An odorless thia-Michael addition using Bunte salts as thiol surrogates

Lin Ya-mei; Lu Guo-ping; Cai Chun; Yi Wen-bin

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An odorless thia-Michael addition using Bunte salts as thiol surrogates

机译：使用Bunte Salts作为硫醇替代品的无臭的紫猴添加

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A newly developed C-S bond formation process via acid-catalyzed thia-Michael addition has been demonstrated. The protocol, in which Bunte salts generated from odorless, inexpensive sodium thiosulfate and organic halides are used as the thiol precursors, provides an efficient approach for the synthesis of beta-sulfido carbonyl compounds.

机译：已经证明了通过酸催化的硫脲添加的新开发的C-S键形成方法。该方案，其中来自无味，廉价的硫代硫酸钠和有机卤化物产生的Bunte盐用作硫醇前体，提供了合成β-磺酰羰基化合物的有效方法。

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来源
《RSC Advances》 |2015年第34期|共5页
作者
Lin Ya-mei; Lu Guo-ping; Cai Chun; Yi Wen-bin;
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作者单位

Nanjing Univ Sci &

Technol Chem Engn Coll Nanjing 210094 Jiangsu Peoples R China;

Nanjing Univ Sci &

Technol Chem Engn Coll Nanjing 210094 Jiangsu Peoples R China;

Nanjing Univ Sci &

Technol Chem Engn Coll Nanjing 210094 Jiangsu Peoples R China;

Nanjing Univ Sci &

Technol Chem Engn Coll Nanjing 210094 Jiangsu Peoples R China;

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正文语种 eng
中图分类化学;
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1. An odorless thia-Michael addition using Bunte salts as thiol surrogates [J] . Lin Ya-mei, Lu Guo-ping, Cai Chun, RSC Advances . 2015,第34期

机译：使用Bunte Salts作为硫醇替代品的无臭的紫猴添加
2. Solvent-free Thia-Michael Addition Reactions Using 3-[Bis(alkylthio)methylene]pentane-2,4-diones as Efficient and Odorless Thiol Equivalents [J] . Chun LIN, Xiao-Liang ZHAO, Yan OUYANG, Chinese Journal of Chemistry . 2008,第8期

机译：使用3- [双（烷硫基亚甲基）戊]戊烷-2,4-二酮作为高效无臭硫醇当量的无溶剂Thia-Michael加成反应
3. Solvent-free Thia-Michael Addition Reactions Using 3-Bis(alkylthio)methylenepentane-2,4-diones as Efficient and Odorless Thiol Equivalents [J] . LIN Chun, ZHAO Xiao-Liang, OUYANG Yan, 中国化学（英文版） . 2008,第008期

机译：使用3- 双（烷硫基亚甲基）戊戊烷-2,4-二酮作为高效无臭硫醇当量的无溶剂Thia-Michael加成反应
4. Hexamethylene bis-bunte salt in place of cobalt salts for steel cord adhesion [C] . C. Jeffrey Lin, F. Ignatz-Hoover, L. Forciniti, International Elastomer Conference . 2020

机译：六亚甲基双 - Bunte盐代替钢丝绳粘连的钴盐
5. Controlling the synthesis of bunte salt stabilized gold nanoparticles using a microreactor platform in concert with small angle x-ray scattering analysis. [D] . Haben, Patrick Michael. 2013

机译：使用微反应器平台与小角X射线散射分析相结合，控制丁苯橡胶盐稳定的金纳米颗粒的合成。
6. Alkyl selenosulphates (seleno Bunte salts). A new class of thiol-blocking reagents. [O] . A R Scarf, E R Cole, P T Southwell-Keely 1982

机译：烷基硒代硫酸盐（硒代布丁盐）。一类新的硫醇封闭剂。
7. Odorless regioselective ring opening of epoxides with S-alkylisothiouronium salts as masked thiols in water [O] . Rajib Panchadhayee, Anup Kumar Misra 2009

机译：环氧化物的无气味区域选择性开环，用s-烷基异硫脲盐作为水中的掩蔽硫醇
8. Potential Radiation-Protective Compounds. Synthesis of the Three Isomeric Three-Carbon Aminohydroxy Bunte Salts and Related Compounds [R] . Ball, D. H., Williams, J. M., Long, L. 1962

机译：潜在的辐射防护化合物。三种异构三碳氨基羟基Bunte盐及相关化合物的合成

An odorless thia-Michael addition using Bunte salts as thiol surrogates

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