Synthesis of 4-polyfluoroalkyl-1,3-dithiolanes via [3+2] cycloaddition of thiocarbonyl ylide to polyfluoroalkanethioamides

Mykhaylychenko Sergiy S.; Markitanov Yuriy N.; Rudenko Timofii V.; Rusanov Eduard B.; Shermolovich Yuriy G.

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Synthesis of 4-polyfluoroalkyl-1,3-dithiolanes via [3+2] cycloaddition of thiocarbonyl ylide to polyfluoroalkanethioamides

机译：通过[3 + 2]硫代羰基ylide的4-聚氟烷基-1,3-二硫醇的合成硫代羰基亚烷基甲基甲酰胺

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摘要

New 4-polyfluoroalkyl-1,3-dithiolanes were synthesized by reaction of polyfluoroalkanethioamides with thiocarbonyl ylide that was generated in situ by desilylation of chloromethyl (trimethylsilyl)methyl sulfide with tetramethylammonium fluoride.

机译：通过用氯甲基酰胺与氯甲基（三甲基甲硅烷基）甲基硫醚与四甲基铵氟化物的甲基硫化物反应，通过聚氟烷基乙酰甲基酰胺反应来合成新的4-聚氟烷基-1,3-二硫醇。

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来源
《Chemistry of heterocyclic compounds》 |2019年第2期|共4页
作者
Mykhaylychenko Sergiy S.; Markitanov Yuriy N.; Rudenko Timofii V.; Rusanov Eduard B.; Shermolovich Yuriy G.;
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作者单位

Natl Acad Sci Ukraine Inst Organ Chem 5 Murmanska St UA-02660 Kiev Ukraine;

Natl Acad Sci Ukraine Inst Organ Chem 5 Murmanska St UA-02660 Kiev Ukraine;

Enamine Ltd 78 Krasnotkatska St UA-02094 Kiev Ukraine;

Natl Acad Sci Ukraine Inst Organ Chem 5 Murmanska St UA-02660 Kiev Ukraine;

Natl Acad Sci Ukraine Inst Organ Chem 5 Murmanska St UA-02660 Kiev Ukraine;

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原文格式 PDF
正文语种 eng
中图分类杂环化合物;
关键词
1; 3-dithiolane; polyfluoroalkanethiocarboxylic acids; thioamide; thiocarbonyl ylide; 3+2 cycloaddition;

机译：1;3-二硫胺;聚氟烷烷噻吩羧酸;硫代酰胺;硫代羰基ylide;[3 + 2]环加成;

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专利

1. Synthesis of 4-polyfluoroalkyl-1,3-dithiolanes via [3+2] cycloaddition of thiocarbonyl ylide to polyfluoroalkanethioamides [J] . Mykhaylychenko Sergiy S., Markitanov Yuriy N., Rudenko Timofii V., Chemistry of heterocyclic compounds . 2019,第2期

机译：通过[3 + 2]硫代羰基ylide的4-聚氟烷基-1,3-二硫醇的合成硫代羰基亚烷基甲基甲酰胺
2. Ferrocenyl substituted 1,3-dithiolanes via [3+2]-cycloadditions of thiocarbonyl S-methanides with ferrocenyl/hetaryl thioketones [J] . Hamera Roza, Mloston Grzegorz Phosphorus, Sulfur, and Silicon and the Related Elements . 2016,第4a6期

机译：二茂铁基通过硫代羰基S-甲烷的[3 + 2]-环与二茂铁基/杂芳基硫代酮的加成反应取代1,3-二硫杂环戊烷
3. 1,3-Dithiolanes from Cycloadditions of Alicyclic and Aliphatic Thiocarbonyl Ylides with Thiones: Regioselectivity [J] . Rolf Huisgen, Grzegorz Mloston, Kurt Polborn, Chemistry: A European journal . 2003,第10期

机译：脂环族和脂族硫代羰基内酯与亚硫醚的环加成反应中的1,3-二硫杂环戊烷：区域选择性
4. A facial regioselective synthesis of novel pyrrolizidines through azomethine ylide cycloaddition reaction [C] . Yaghoub Sarrafi, Kamal Alimohammadi European Symposium on Organic Chemistry . 2009

机译：通过氮杂甲酸钠环加入反应进行新型吡咯烷的面部区域选择性合成
5. I. Completion of the synthesis of Kopsia lapidilecta alkaloid (+/-)-lapidilectine B. II. Synthesis of 1-azabicyclo[n.3.0]alkanes via [3+2] cycloadditions of nonstabilized azomethine ylides [D] . Stoy, Patrick 2004

机译：I.完成了Kopsia lapidilecta生物碱（+/-）-lapidilectine的合成B. II。通过不稳定的偶氮甲亚胺的[3 + 2]环加成反应合成1-氮杂双环[n.3.0]烷烃
6. Expeditious synthesis of cis-1-methyl-2 33a459b-hexahydro-1H-pyrrolo-32hisoquinoline / 23-fquinoline via azomethine ylide-alkene 3+2 cycloaddition [O] . Zhenfa Zhang, Linda P. Dwoskin, Peter A. Crooks -1

机译：迅速合成顺式-1-甲基-233a45252b-六羟基-1H-吡咯 - 32H异喹啉/ 23-F喹啉通过氮杂甲酰基烯烃3+ 2环加成
7. Synthesis of ferrocenyl-substituted 1,3-dithiolanes via [3 + 2]-cycloadditions of ferrocenyl hetaryl thioketones with thiocarbonyl S-methanides [O] . Mloston, Grzegorz, Hamera-Faldyga, Roza, Linden, Anthony, 2016

机译：二茂铁基杂芳基硫酮与硫代羰基S-甲酰胺的[3 + 2]-环加成反应合成二茂铁基取代的1,3-二硫杂环戊烷

Synthesis of 4-polyfluoroalkyl-1,3-dithiolanes via [3+2] cycloaddition of thiocarbonyl ylide to polyfluoroalkanethioamides

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