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Amino‐functional electrospun nanofibrous membrane for detecting nitroaromatic compounds

机译：用于检测硝基芳族化合物的氨基功能性电纺纳米纤维膜

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ABSTRACT > A novel amino‐functionalized polystyrene copolymer (PS‐NH <sub>2</sub> ) was designed and synthesized with styrene and 4‐vinylbenzyl amine. Additionally, an amino modified glass (G‐NH <sub>2</sub> ) was obtained as a carrier. (PS‐NH <sub>2</sub> /pyrene)/G‐NH <sub>2</sub> fluorescent nanofibrous membrane [named (PS‐NH <sub>2</sub> /pyrene)/G‐NH <sub>2</sub> ] was designed and prepared via electrospinning technique to detect representative saturated nitroaromatic (NAC) explosive vapor. The (PS‐NH <sub>2</sub> /pyrene)/G‐NH <sub>2</sub> showed highly fluorescence stability in ambient condition and further displayed a high quenching efficiency of 70.9% toward trinitrotoluene (TNT) vapor (～10?ppb) with an exposure time of 150?s at room temperature. The abundance of amino groups could effectively adsorb NACs and the binding of electron‐deficient NACs to the amino groups on the (PS‐NH <sub>2</sub> /pyrene)/G‐NH <sub>2</sub> surface led to the formation of charge‐transfer complexes. The quenching constant ( K <sub>SV</sub> ) to TNT was obtained to be 1.07 × 10 11 ?mL/g in gaseous phase with a limit of detection up to 2.76 × 10 ?13 g/mL. Importantly, the (PS‐NH <sub>2</sub> /pyrene)/G‐NH <sub>2</sub> showed notable selectivity toward TNT and 2,4‐dinitrotoluene vapors. Straightforwardly, the colorimetric sensing performance can be visualized by naked eye with a color change for detecting of different vapor phase NACs explosives. ? 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018 , </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”> <title type =“main”>抽象</ title> >一种新型氨基官能化聚苯乙烯共聚物（PS - 用苯乙烯和4-乙烯基苄基胺设计和合成-NH <sub> 2 </ sub>。另外，获得氨基改性玻璃（G-NH <亚> 2 </ sub>）作为载体。（PS-NH <SUB> 2 </亚> /芘）/ G-NH <亚> 2 </亚>荧光纳米纤维膜[命名（PS-NH <sub> 2 </ sub> /芘）/ g-通过静电纺丝技术设计和制备NH <sub> 2 </ sub>以检测代表性的饱和硝基芳族（NAC）爆炸蒸气。（ps-nh <sub> 2 </ sub> /芘）/ g-nh <sub> 2 </ sup>在环境条件下显示出高荧光稳定性，并进一步展示了朝向三硝基甲苯（TNT）的高70.9％的高淬火效率在室温下蒸汽（〜10·ppb），曝光时间为150Ω秒。氨基的丰度可以有效地吸附NAC和电子缺陷NAC与氨基上的氨基（PS-NH <sub> 2 /亚> /芘）/ G-NH <sub> 2 </ sub>的结合表面导致形成电荷转移复合物。在气相中获得至TNT的淬火常数（ k / i> <亚> sv sv ）以极限为1.07×10 11 / g的气相相中高达2.76×10 ？13 </ sup> g / ml。重要的是，（PS-NH <Sub> 2 </ sub> /芘）/ G-NH <sub> 2 </ sub>对TNT和2,4-二硝基甲苯蒸汽显示出显着的选择性。直截了当的，比色感测性能可以通过肉眼可视化，具有颜色变化，用于检测不同的气相NACS爆炸物。还是2018 Wiley期刊，Inc.J.Phill。聚合物。 SCI。 2018 </ b>， </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-33581/'>《Journal of Applied Polymer Science》</a> <b style="margin: 0 2px;">|</b><span>2018年第40期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yu Run‐Hui&option=202" target="_blank" rel="nofollow">Yu Run‐Hui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Kai&option=202" target="_blank" rel="nofollow">Li Kai;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cui Yue‐Zhi&option=202" target="_blank" rel="nofollow">Cui Yue‐Zhi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tao Fu‐Rong&option=202" target="_blank" rel="nofollow">Tao Fu‐Rong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zheng Bing&option=202" target="_blank" rel="nofollow">Zheng Bing;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ma Xiao‐Shuang&option=202" target="_blank" rel="nofollow">Ma Xiao‐Shuang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Tian‐Duo&option=202" target="_blank" rel="nofollow">Li Tian‐Duo;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Shandong Provincial Key Laboratory of Fine Chemicals School of Chemistry and Pharmaceutical EngineeringQiLu University of TechnologyJinan 250353 China;</p> <p>Shandong Provincial Key Laboratory of Fine Chemicals School of Chemistry and Pharmaceutical EngineeringQiLu University of TechnologyJinan 250353 China;</p> <p>Shandong Provincial Key Laboratory of Fine Chemicals School of Chemistry and Pharmaceutical EngineeringQiLu University of TechnologyJinan 250353 China;</p> <p>Shandong Provincial Key Laboratory of Fine Chemicals School of Chemistry and Pharmaceutical EngineeringQiLu University of TechnologyJinan 250353 China;</p> <p>Shandong Provincial Key Laboratory of Fine Chemicals School of Chemistry and Pharmaceutical EngineeringQiLu University of TechnologyJinan 250353 China;</p> <p>Shandong Provincial Key Laboratory of Fine Chemicals School of Chemistry and Pharmaceutical EngineeringQiLu University of TechnologyJinan 250353 China;</p> <p>Shandong Provincial Key Laboratory of Fine Chemicals School of Chemistry and Pharmaceutical EngineeringQiLu University of TechnologyJinan 250353 China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1821.html" title="高分子化合物工业（高聚物工业）">高分子化合物工业（高聚物工业）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=applications&option=203" rel="nofollow">applications;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanoparticles&option=203" rel="nofollow">nanoparticles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanowires and nanocrystals&option=203" rel="nofollow">nanowires and nanocrystals;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=non‐polymeric materials and composites&option=203" rel="nofollow">non‐polymeric materials and composites;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=optical and photovoltaic applications&option=203" rel="nofollow">optical and photovoltaic applications;</a> </p> <div class="translation"> 机译：应用;纳米粒子;纳米线和纳米晶体;非聚合物材料和复合材料;光学和光伏应用; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" 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