Solvent free oxidative coupling polymerization of 3-hexylthiophene (3HT) in the presence of FeCl3 particles

Hirai T.; Nagae Y.; White K. L.; Kamitani K.; Kido M.; Uchiyama T.; Nishibori M.; Konishi Y.; Yokomachi K.; Sugimoto R.; Saigo K.; Ohishi T.; Higaki Y.; Kojio K.; Takahara A.

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Solvent free oxidative coupling polymerization of 3-hexylthiophene (3HT) in the presence of FeCl3 particles

机译：在FECL3颗粒存在下，3-己基噻吩（3HT）的溶剂无氧化偶联聚合

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摘要

A solvent free oxidative coupling reaction of 3-hexylthiophene (3HT) within a nanocavity is reported. It is found that 3HT can be encapsulated in nanocavities larger than 1 nm, which corresponds to the size of the molecule. In this case, the side reaction at the 4-position in 3HT is regulated.

机译：报道了3-己基噻吩（3Ht）内的溶剂无氧化偶联反应在纳米恒温内。发现3HT可以封装在大于1nm的纳米覆盖物中，这对应于分子的尺寸。在这种情况下，调节在3HT中的4位的副反应。

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来源
《RSC Advances》 |2016年第113期|共4页
作者
Hirai T.; Nagae Y.; White K. L.; Kamitani K.; Kido M.; Uchiyama T.; Nishibori M.; Konishi Y.; Yokomachi K.; Sugimoto R.; Saigo K.; Ohishi T.; Higaki Y.; Kojio K.; Takahara A.;
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作者单位

Kyushu Univ Grad Sch Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Grad Sch Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Int Inst Carbon Neutral Energy Res WPI I2CNER Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Inst Mat Chem &

Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Grad Sch Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Fac Engn Sci 6-1 Kasugakoen Kasuga Fukuoka 8168580 Japan;

Kyushu Univ Fac Engn Sci 6-1 Kasugakoen Kasuga Fukuoka 8168580 Japan;

Kyushu Univ Inst Mat Chem &

Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Inst Mat Chem &

Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kochi Univ Technol Sch Environm Sci &

Engn Kami Kochi 7828502 Japan;

Kochi Univ Technol Sch Environm Sci &

Engn Kami Kochi 7828502 Japan;

Kyushu Univ Inst Mat Chem &

Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Grad Sch Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Grad Sch Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

Kyushu Univ Grad Sch Engn Nishi Ku 744 Motooka Fukuoka 8190395 Japan;

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正文语种 eng
中图分类化学;
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1. Solvent free oxidative coupling polymerization of 3-hexylthiophene (3HT) in the presence of FeCl3 particles [J] . Hirai T., Nagae Y., White K. L., RSC Advances . 2016,第113期

机译：在FECL3颗粒存在下，3-己基噻吩（3HT）的溶剂无氧化偶联聚合
2. Poly(3-hexylthiophene) Grains Synthesized by Solvent-Free Oxidative Coupling Polymerization and Their Use as Light-Responsive Liquid Marble Stabilizer [J] . Inoue Hiroki, Hirai Tomoyasu, Hanochi Haruka, Macromolecules . 2019,第2期

机译：聚（3-己基噻吩）通过无溶剂氧化偶联聚合合成的晶粒及其用作轻响应液体大理石稳定剂
3. Synthesis of anisotropic polymer particles with soap-free emulsion polymerization in the presence of a reactive silane coupling agent [J] . Nagao D, Hashimoto M, Hayasaka K, Macromolecular rapid communications: Publishing the newsletters of the European Polymer Federation . 2008,第17期

机译：在反应性硅烷偶联剂存在下用无皂乳液聚合法合成各向异性聚合物颗粒
4. Binary Fe and Mn Oxide Nanoparticle Supported Polymeric Anion Exchanger for Arsenic Adsorption: Role of Oxides, Supported Materials, and Preparation Solvent [C] . Antika Pranudta, Pornsawai Praipipat, Medhat Mohamed EI-Moselhy International Engineering Conference . 2017

机译：二元Fe和Mn氧化物纳米颗粒负载用于砷吸附的聚合物阴离子交换剂：氧化物，负载材料和制备溶剂的作用
5. New developments using carbon dioxide as a solvent: Monolayers and nanocomposites. 1. Reactions of organosilanes with oxidized silicon surfaces in carbon dioxide. 2. Polymer/polymer nanocomposites synthesized in carbon dioxide. [D] . Cao, Chuntao. 2002

机译：使用二氧化碳作为溶剂的新发展：单层和纳米复合材料。 1.有机硅烷与二氧化碳中氧化的硅表面的反应。 2.在二氧化碳中合成的聚合物/聚合物纳米复合材料。
6. Self-Assembly of Polymer-Grafted Nanoparticles in Solvent-freeConditions [O] . Alexandros Chremos, Jack F. Douglas -1

机译：无溶剂的聚合物接枝纳米颗粒的自组装条件
7. Polymerization of 3-hexylthiophene with FeCl3 in aromatic solvents [O] . Liu Yi, Nishiwaki Nagatoshi, Saigo Kazuhiko, 2015

机译：3-己基噻吩与FeCl3在芳族溶剂中的聚合

Solvent free oxidative coupling polymerization of 3-hexylthiophene (3HT) in the presence of FeCl3 particles

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