Synthesis, characterization and application of MCM-22 zeolites via a conventional HMI route and temperature-controlled phase transfer hydrothermal synthesis

Xing Enhui; Shi Yanchun; Xie Wenhua; Zhang Fengmei; Mu Xuhong; Shu Xingtian

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Synthesis, characterization and application of MCM-22 zeolites via a conventional HMI route and temperature-controlled phase transfer hydrothermal synthesis

机译：通过常规HMI途径和温度控制相移水热合成的MCM-22沸石的合成，表征和应用

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With less environmental and economical impact, temperature-controlled phase transfer hydrothermal synthesis of MWW zeolites was realized with hexamethyleneimine as a structure-directing agent and aniline as a structure-promoting agent. MCM-22 zeolite, synthesized via temperature-controlled phase transfer hydrothermal synthesis, is nearly identical concerning chemical composition and structure, and possesses nearly identical properties with respect to porosity, Si/Al ratio, thermal behavior and catalytic activity at 200 degrees C, compared with that made from conventional synthesis with hexamethyleneimine as the only template.

机译：由于环境和经济的影响较少，用六亚甲基亚胺作为结构引导剂和苯胺作为结构促进剂实现了MWW沸石的温度控制相移水热合成。通过温度控制相转移水热合成合成的MCM-22沸石几乎与化学成分和结构相同，相对于200摄氏度的孔隙率，Si / Al比，热行为和催化活性具有几乎相同的性质用常规合成与六亚甲基亚胺制成的唯一模板。

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《RSC Advances》 |2015年第11期|共9页
作者
Xing Enhui; Shi Yanchun; Xie Wenhua; Zhang Fengmei; Mu Xuhong; Shu Xingtian;
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作者单位

Sinopec Res Inst Petr Proc State Key Lab Catalyt Mat &

React Engn Beijing 100083 Peoples R China;

Sinopec Res Inst Petr Proc State Key Lab Catalyt Mat &

React Engn Beijing 100083 Peoples R China;

Sinopec Res Inst Petr Proc State Key Lab Catalyt Mat &

React Engn Beijing 100083 Peoples R China;

Sinopec Res Inst Petr Proc State Key Lab Catalyt Mat &

React Engn Beijing 100083 Peoples R China;

Sinopec Res Inst Petr Proc State Key Lab Catalyt Mat &

React Engn Beijing 100083 Peoples R China;

Sinopec Res Inst Petr Proc State Key Lab Catalyt Mat &

React Engn Beijing 100083 Peoples R China;

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正文语种 eng
中图分类化学;
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1. Synthesis, characterization and application of MCM-22 zeolites via a conventional HMI route and temperature-controlled phase transfer hydrothermal synthesis [J] . Xing Enhui, Shi Yanchun, Xie Wenhua, RSC Advances . 2015,第11期

机译：通过常规HMI途径和温度控制相移水热合成的MCM-22沸石的合成，表征和应用
2. Temperature-controlled phase-transfer hydrothermal synthesis of MWW zeolites and their alkylation performances [J] . Xing Enhui, Shi Yanchun, Xie Wenhua, RSC Advances . 2016,第35期

机译：温度控制的相转移水热合成MWW沸石及其烷基化性能
3. Synthesis and characterization of zeolites using phenyltrimethylammonium hydroxide (PTMAOH) as template by conventional hydrothermal and microwave assisted methods [J] . Samadi-Maybodi Abdolraouf, Azizi S. Nasser, Yarmohammadi Mohammad Journal of the Indian Chemical Society . 2014,第10期

机译：常规水热和微波辅助方法以苯基三甲基氢氧化铵（PTMAOH）为模板合成和表征沸石
4. Preparation and characterization of MCM-22 zeolite by varying-temperature hydrothermal synthesis [C] . Yue Cheng, Xiao-yuan Su, Mang Lu International Conference on Manufacturing Science and Engineering . 2011

机译：不同温度水热合成的MCM-22沸石的制备与表征
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

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Synthesis, characterization and application of MCM-22 zeolites via a conventional HMI route and temperature-controlled phase transfer hydrothermal synthesis

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