrofuran-derived secondary amines under mild conditions [O] . Shi Jiang, Eric Muller, François Jerôme, 2020

机译：在温和条件下将糠醛转化为四氢呋喃衍生的仲胺

Oxone-sodium nitrite mediated N-nitrosamines formation under mild conditions from secondary amines

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