Initiator‐free atom transfer radical polymerization of methyl methacrylate based on FeBr <sub xmlns='http://www.wiley.com/namespaces/wiley'>3</sub>3 (PPh <sub xmlns='http://www.wiley.com/namespaces/wiley'>3</sub>3 ) <sub xmlns='http://www.wiley.com/namespaces/wiley'> n </sub> <i xmlns='http://www.wiley.com/namespaces/wiley'>nn system

Yang Danfeng; Wang Jirong; Han Jianyu; Khan Mohd Yusuf; Xie Xiaolin; Xue Zhigang

摘要

ABSTRACT > A tricomponent system, constituting monomer (methyl methacrylate, MMA), higher oxidation state transition‐metal catalyst (FeBr <sub>3</sub> ) and a ligand (triphenylphosphine, PPh <sub>3</sub> ), MMA/FeBr <sub>3</sub> /PPh <sub>3</sub> system without external initiator (alkyl halide) has been studied extensively with different spectroscopic analyses. To figure out the mechanism, a series of explicit model reactions were conducted with a molar ratio of [MMA] <sub>0</sub> /[FeBr <sub>3</sub> ] <sub>0</sub> /[PPh <sub>3</sub> ] <sub>0</sub> ?=?200/1/ n ( n ?=?0.1–3.0) at 80 °C, and the corresponding polymerization behaviors were investigated. Combined with theoretical deduction and spectroscopic evidences, the composition of the in‐situ generated initiators was gradually confirmed, which were redox products of FeBr <sub>3</sub> and PPh <sub>3</sub> . ? 2017 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2017 , 55 , 3842–3850 </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><抽象的xmlns = “http://www.wiley.com/namespaces/wiley” 类型= “主”> <标题类型= “主”>摘要</ TITLE> >一个三组分系统中，构成单体（甲基丙烯酸甲酯，MMA），较高氧化态的过渡金属催化剂（FeBr <子> 3 </子>）和配体（三苯基膦，PPH <子> 3 </子>），MMA / FeBr <子> 3 </子> / PPH <子> 3 </子>没有外部引发剂（烷基卤化物）系统已被广泛地用不同的分光分析研究。找出机构，一系列显式模型反应用的摩尔比进行的[MMA] <子> 0 </子> / [FeBr <子> 3 </子>] <子> 0 </子> / [PPH <子> 3 </子>] <子> 0 </子> =ρ200/1 / 名词</ i>的（名词</ i>的？=？0.1-3.0 ）在80℃下，和对应的聚合行为进行了研究。与理论推导和光谱证据，的<I>原位</ i>的生成的引发剂逐渐确认，这是氧化还原产品FeBr <子> 3 </子>和PPH <子> 3 </所述组合物组合子>。还是2017 Wiley期刊，Inc.J.Colom。 SCI。，A部分：polym。化学。 <B> 2017 </ B>，<I> 55 </ i>的，3842-3850 </ p> </抽象> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35621/'>《Journal of Polymer Science, Part A. Polymer Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2017年第23期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Danfeng&option=202" target="_blank" rel="nofollow">Yang Danfeng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Jirong&option=202" target="_blank" rel="nofollow">Wang Jirong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Han Jianyu&option=202" target="_blank" rel="nofollow">Han Jianyu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Khan Mohd Yusuf&option=202" target="_blank" rel="nofollow">Khan Mohd Yusuf;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xie Xiaolin&option=202" target="_blank" rel="nofollow">Xie Xiaolin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xue Zhigang&option=202" target="_blank" rel="nofollow">Xue Zhigang;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Key Laboratory for Material Chemistry of Energy Conversion and Storage Ministry of Education School of Chemistry and Chemical EngineeringHuazhong University of Science and TechnologyWuhan 430074 China;</p> <p>Key Laboratory for Material Chemistry of Energy Conversion and Storage Ministry of Education School of Chemistry and Chemical EngineeringHuazhong University of Science and TechnologyWuhan 430074 China;</p> <p>Key Laboratory for Material Chemistry of Energy Conversion and Storage Ministry of Education School of Chemistry and Chemical EngineeringHuazhong University of Science and TechnologyWuhan 430074 China;</p> <p>Center of Research Excellence in Nanotechnology King Fahad University of Petroleum &</p> <p>MineralsDhahran 31261 Saudi Arabia;</p> <p>Key Laboratory for Material Chemistry of Energy Conversion and Storage Ministry of Education School of Chemistry and Chemical EngineeringHuazhong University of Science and TechnologyWuhan 430074 China;</p> <p>Key Laboratory for Material Chemistry of Energy Conversion and Storage Ministry of Education School of Chemistry and Chemical EngineeringHuazhong University of Science and TechnologyWuhan 430074 China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1184.html" title="有机化学">有机化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=atom transfer radical polymerization (ATRP)&option=203" rel="nofollow">atom transfer radical polymerization (ATRP);</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=in‐situ generated initiators&option=203" rel="nofollow">in‐situ generated initiators;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=initiator‐free ATRP&option=203" rel="nofollow">initiator‐free ATRP;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=kinetics (polym.)&option=203" rel="nofollow">kinetics (polym.);</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=living polymerization&option=203" rel="nofollow">living polymerization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=mechanism&option=203" rel="nofollow">mechanism;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=MMA/FeBr3/PPh3 system&option=203" rel="nofollow">MMA/FeBr3/PPh3 system;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=spectroscopic analyses&option=203" rel="nofollow">spectroscopic analyses;</a> </p> <div class="translation"> 机译：原子转移自由基聚合（ATRP）;原位生成的引发剂;免疫增生ATRP;动力学（Polym。）;生物聚合;机制;MMA / FEBR3 / PPH3系统;光谱分析; 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mml：mi> </ mml：mrow> </ mml：msub> </ mml：math>在p–Pb中<mml：math处发生碰撞altimg =“ si2.gif”溢出=“滚动” xmlns：xocs =“ http://www.elsevier.com/xml/xocs/dtd” xmlns：xs =“ http：// www。 w3.org/2001/XMLSchema” xmlns：xsi =“ http://www.w3.org/ 2001 / XMLSchema-instance“ xmlns =” http://www.elsevier.com/xml/ja/dtd“ xmlns：ja =” http://www.elsevier.com/xml/ja/dtd“ xmlns：mml = “ http://www.w3.org/1998/Math/MathML” xmlns：tb =“ http://www.elsevier.com/xml/common/table/dtd” xmlns：sb =“ http：// www .elsevier.com / xml / common / struct-bib / dtd“ xmlns：ce =” http://www.elsevier.com/xml/common/dtd“ xmlns：xlink =” http://www.w3.org / 1999 / xlink“ xmlns：cals =” http://www.elsevier.com/xml/common/cals/dtd“ xmlns：sa =” http://www.elsevier.com/xml/common/struct-aff / dtd“> <mml：msqrt> <mml：msub> <mml：mrow> <mml：mi> s </ mml：mi> </ mml：mrow> <mml：mrow> <mml：mi mathvariant =”正常“> NN </ mml：mi> </ mml：mrow> </ mml：msub> </ mml：msqrt> <mml：mo> = </ mml：mo> <mml：mn> 5.02 </ mml：mn > <mml：mtext> TeV </ mml：mtext> </ mml：math></span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06130430441865.html">Method and system for processing HTTP requests creating a new map for an entire namespace that is associated with the request and that maps the name extension to the further content type within namespace</a> <b>[P]</b> . <span> 外国专利：  US7457805B2 </span> <span> . 2008-11-25</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于处理HTTP请求的方法和系统，用于为与该请求相关联的整个名称空间创建新映射，并将名称扩展名映射到名称空间内的其他内容类型 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > 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Initiator‐free atom transfer radical polymerization of methyl methacrylate based on FeBr 33 (PPh 33 ) n nn system

摘要

Initiator‐free atom transfer radical polymerization of methyl methacrylate based on FeBr ₃3 (PPh ₃3 ) _n nn system