Total synthesis of (+)-petromyroxol via tandem alpha-aminoxylation-allylation and asymmetric dihydroxylation-S(N)2 cyclization approach

Nookaraju U.; Kumar Pradeep

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Total synthesis of (+)-petromyroxol via tandem alpha-aminoxylation-allylation and asymmetric dihydroxylation-S(N)2 cyclization approach

机译：通过串联α-氨基氧基化 - 烯丙基化和不对称二羟基化-S（n）2环化方法的总合成（+） - 甲状腺氧基醇

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摘要

The total synthesis of (+)-petromyroxol, a tetrahydrofuran (THF)-diol fatty acid, isolated from sea lamprey larvae (Petromyzon marinus) is reported. The present synthesis employs a tandem alpha-aminoxylationallylation, cross metathesis and tandem asymmetric dihydroxylation-S(N)2 cyclization as key steps.

机译：报道了（+） - 甲状腺氧基，四氢呋喃（THF）二醇脂肪酸的总合成，从海绵Pherey幼虫（Petromyzon Marinus）。本合成采用串联α-氨基氧基化，交叉复分解和串联不对称二羟基化-S（n）2环化作为关键步骤。

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《RSC Advances》 |2015年第78期|共7页
作者
Nookaraju U.; Kumar Pradeep;
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CSIR Natl Chem Lab Div Organ Chem Pune 411008 Maharashtra India;

CSIR Natl Chem Lab Div Organ Chem Pune 411008 Maharashtra India;

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正文语种 eng
中图分类化学;
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专利

1. Total synthesis of (+)-petromyroxol via tandem alpha-aminoxylation-allylation and asymmetric dihydroxylation-S(N)2 cyclization approach [J] . Nookaraju U., Kumar Pradeep RSC Advances . 2015,第78期

机译：通过串联α-氨基氧基化 - 烯丙基化和不对称二羟基化-S（n）2环化方法的总合成（+） - 甲状腺氧基醇
2. Total synthesis of (+)-monocerin via tandem dihydroxylation-S_N2 cyclization and a copper mediated tandem cyanation-lactonization approach [J] . U. Nookaraju, Eeshwaraiah Begari, Pradeep Kumar Organic & biomolecular chemistry . 2014,第31期

机译：通过串联二羟基化-S_N2环化和铜介导的串联氰化-内酯化法合成（+）-甘油
3. Stereodivergent total asymmetric synthesis of polyhydroxylated pyrrolidines via tandem allylic epoxidation and intramolecular cyclization reactions [J] . Satwinder Singh, Hyunsoo Han Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2004,第33期

机译：通过串联烯丙基环氧化和分子内环化反应的立体发散完全不对称合成多羟基吡咯烷
4. ANIONIC CYCLIZATION APPROACH TOWARD PERHYDROINDOLONES: APPLICATION TO THE TOTAL SYNTHESIS OF ALKALOIDS [C] . Chin-Kang Sha International symposium for Chinese organic chemists . 2000

机译：对氯羟酮酮的阴离子环化方法：应用于生物碱的总合成
5. Part I: Total Synthesis of (+/-)-Pallambins C and D, and, Part II: Gold-Catalyzed Tandem Cyclization towards Substituted Bicyclo[3.2.1]Octenone Derivatives: Lead to Total Synthesis of Dhilirolides A-D. [D] . Xu, Xuesong. 2013

机译：第一部分：（+/-）-戊二烯C和D的全合成，第二部分：金催化的串联环化反应取代双环[3.2.1]大黄酮衍生物：导致Dhilirolides A-D的全合成。
6. Synthesis of Polycyclic Benzofused Nitrogen Heterocycles via a Tandem Ynamide Benzannulation/Ring Closing Metathesis Strategy. Application in a Formal Total Synthesis of (+)-FR900482 [O] . Xiao Yin Mak, Aimee L. Crombie, Rick L. Danheiser -1

机译：经由串联炔酰胺苯并环化/环多环苯并稠氮合成杂环闭合置换策略。在正式的全合成（+）应用 - FR900482
7. A Formal Total Synthesis of (-)-FR901483, Using a Tandem Cationic Aza-Cope Rearrangement/Mannich Cyclization Approach [O] . -1

机译：（ - ） - FR901483的正式合成，使用串联阳离子AZA-COPE重排/曼尼希旋转方法

Total synthesis of (+)-petromyroxol via tandem alpha-aminoxylation-allylation and asymmetric dihydroxylation-S(N)2 cyclization approach

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