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The Atomic Scale Electrochemical Lithiation and Delithiation Process of Silicon

机译：硅的原子尺度电化学锂化和脱轨过程

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Abstract > While silicon (Si) has tenfold capacity of commercially used graphite, its application is still limited due to its limited cyclability. In this in situ X‐ray reflectivity study, a detailed mechanistic model of the first two (de)lithiation processes of a silicon wafer is presented, which sheds light onto the fundamental difference of the reaction of Li ions with crystalline and amorphous materials. Furthermore, this study provides insight into the formation and further evolution of the inorganic solid electrolyte interphase (SEI) layer on Si anodes. The results show that the lithiation of crystalline Si is a layer‐by‐layer, reaction limited two‐phase process, but the delithiation of Li <sub>x</sub> Si (resulting in amorphous Si) and the lithiation of amorphous Si are reaction‐limited single‐phase processes. Furthermore, the thickness‐density product of the inorganic SEI layer increases during lithiation and decreases during delithiation, resembling a “breathing” behavior; the inorganic SEI layer thickness varies between 40 and 70 ?. Additionally, a low‐electron‐density “Li‐dip” layer is found between the SEI and lithiated Si during the delithiation process, suggesting kinetically limited ion transport within the SEI, which is speculated to be one of the origins of battery's internal resistance. Several implications of the findings on battery performance in general are discussed. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 虽然硅（Si）具有商业二手石墨的十倍容量，但由于其可行性有限，其应用仍然有限。在这种原位X射线反射率研究中，提出了硅晶片的前两个（DE）锂化方法的详细机械模型，其缩小了Li离子与结晶和无定形材料的反应的基本差异。此外，该研究提供了洞察Si阳极上无机固体电解质间（SEI）层的形成和进一步演变。结果表明，结晶Si的锂化是逐层，反应有限的两相过程，但Li的脱发 <sub> x </ sub> </ i> Si（导致无定形Si）和无定形Si的锂化是反应有限的单相过程。此外，无机SEI层的厚度密度乘积在锂化期间增加，并且在脱轨期间减少，类似于“呼吸”行为;无机SII层厚度在40到70之间变化？。另外，在脱轨过程中，在SEI和Li-Dip“层之间发现了低电子密度”Li-Dip“层，表明SEI内的动力学有限，这被推测为电池内阻的起源之一。讨论了对电池性能的几种影响是一般的。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2017年第22期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cao Chuntian&option=202" target="_blank" rel="nofollow">Cao Chuntian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Steinrück Hans‐Georg&option=202" target="_blank" rel="nofollow">Steinrück Hans‐Georg;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shyam Badri&option=202" target="_blank" rel="nofollow">Shyam Badri;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Toney Michael F.&option=202" target="_blank" rel="nofollow">Toney Michael F.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>SSRL Materials Science DivisionSLAC National Accelerator LaboratoryMenlo Park CA 94025 USA;</p> <p>SSRL Materials Science DivisionSLAC National Accelerator LaboratoryMenlo Park CA 94025 USA;</p> <p>SSRL Materials Science DivisionSLAC National Accelerator LaboratoryMenlo Park CA 94025 USA;</p> <p>SSRL Materials Science DivisionSLAC National Accelerator LaboratoryMenlo Park CA 94025 USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=in situ&option=203" rel="nofollow">in situ;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li‐ion battery&option=203" rel="nofollow">Li‐ion battery;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=silicon anode&option=203" rel="nofollow">silicon anode;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solid electrolyte interphase&option=203" rel="nofollow">solid electrolyte interphase;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=X‐ray reflectivity&option=203" rel="nofollow">X‐ray reflectivity;</a> </p> <div class="translation"> 机译：原位;锂离子电池;硅阳极;固体电解质相互作用;X射线反射率; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022434745.html">The Atomic Scale Electrochemical Lithiation and Delithiation Process of Silicon</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cao Chuntian&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Cao Chuntian,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Steinrück Hans‐Georg&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Steinrück Hans‐Georg,</a> <a 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