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Synthesis and properties of microencapsulated phase change material with a urea-formaldehyde resin shell and paraffin wax core

机译:用尿素 - 甲醛树脂壳和石蜡芯的微胶囊化相变材料的合成与性能

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During this study, paraffin wax with low melting point was encapsulated in a urea-formaldehyde resin to prepare a novel microencapsulated phase change material (Micro-P6) for temperature regulation and thermal energy storage. The structure and properties of Micro-P6 were characterized by using Fourier transform infrared spectroscopy, differential scanning calorimeter, laser particle size analyzer, thermogravimetric analysis, contact angle analysis, and scanning electron microscope. The results indicated that the chemical structure of Micro-P6 meets the designed core-shell structure; and the paraffin wax with low melting point was successfully encapsulated by using urea-formaldehyde resin; and the Micro-P6 shows a spherical structure and rough surface, and the average size is 8.0-10.0 mu m. Then, the performances of Micro-P6, such as core content, mechanical property, thermal conductivity and durability, were tested. Based on above characterization and performance test, it was indicated that the synthesized Micro-P6 could be used in the field of cementing and construction for temperature regulation and thermal energy storage. The applications of Micro-P6 in the field of cementing and construction will be completed in our next study. (c) 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019, 137, 48578.
机译:在该研究期间,用低熔点的石蜡蜡包封在尿素 - 甲醛树脂中,以制备用于温度调节和热能储存的新型微胶囊化相变材料(Micro-P6)。通过使用傅里叶变换红外光谱,差示扫描量热计,激光粒度分析仪,热重分析,接触角分析和扫描电子显微镜,表征了微p6的结构和性质。结果表明,Micro-P6的化学结构符合设计的芯壳结构;通过使用尿素 - 甲醛树脂成功包封具有低熔点的石蜡蜡;并且微p6表示球形结构和粗糙表面,平均尺寸为8.0-10.0μm。然后,测试了Micro-P6的性能,例如核心含量,机械性能,导热性和耐久性。基于以上表征和性能测试,表示合成的Micro-P6可用于胶合和施工领域,用于温度调节和热能储存。微p6在胶结和施工领域的应用将在我们的下一项研究中完成。 (c)2019 Wiley期刊,Inc.J.Phill。聚合物。 SCI。 2019,137,48578。

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