Influence of annealing time on linear rheology and morphology of silica filled polyisoprene rubber and ethylene-propylene rubber

Xie Zhou; Xu Yiting; Song Yihu; Zheng Qiang

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Influence of annealing time on linear rheology and morphology of silica filled polyisoprene rubber and ethylene-propylene rubber

机译：退火时间对二氧化硅填充聚异戊二烯橡胶和乙烯 - 丙烯橡胶线性流变学及形态的影响

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Dynamic rheology in combination of fluorescence and molecular weight analysis was carried out to explore annealing-induced structural evolutions in silica filled polyisoprene rubber (IR) and ethylene-propylene rubber compounds containing rhodamine B modified silica of 2.5% in volume fraction. The results show that storage modulus of the ethylene-propylene rubber compounds increases slightly with increasing annealing time while that of the IR compounds exhibits a peaking behavior at mediate silica contents. Fluorescence tests reveal that the silica agglomerates in both compounds while the agglomeration is more significant in the IR ones. Molecular weight analysis shows that IR in the compounds undergoes degradation during the annealing. (c) 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018, 135, 46679.

机译：荧光和分子量分析组合的动态流变学进行了探讨二氧化硅填充聚异戊二烯橡胶（IR）和含有罗丹明B改性二氧化硅的乙二醇丙烯橡胶化合物在体积分数中的退火诱导的结构演进。结果表明，乙烯 - 丙烯橡胶化合物的储存模量随着退火时间的增加而略有增加，而IR化合物的含量在介导的二氧化硅含量上表现出峰值行为。荧光试验表明，两种化合物中的二氧化硅凝聚，而在IR组中的聚集在附聚中更显着。分子量分析表明，化合物中的IR在退火过程中经历降解。（c）2018 Wiley期刊，Inc.J.Phill。聚合物。 SCI。 2018,135,46679。

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《Journal of Applied Polymer Science》 |2018年第36期|共11页
作者
Xie Zhou; Xu Yiting; Song Yihu; Zheng Qiang;
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作者单位

Zhejiang Univ Dept Polymer Sci &

Engn MOE Key Lab Macromol Synth &

Functionalizat Hangzhou 310027 Peoples R China;

Zhejiang Univ Dept Polymer Sci &

Engn MOE Key Lab Macromol Synth &

Functionalizat Hangzhou 310027 Peoples R China;

Zhejiang Univ Dept Polymer Sci &

Engn MOE Key Lab Macromol Synth &

Functionalizat Hangzhou 310027 Peoples R China;

Zhejiang Univ Dept Polymer Sci &

Engn MOE Key Lab Macromol Synth &

Functionalizat Hangzhou 310027 Peoples R China;

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原文格式 PDF
正文语种 eng
中图分类高分子化合物工业（高聚物工业）;
关键词
composites; microscopy; rheology; spectroscopy; structure-property relationships;

机译：复合材料;显微镜;流变学;光谱学;结构性质关系;

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1. Influence of annealing time on linear rheology and morphology of silica filled polyisoprene rubber and ethylene-propylene rubber [J] . Xie Zhou, Xu Yiting, Song Yihu, Journal of Applied Polymer Science . 2018,第35a36期

机译：退火时间对二氧化硅填充聚异戊二烯橡胶和乙烯 - 丙烯橡胶线性流变学及形态的影响
2. Influence of immobilized rubber on the non-linear viscoelasticity of filled silicone rubber with different interfacial interaction of silica [J] . Hanmei Zhou, Lixian Song, Ai Lu, RSC Advances . 2016,第18期

机译：固定化橡胶对具有二氧化硅不同界面相互作用的填充硅橡胶非线性粘弹性的影响
3. Morphology evolution and dynamic relaxation behavior of solution-polymerized styrene-butadiene rubber/polyisoprene/silica ternary composites influenced by shear [J] . Liu Xianggui, Dong Xia, Liu Wei, Polymer: The International Journal for the Science and Technology of Polymers . 2018,第期

机译：剪切影响的溶液聚合苯乙烯 - 丁二烯橡胶/聚异戊二烯/二氧化硅三元复合材料的形态演化和动态松弛行为
4. The Influence of Recycled Poly(ethylene terephthalate) Powder on Fatigue Life, Thermal Stability, and Morphology of Halloysite Nanotubes (HNTs) and Precipitated Silica Filled Natural Rubber Composites [C] . H. Nabil, H. Ismail, A.R. Azura ICCST8;International Conference on Composite Science and Technology . 2011

机译：再生聚对苯二甲酸乙二醇酯粉末对埃洛石纳米管（HNTs）和沉淀二氧化硅填充天然橡胶复合材料的疲劳寿命，热稳定性和形态的影响
5. NMR studies of carbon black filled, accelerated sulfur-vulcanization of natural rubber and cis-polyisoprene. [D] . Mori, Makio. 1997

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6. Rubber-Filler Interactions in Polyisoprene Filled with In Situ Generated Silica: A Solid State NMR Study [O] . Silvia Borsacchi, Umayal Priyadharsini Sudhakaran, Lucia Calucci, 2018

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Influence of annealing time on linear rheology and morphology of silica filled polyisoprene rubber and ethylene-propylene rubber

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