Mass Transfer During Droplet Formation – A Measuring Technique Study

Heine Jens S.; Bart Hans‐J?rg

摘要

Abstract >In liquid‐liquid extraction processes, the mass transfer coefficient is one of the key design parameters. In the present study, the impact on mass transfer during droplet formation in a quiescent continuous phase is investigated analytically. Therefore, confocal Raman spectroscopy in a novel measurement cell combined with interfacial tension measurements are applied. It could be shown, that Marangoni effects in the system toluene‐acetonitrile‐water (mass transfer direction from the dispersed to the continuous phase) lead to 50% of mass transferred in the first 5s when 90% is transferred in 1 min. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>液体中的抽象</ title> > - 水屑提取过程，传质系数是关键设计参数之一。在本研究中，分析研究了在静态连续相中液滴形成期间对传质的影响。因此，应用了新型测量电池中的共聚变拉曼光谱与界面张力测量相结合。可以表明，在系统甲苯 - 乙腈 - 水中的Marangoni作用（来自分散到连续相的质量转移方向），当90％在1分钟内转移时，在前5S中转移的50％的质量。</ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16114/'>《Chemie-Ingenieur-Technik: Verfahrenstechnik Technische Chemie Apparatewesen Biotechnologie》</a> <b style="margin: 0 2px;">|</b><span>2017年第12期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Heine Jens S.&option=202" target="_blank" rel="nofollow">Heine Jens S.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bart Hans‐J?rg&option=202" target="_blank" rel="nofollow">Bart Hans‐J?rg;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Chair of Separation Science and TechnologyUniversity of KaiserslauternPO Box 3049 67653 Kaiserslautern Germany;</p> <p>Chair of Separation Science and TechnologyUniversity of KaiserslauternPO Box 3049 67653 Kaiserslautern Germany;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/238.html" title="化学工业">化学工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Interfacial phenomena&option=203" rel="nofollow">Interfacial phenomena;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liquid‐liquid extraction&option=203" rel="nofollow">Liquid‐liquid extraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Marangoni convection&option=203" rel="nofollow">Marangoni convection;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mass transfer&option=203" rel="nofollow">Mass transfer;</a> </p> <div class="translation"> 机译：界面现象;液液提取;Marangoni对流;传质; 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href="/patent-detail/061202153058.html">形成液滴的方法和所形成的液滴的分散体</a> <b>[P]</b> . <span> 中国专利： CN103635252B </span> <span> . 2016.08.10</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061202281299.html">液滴形成装置及液滴形成方法</a> <b>[P]</b> . <span> 中国专利： CN104169008B </span> <span> . 2016.12.14</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130442506596.html">Transgenic animal, embryo, transgenic mouse, animal model for the study of bone density modulation, isolated cell, nucleic acid to mark the gene by homologous recombination, and methods to study bone mass determinants, to study bone mass modulators, to study bone mass, to study an hbm effect on bone disorders, to identify surrogate markers of bone formation / resorption, to study hbm effects on cardiac disorders, to assess cardio-protective treatments for bone mass modulation effects, to modulate bone density, to produce a transgenic mouse and to identify genes associated with bone mass</a> <b>[P]</b> . <span> 外国专利：  BR0209564A </span> <span> . 2004-10-26</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：转基因动物，胚胎，转基因小鼠，用于骨密度调节研究的动物模型，分离的细胞，通过同源重组标记该基因的核酸以及研究骨量决定因素，研究骨量调节剂，研究骨量的方法，研究hbm对骨骼疾病的影响，鉴定骨形成/再吸收的替代标志物，研究hbm对心脏疾病的影响，评估对骨骼质量调节作用的心脏保护性治疗，调节骨密度，生产转基因小鼠和识别与骨量相关的基因 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130431259097.html">APPARATUS FOR MEASURING MASS DEVIATION OF DROPLETS, METHOD FOR MEASURING MASS DEVIATION OF DROPLETS USING THE SAME, PATTERN FORMING SYSTEM USING THE SAME, AND METHOD OF CONTROLLING PATTERN FORMING SYSTEM USING THE SAME</a> <b>[P]</b> . <span> 外国专利：  JP2009148754A </span> <span> . 2009-07-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于测量液滴的质量偏差的装置，使用相同的方法测量液滴的质量偏差的方法，使用相同的方法形成图形的系统以及使用相同的方法来控制图形形成系统的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130421781964.html">Method for quality control of study objects i.e. snacks, involves determining quality characteristics using NMR technique, directly measuring moved sample in production line, and determining inner and outer geometries of study objects</a> <b>[P]</b> . <span> 外国专利：  DE102010021260A1 </span> <span> . 2011-11-24</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：研究对象（即零食）质量控制的方法包括使用NMR技术确定质量特征，直接测量生产线中移动的样本以及确定研究对象的内部和外部几何形状 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div 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