Metal-substituted tungstosulfates with Keggin structure: synthesis and characterization

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Metal-substituted tungstosulfates with Keggin structure: synthesis and characterization

机译：具有Keggin结构的金属取代钨磺酸盐：合成和表征

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Simple synthetic procedures for accessing novel metal-substituted tungstosulfates [SMW11O39](4-) with Keggin-type structures were developed based on the reaction of metal ions (M = Mn2+, Co2+, Ni2+, and Cu2+) with lacunary tungstosulfate, [SW11O39](6-), which was obtained by treating [SW12O40](2-) with a weak base in acetone. All metal-substituted tungstosulfates were characterized by elemental analysis, X-ray crystallography, ESI-MS, IR, Raman, UV-Vis and cyclic voltammetry analyses.

机译：基于金属离子（M = MN2 +，CO 2 +，Ni2 +和Cu2 +）的金属离子（M = MN2 +，CO 2 +，Ni2 +和Cu2 +），显着具有Keggin型结构的新型金属取代的钨磺酸盐的简单合成方法是基于金属离子（M = MN2 +，CO 2 +，Ni2 +和Cu2 +），[SW11O39] （6-），其通过用丙酮的弱碱处理[SW12O40]（2-）获得。通过元素分析，X射线晶体学，ESI-MS，IR，Raman，UV-Vis和循环伏安法分析来表征所有金属取代的钨磺酸盐。

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《Dalton transactions: An international journal of inorganic chemistry》 |2020年第9期|共5页
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中图分类化学;无机化学;
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1. Metal-substituted tungstosulfates with Keggin structure: synthesis and characterization [J] . Dalton transactions: An international journal of inorganic chemistry . 2020,第9期

机译：具有Keggin结构的金属取代钨磺酸盐：合成和表征
2. New Path for Polyoxometalates: Controlled Synthesis and Characterization of Metal-Substituted Tungstosulfates [J] . Hirabaru Hikaru, Kawamoto Daisuke, Ohnishi Miho, European journal of inorganic chemistry . 2020,第8期

机译：多血清液的新途径：金属取代钨磺酸盐的受控合成及表征
3. About the Keggin Isomers: Crystal Structure of [N(C_4H_9)_4]_4-#gamma#-[SiW_(12)O_(40)], the #gamma#-Isomer of the Keggin Ion. synthesis and ~(183)W NMR Characterization of the Mixed #gamma#-[siMo_2W_(10)O_(40)]~(n-) (n=4 or 6) [J] . Andre Teze, Emmanuel Cadot, Virginie Bereau, Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2001,第9期

机译：关于Keggin异构体：[N（C_4H_9）_4] _4-＃gamma＃-[SiW_（12）O_（40）]的晶体结构，Keggin离子的＃gamma＃-异构体。＃γ＃-[siMo_2W_（10）O_（40）]〜（n-）（n = 4或6）的合成及〜（183）W NMR表征
4. Study on synthesis, characterization and photocatalytic property of FeZrMo heteropoly salt with Keggin structure [C] . Zhihong Zhang, Feng Xue International Conference on Chemical, Material and Metallurgical Engineering . 2012

机译：euzrmo杂盈盐与Keggin结构的合成，表征和光催化性能研究
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7. Hydrothermal synthesis and characterization of one dimensional chain structures of monolacunary Keggin polyoxoanions substituted with copper [O] . Emirdağ Eanes Mehtap, Önen Banu, McMillen Colin D. 2015

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8. Study on Synthesis and Characterization of Large Space Structures. Part 3: Characterization and Synthesis [R] . Arduini, C., Ponzi, U. 1980

机译：大空间结构的合成与表征研究。第3部分：表征和合成

Metal-substituted tungstosulfates with Keggin structure: synthesis and characterization

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