Practical and Scalable Syntheses of Substituted Ketene Dithioacetal Monoxides

Murakami Kei; Yorimitsu Hideki; Osuka Atsuhiro

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Practical and Scalable Syntheses of Substituted Ketene Dithioacetal Monoxides

机译：实用且可缩放的取代酮二乙醛一氧化铁

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摘要

Practical syntheses of substituted ketene dithioacetal monoxides (KDMs) from the corresponding aldehydes or ethyl trifluoroacetate are described. Newly developed procedures are scalable and versatile to provide aryl-, alkyl-, and trifluoromethyl-substituted KDMs in gram scales.

机译：描述了来自相应醛或三氟乙酸乙酯的取代的氯烯二乙酰乙醛一氧化胺（KDMS）的实际合成。新开发的程序是可伸缩和通用的，可在克鳞片中提供芳基，烷基 - 和三氟甲基取代的KDMS。

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《Bulletin of the Chemical Society of Japan》 |2013年第10期|共3页
作者
Murakami Kei; Yorimitsu Hideki; Osuka Atsuhiro;
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Kyoto Univ Dept Chem Grad Sch Sci Sakyo Ku Kyoto 6068502 Japan;

Kyoto Univ Dept Chem Grad Sch Sci Sakyo Ku Kyoto 6068502 Japan;

Kyoto Univ Dept Chem Grad Sch Sci Sakyo Ku Kyoto 6068502 Japan;

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正文语种 eng
中图分类化学;
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1. Practical and Scalable Syntheses of Substituted Ketene Dithioacetal Monoxides (vol 86, pg 1193, 2013) [J] . Murakami Kei, Yorimitsu Hideki, Osuka Atsuhiro Bulletin of the Chemical Society of Japan . 2014,第3期

机译：实用且可缩放合成取代的酮二乙酰缩醛丙酮一氧化胺（Vol 86，PG 1193,2013）
2. The Alkoxy Substitution Reaction on alpha-Oxo Ketene Dithioacetals:A New Access to alpha-Oxo ketene O,S-O,O-Acetals [J] . Mang Wang, Xian-Xiu Xu, Shao-Guang Sun, Synthetic Communications . 2004,第2期

机译：α-氧代乙烯酮二硫缩醛上的烷氧基取代反应：α-氧代乙烯酮O，S-O，O-缩醛的新途径
3. A Route to Indoles via Modified Fischer Indole Intermediates from Sulfonanilides and Ketene Dithioacetal Monoxides [J] . Kinoshita Jun, Baralle Alexandre, Yoshida Akira, Asian Journal of Organic Chemistry . 2020,第10期

机译：通过改性的费斯吲哚中间体来自磺酰氯和酮二甲基丙酮一氧化铁的途径
4. Novel Synthesis of Ketene Dithioacetals via Ruthenium-catalyzed 1,1-Addition of Organic Disulfides to Terminal Alkynes [C] . Takashi Fukuda, Kenji Wada, Take-aki Mitsudo Symposium on Organometallic Chemistry . 2007

机译：通过钌催化的1,1-加入有机二硫化物的酮二缩醛的新颖合成至末端炔烃
5. I. Syntheses of E- and Z-volkendousin. II. Oxidative cyclization of unsaturated ketene dithioacetals with ceric ammonium nitrate to form bicyclic lactones. III. Synthesis of pyrinodemins A and B; assignment of the double bond position of pyrinodemin A. IV. Formal synthesis of guanacastepene A [D] . Shi, Bo 2003

机译：I.E-和Z-Volkendousin的合成。二。不饱和烯酮二硫缩醛与硝酸铈铵的氧化环化反应，形成双环内酯。三，嘧啶A和B的合成；嘧啶A的双键位置的分配。胍基丁烯A的形式合成
6. α-Selective Ni-Catalyzed Hydroalumination of Aryl- and Alkyl-Substituted Terminal Alkynes. Practical Syntheses of Internal Vinyl Aluminums Halides or Boronates [O] . Fang Gao, Amir H. Hoveyda -1

机译：α-选择性镍催化芳基 - 的铝氢化和烷基取代的末端炔烃。内部乙烯基铝卤化物或硼酸酯的合成实用
7. Synthesis and Characterization of Fully Substituted Pyrimidines by Using Ketene Dithioacetal as Potent Antimicrobial Agent [O] . Hasmukh R. Khunt, Piyush P. Pipaliya, Satish M. Ghelani, 2013

机译：用酮二缩醛作为有效抗微生物剂的完全取代嘧啶的合成与表征

Practical and Scalable Syntheses of Substituted Ketene Dithioacetal Monoxides

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