X-ray resonant single-crystal diffraction technique, a powerful tool to investigate the kesterite structure of the photovoltaic Cu_2ZnSnS_4 compound

Alain Lafond; Léo Choubrac; Catherine Guillot-Deudon; Pierre Fertey; Michel Evain; Stéphane Jobic

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X-ray resonant single-crystal diffraction technique, a powerful tool to investigate the kesterite structure of the photovoltaic Cu_2ZnSnS_4 compound

机译：X射线共振单晶衍射技术，研究光伏Cu_2ZnSnS_4化合物的硅藻土结构的有力工具

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Cu/Zn disorder in the kesterite Cu_2ZnSnS_4 derivatives used for thin film based solar cells is an important issue for photovoltaic performances. Unfortunately, Cu and Zn cannot be distinguished by conventional laboratory X-ray diffraction. This paper reports on a resonant diffraction investigation of a Cu_2ZnSnS_4 single crystal from a quenched powdered sample. The full disorder of Cu and Zn in the z = 1/4 atomic plane is shown. The structure, namely disordered kesterite, is then described in the I-442m space group.

机译：用于薄膜基太阳能电池的硅藻土中的Cu / ZnSnS_4衍生物中的Cu / Zn无序是光伏性能的重要问题。不幸的是，铜和锌不能通过常规的实验室X射线衍射来区分。本文报道了淬火粉末样品中Cu_2ZnSnS_4单晶的共振衍射研究。显示了z = 1/4原子平面中Cu和Zn的完全无序。然后，在I-442m空间群中描述了该结构，即无序的锂霞石。

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《Acta Crystallographica, Section B. Structural Science》 |2014年第2期|共5页
作者
Alain Lafond; Léo Choubrac; Catherine Guillot-Deudon; Pierre Fertey; Michel Evain; Stéphane Jobic;
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正文语种 eng
中图分类晶体学;
关键词
X-ray; resonant; single-crystal;

机译：X射线;共振;单晶;

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1. X-ray resonant single-crystal diffraction technique, a powerful tool to investigate the kesterite structure of the photovoltaic Cu_2ZnSnS_4 compound [J] . Alain Lafond, Léo Choubrac, Catherine Guillot-Deudon, Acta Crystallographica, Section B. Structural Science . 2014,第2期

机译：X射线共振单晶衍射技术，研究光伏Cu_2ZnSnS_4化合物的硅藻土结构的有力工具
2. Investigation of the commensurate magnetic structure in the heavy-fermion compound CePt_2In_7 using magnetic resonant x-ray diffraction [J] . Nicolas Gauthier, Didier Wermeille, Nicola Casati, Physical review. B, Condensed Matter And Materals Physics . 2017,第6期

机译：磁共振X射线衍射研究重铁化合物CePt_2In_7中的相应磁结构
3. Investigation of the commensurate magnetic structure in the heavy-fermion compound CePt2In7 using magnetic resonant x-ray diffraction [J] . Gauthier Nicolas, Wermeille Didier, Casati Nicola, Physical review, B . 2017,第6期

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4. Formation of Cu_2ZnSnS_4 and Cu_2ZnSnS_4-CuInS_2 Thin Films Investigated by In-Situ Energy Dispersive X-Ray Diffraction [C] . Alfons Weber, Immo Koetschau, Susan Schorr, MRS spring meeting . 2007

机译：原位能量色散X射线衍射研究Cu_2ZnSnS_4和Cu_2ZnSnS_4-CuInS_2薄膜的形成
5. Optimization techniques for phase retrieval based on single-crystal X-ray diffraction data. [D] . Smith, Alexander Barton. 2008

机译：基于单晶X射线衍射数据的相位检索优化技术。
6. X-ray diffraction: a powerful tool to probe and understand the structure of nanocrystalline calcium silicate hydrates [O] . Sylvain Grangeon, Francis Claret, Yannick Linard, -1

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7. Single-crystal polarized electronic spectra of the compounds dichlorotetrakis ([mu]-pivalato)dirhenium(III),tetra-n-butylammonium octachlorodirhenate(III), tetra-n-butylammonium octabromodirhenate(III), dimolybdenum(II)tetrapivalate, and the X-ray diffraction cyrstal structures of tetra-n-butylammonium octobromodirhenate(III) and two polymorphs of dimolybdenum(II) tetrapivalate [O] . Huang, Hai-Wei 1985

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8. Resonant (1s to 3d) X-Ray Bragg Diffraction by Transition-Metal Compounds [R] . Lovesey, S. W., Knight, K. S., Balcar, E. 2000

机译：过渡金属化合物的共振（1s至3d）X射线布拉格衍射

X-ray resonant single-crystal diffraction technique, a powerful tool to investigate the kesterite structure of the photovoltaic Cu_2ZnSnS_4 compound

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