Total synthesis of Sparstolonin B, a potent anti-inflammatory agent

Wang Yongqiang; Wang Chao; Wang Yuanxun; Dong Lijin; Sun Jian

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Total synthesis of Sparstolonin B, a potent anti-inflammatory agent

机译：总合成Sparstolonin B，有效的抗炎剂

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Two concise routes for the first total synthesis of Sparstolonin B (SsnB) have been described. The synthesis of SsnB could be accomplished in 5 and 6 steps with 40% and 38% overall yield, respectively. The rhodium-catalysed oxidative coupling of benzoic acid with internal alkyne was used in both strategies to construct the core structure of SsnB.

机译：已经描述了用于第一个总合成的Sparstolonin B（SSNB）的简明途径。 SSNB的合成可以分别在5个和6步中完成，分别为40％和38％的总屈服。在两种策略中使用苯甲酸与内甲酸的铑催化氧化偶联以构建SSNB的核心结构。

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《RSC Advances》 |2015年第16期|共4页
作者
Wang Yongqiang; Wang Chao; Wang Yuanxun; Dong Lijin; Sun Jian;
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Chinese Acad Sci Chengdu Inst Biol Chengdu 610041 Peoples R China;

Chinese Acad Sci Chengdu Inst Biol Chengdu 610041 Peoples R China;

Chinese Acad Sci Chengdu Inst Biol Chengdu 610041 Peoples R China;

Chinese Acad Sci Chengdu Inst Biol Chengdu 610041 Peoples R China;

Chinese Acad Sci Chengdu Inst Biol Chengdu 610041 Peoples R China;

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正文语种 eng
中图分类化学;
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1. Total synthesis of Sparstolonin B, a potent anti-inflammatory agent [J] . Wang Yongqiang, Wang Chao, Wang Yuanxun, RSC Advances . 2015,第16期

机译：总合成Sparstolonin B，有效的抗炎剂
2. Total synthesis and biological evaluation of viscolin, a 1,3-diphenylpropane as a novel potent anti-inflammatory agent. [J] . Su CR, Shen YC, Kuo PC, Bioorganic and Medicinal Chemistry Letters . 2006,第24期

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3. Antitumor agents. 271: total synthesis and evaluation of brazilein and analogs as anti-inflammatory and cytotoxic agents. [J] . Yen CT, Nakagawa Goto K, Hwang T Bioorganic and Medicinal Chemistry Letters . 2010,第3期

机译：抗肿瘤剂。 271：含有抗炎和细胞毒剂的碱和类似物的总合成和评价。
4. Design, Synthesis and Characterisation of Potent Anti-inflammatory Peptidomimetics [C] . Andras Varga, Monika Huszar, Gyorgy Keri International Peptide Symposium . 2009

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5. Synthesis and Utility of New Ynamide and Organo-allyltrifluoroborate Reagents: Application to the Total Synthesis of Geralcin A, Hydrazidomycins A-B, (±)-CPC–1, (±)-Alline, Splenocin-B, and the Potent Cancer Cell Growth Inhibitors Kitastatin and Respirantin [D] . Beveridge, Ramsay Eaton 2014

机译：新型酰胺和有机烯丙基三氟硼酸盐试剂的合成与应用：在Geralcin A，Hydrazidomycins AB，（±）-CPC-1，（±）-Alline，Splenocin-B和有效的癌细胞生长抑制剂Kitastatin的总合成中的应用和呼吸素
6. An Efficient Total Synthesis of a Potent Anti-Inflammatory Agent Benzocamphorin F and Its Anti-Inflammatory Activity [O] . Yu-Ren Liao, Ping-Chung Kuo, Jun-Weil Liang, 2012

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7. Total synthesis of Sparstolonin B, a potent anti-inflammatory agent [O] . Wang Yongqiang, Wang Chao, Wang Yuanxun, 2015

机译：全合成Sparstolonin B，一种有效的抗炎药

Total synthesis of Sparstolonin B, a potent anti-inflammatory agent

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