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Synthesis of a novel ferrocene-based epoxy compound and its burning rate catalytic property

机译：基于二茂铁基环氧化合物的合成及其燃烧率催化性能

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摘要

3-(Ferrocenylcarbonyl) propionic acid diglycidyl ester (FCPADE) was synthesized by Friedel-Craft acylation of ferrocene with succinic anhydride followed by reaction with epichlorohydrin. The synthesis of FCPADE was confirmed by H-1-NMR, C-13-NMR, MS and FT-IR. The electrochemical behavior and catalytic performance on decomposition of ammonium perchlorate (AP) were investigated. The results showed that FCPADE has a good catalytic effect on lowering the thermal decomposition temperature of AP. Anti-migration studies showed that FCPADE has a better anti-migration performance than ferrocene and catocene.
机译：用琥珀酸铁素酰化与琥珀酸酐的Friedel-Craft酰化合成3-（二氧化羰基羰基）丙酸二缩水甘油酯（FCPADE），然后与表氯醇反应。 通过H-1-NMR，C-13-NMR，MS和FT-IR确认FCPADE的合成。 研究了对高氯酸铵（AP）分解的电化学行为和催化性能。 结果表明，FCPADE对降低AP的热分解温度具有良好的催化作用。 反迁移研究表明，FCPADE具有比二茂铁和树胶的更好的抗迁移性能。

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  • 来源
    《RSC Advances》 |2016年第59期|共9页
  • 作者

    Zhou Weidong; Wang Li; Yu Haojie; Zain-ul-Abdin; Yang Xianpeng; Chen Qing; Wang Junhua;

  • 作者单位

    Zhejiang Univ State Key Lab Chem Engn Coll Chem &

    Biol Engn Hangzhou 310027 Zhejiang Peoples R China;

    Zhejiang Univ State Key Lab Chem Engn Coll Chem &

    Biol Engn Hangzhou 310027 Zhejiang Peoples R China;

    Zhejiang Univ State Key Lab Chem Engn Coll Chem &

    Biol Engn Hangzhou 310027 Zhejiang Peoples R China;

    Zhejiang Univ State Key Lab Chem Engn Coll Chem &

    Biol Engn Hangzhou 310027 Zhejiang Peoples R China;

    Zhejiang Univ State Key Lab Chem Engn Coll Chem &

    Biol Engn Hangzhou 310027 Zhejiang Peoples R China;

    Zhejiang Univ State Key Lab Chem Engn Coll Chem &

    Biol Engn Hangzhou 310027 Zhejiang Peoples R China;

    Zhejiang Univ State Key Lab Chem Engn Coll Chem &

    Biol Engn Hangzhou 310027 Zhejiang Peoples R China;

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  • 正文语种 eng
  • 中图分类 化学;
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