Monolithic porous magnesium silicide

Hayati-Roodbari N.; Berger R. J. F.; Bernardi J.; Kinge S.; Huesing N.; Elsaesser M. S.

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Monolithic porous magnesium silicide

机译：单片多孔镁硅化物

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Macroporous magnesium silicide monoliths were successfully prepared by a two-step synthesis procedure. The reaction of gaseous magnesium vapor with macro-/mesoporous silicon, which was generated from hierarchically organized meso-/macroporous silica by a magnesiothermic reduction reaction, resulted in monolithic magnesium silicide with a cellular, open macroporous structure. By adjusting the reaction conditions, such as experimental set-up, temperature and time, challenges namely loss of porosity or phase purity of Mg2Si were addressed and monolithic magnesium silicide with a cellular network builtup was obtained.

机译：通过两步合成程序成功制备了大孔镁硅化物整料。气态镁蒸气用宏观/介孔硅的反应，通过镁热还原反应从分层组织的中间/大孔二氧化硅产生，导致整体硅化镁，具有细胞，开放的大孔结构。通过调节反应条件，例如实验设置，温度和时间，挑战即Mg2Si的孔隙率或相纯度的损失，并获得了具有蜂窝网络内置的整体硅化镁。

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《Dalton transactions: An international journal of inorganic chemistry》 |2017年第27期|共6页
作者
Hayati-Roodbari N.; Berger R. J. F.; Bernardi J.; Kinge S.; Huesing N.; Elsaesser M. S.;
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作者单位

Univ Salzburg Chem &

Phys Mat A-5020 Salzburg Austria;

Univ Salzburg Chem &

Phys Mat A-5020 Salzburg Austria;

Tech Univ Wien USTEM A-1040 Vienna Austria;

Toyota Motors Co Europe B-2000 Antwerp Belgium;

Univ Salzburg Chem &

Phys Mat A-5020 Salzburg Austria;

Univ Salzburg Chem &

Phys Mat A-5020 Salzburg Austria;

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正文语种 eng
中图分类化学;无机化学;
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Monolithic porous magnesium silicide

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