Microwave Specific Specific Effect on Catalytic atropo-Enantioselective Ring-Opening Reaction of Biaryl Lactones

Tashima Shigeki; Nushiro Kazuya; Saito Kodai; Yamada Tohru

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Microwave Specific Specific Effect on Catalytic atropo-Enantioselective Ring-Opening Reaction of Biaryl Lactones

机译：微波特异性对催化ATROPO-对致致致倾斜反应的催化ATROPO-对反应的致态乳酰胺

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The microwave specific effect on the catalytic atropo-enantioselective ring-opening reaction of biaryl lactones was investigated. Under strictly controlled temperature conditions, the reaction was accelerated by microwave irradiation without any loss of the enantioselectivity. Also, the racemization rate of the atropo-optically active biaryl lactone was enhanced by the microwave irradiation.

机译：研究了对催化Atropo-enairoIsExective的辅助偶联剂的催化Atropo-enaIsExective反应的微波特异性效果。在严格控制的温度条件下，通过微波辐射加速反应，而不会丧失对映选择性的任何损失。此外，通过微波辐射增强了阿联器光学活性炭芳土内酯的外消旋速率。

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《Bulletin of the Chemical Society of Japan》 |2016年第7期|共3页
作者
Tashima Shigeki; Nushiro Kazuya; Saito Kodai; Yamada Tohru;
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作者单位

Keio Univ Dept Chem Kohoku Ku Yokohama Kanagawa 2238522 Japan;

Keio Univ Dept Chem Kohoku Ku Yokohama Kanagawa 2238522 Japan;

Keio Univ Dept Chem Kohoku Ku Yokohama Kanagawa 2238522 Japan;

Keio Univ Dept Chem Kohoku Ku Yokohama Kanagawa 2238522 Japan;

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正文语种 eng
中图分类化学;
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专利

1. Microwave Specific Specific Effect on Catalytic atropo-Enantioselective Ring-Opening Reaction of Biaryl Lactones [J] . Tashima Shigeki, Nushiro Kazuya, Saito Kodai, Bulletin of the Chemical Society of Japan . 2016,第7期

机译：微波特异性对催化ATROPO-对致致致倾斜反应的催化ATROPO-对反应的致态乳酰胺
2. Catalytic atropo-enantioselective reduction of biaryl lactones to axially chiral biaryl compounds [J] . Ashizawa T, Tanaka S, Yamada T Organic letters . 2008,第12期

机译：联芳基内酯催化熵变对映体还原为轴向手性联芳基化合物
3. Catalytic atropo-Enantioselective Ring Opening of Biaryl Lactones [J] . T. ASHIZAWA, T. YAMADA Synfacts: highlights in current synthetic organic chemistry . 2009,第5期

机译：联芳基内酯的催化对映体对映选择性开环
4. Microwave Specific Effect on Catalytic Enantioselective Reactions [C] . Tohru Yamada Asia-Pacific Microwave Conference . 2018

机译：微波对催化对映选择性反应的影响
5. The discovery and synthetic applications of catalytic asymmetric ring-opening reactions. [D] . Wu, Michael Han-cheng. 1999

机译：催化不对称开环反应的发现和合成应用。
6. Natural structural variation in enzymes as a tool in the study of mechanism exemplified by a comparison of the catalytic-site structure and characteristics of cathepsin B and papain. pH-dependent kinetics of the reactions of cathepsin B from bovine spleen and from rat liver with a thiol-specific two-protonic-state probe (22-dipyridyl disulphide) and with a specific synthetic substrate (N-alpha-benzyloxycarbonyl-L-arginyl-L-arginine 2-naphthylamide). [O] . F Willenbrock, K Brocklehurst 1984

机译：通过比较组织蛋白酶B和木瓜蛋白酶的催化位点结构和特性可以证明酶的天然结构变异是研究机理的工具。牛脾脏和大鼠肝脏组织蛋白酶B与巯基特异性二质子状态探针（22-联吡啶二硫化物）和特定合成底物（N-α-苄氧基羰基- L-精氨酸-L-精氨酸2-萘酰胺）。
7. Microwave Specific Effect on Catalyticatropo-Enantioselective Ring-Opening Reaction of Biaryl Lactones [O] . Shigeki Tashima, Kazuya Nushiro, Kodai Saito, 2016

机译：微波特异性对丙酮催化催化催化催化催化的致致倾斜反应的影响
8. D(sub 2) + Ni(sub 13) reaction: Mode-specific and structure-specific features. [R] . J. Jellinek Z. B. Guevenc 1991

机译：D（sub 2）+ Ni（sub 13）反应：模式特异性和结构特异性特征。

Microwave Specific Specific Effect on Catalytic atropo-Enantioselective Ring-Opening Reaction of Biaryl Lactones

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