The interconversion between THF center dot B3H7 and B3H8-: an efficient synthetic method for MB3H8 (M = Li and Na)

Liu Xin-Ran; Chen Xi-Meng; Zhang Jie; Jensen Torben R.; Chen Xuenian

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The interconversion between THF center dot B3H7 and B3H8-: an efficient synthetic method for MB3H8 (M = Li and Na)

机译：THF中心点B3H7和B3H8-：MB3H8的有效合成方法（M = LI和NA）之间的相互互连

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摘要

An efficient synthetic method for MB3H8 (M = Li and Na) has been developed with improved yields on the basis of the investigation of the interconversion between THFB3H7 and corresponding MB3H8. The mechanism was tentatively proposed based on the understanding of the nucleophilicity of the B-H bonding pair electrons.

机译：基于对THFB3H7与相应MB3H8的相互互连的研究，开发了MB3H8（M = Li和Na）的有效合成方法，并在研究THFB37和相应的MB3H8之间的互联的基础上进行了改善的产率。基于对B-H粘合对电子的亲核性的理解提出了该机制。

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《Dalton transactions: An international journal of inorganic chemistry》 |2019年第16期|共4页
作者
Liu Xin-Ran; Chen Xi-Meng; Zhang Jie; Jensen Torben R.; Chen Xuenian;
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作者单位

Henan Normal Univ Sch Chem &

Chem Engn Henan Key Lab Boron Chem &

Adv Energy Mat Xinxiang 453007 Henan Peoples R China;

Henan Normal Univ Sch Chem &

Chem Engn Henan Key Lab Boron Chem &

Adv Energy Mat Xinxiang 453007 Henan Peoples R China;

Henan Normal Univ Sch Chem &

Chem Engn Henan Key Lab Boron Chem &

Adv Energy Mat Xinxiang 453007 Henan Peoples R China;

Aarhus Univ Dept Chem CMC Langelandsgade 140 DK-8000 Aarhus Denmark;

Henan Normal Univ Sch Chem &

Chem Engn Henan Key Lab Boron Chem &

Adv Energy Mat Xinxiang 453007 Henan Peoples R China;

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正文语种 eng
中图分类化学;无机化学;
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1. The interconversion between THF center dot B3H7 and B3H8-: an efficient synthetic method for MB3H8 (M = Li and Na) [J] . Liu Xin-Ran, Chen Xi-Meng, Zhang Jie, Dalton transactions: An international journal of inorganic chemistry . 2019,第16期

机译：THF中心点B3H7和B3H8-：MB3H8的有效合成方法（M = LI和NA）之间的相互互连
2. The efficient in-situ reduction and cyclization reaction of aromatic aldehyde, 1,3-cyclopentanedione (tetronic acid), and nitro-compound under SnCl2 center dot 2H(2)O-THF medium [J] . Xu Hui, Li Lei, Dai Lei, Applied Organometallic Chemistry . 2018,第3期

机译：在SnCl2中心点2H（2）O-THF培养基下的芳香醛，1,3-环戊烷（四烷戊酰基）和硝基化合物的有效原位还原和环化反应和硝基化合物
3. Transformation of NHC center dot BEt3 into AgCl center dot NHC: Efficiently preparative method for early-late heterobimetallic complexes using indenyl-functionalized N-heterocyclic carbene as a bridging ligand [J] . Okayama Tetsuya, Watanabe Takashi, Hatayama Yuki, Inorganica Chimica Acta . 2016,第Null期

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4. Comparative investigation of quantum-dot-like localization centers in InGaN quantum well and quantum dot structures [C] . K. Sebald, H. Lohmeyer, J. Gutowski, Symposium on GaN, AIN, InN and Related Materials . 2006

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5. Synthetic methods for the installation of nitrogen-containing quaternary centers in complex bioactive natural products. [D] . Buller, Matthew Jay. 2009

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The interconversion between THF center dot B3H7 and B3H8-: an efficient synthetic method for MB3H8 (M = Li and Na)

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