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A Facile Surface Reconstruction Mechanism toward Better Electrochemical Performance of Li ₄4 Ti ₅5 O ₁₂12 in Lithium‐Ion Battery

机译：锂电子更好的电化学性能的易于表面重建机制 _{4 4 TI. _{5 5 O. _{12 12 在锂离子电池中}}}

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Abstract > Through a facile sodium sulfide (Na <sub>2</sub> S)‐assisted hydrothermal treatment, clean and nondefective surfaces are constructed on micrometer‐sized Li <sub>4</sub> Ti <sub>5</sub> O <sub>12</sub> particles. The remarkable improvement of surface quality shows a higher first cycle Coulombic efficiency (≈95%), a significantly enhanced cycling performance, and a better rate capability in electrochemical measurements. A combined study of Raman spectroscopy and inductive coupled plasma emission spectroscopy reveals that the evolution of Li <sub>4</sub> Ti <sub>5</sub> O <sub>12</sub> surface in a water‐based hydrothermal environment is a hydrolysis–recrystallization process, which can introduce a new phase of anatase‐TiO <sub>2</sub> . While, with a small amount of Na <sub>2</sub> S (0.004 mol L ?1 at least), the spinel‐Li <sub>4</sub> Ti <sub>5</sub> O <sub>12</sub> phase is maintained without a second phase. During this process, the alkaline environment created by Na <sub>2</sub> S and the surface adsorption of the sulfur‐containing group (HS ? or S 2? ) can suppress the recrystallization of anatase‐TiO <sub>2</sub> and renew the particle surfaces. This finding gives a better understanding of the surface–property relationship on Li <sub>4</sub> Ti <sub>5</sub> O <sub>12</sub> and guidance on preparation and modification of electrode material other than coating or doping. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>抽象</ title> > 通过容易硫化钠（Na <sub> 2 </ sub> S） - 拟合水热处理，清洁和非缺陷表面构建在千分尺寸锂上 <sub> 4 </ sub> TI. <sub> 5 </ sub> O. <sub> 12 </ sub> 粒子。表面质量显着提高显示了较高的第一周期库仑效率（≈95％），显着增强的循环性能，以及电化学测量中的更好的速率能力。拉曼光谱和电感耦合等离子体发射光谱的组合研究揭示了李的演变 <sub> 4 </ sub> TI. <sub> 5 </ sub> O. <sub> 12 </ sub> 水基水热环境中的表面是水解 - 再结晶过程，可以引入anatase-TiO的新阶段 <sub> 2 </ sub> 。而且，少量NA <sub> 2 </ sub> s（0.004 mol l ？1 </ sup> 至少），尖晶石李 <sub> 4 </ sub> TI. <sub> 5 </ sub> O. <sub> 12 </ sub> 阶段没有第二阶段保持。在此过程中，Na创建的碱性环境 <sub> 2 </ sub> S和含硫基团的表面吸附（HS ？</ sup> 或者 2？</ sup> ）可以抑制Anatase-TiO的再结晶 <sub> 2 </ sub> 并更新颗粒表面。这一发现可以更好地了解李的地表关系 <sub> 4 </ sub> TI. <sub> 5 </ sub> O. <sub> 12 </ sub> 并提供除涂层或掺杂之外的电极材料的制备和改性的指导。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2017年第11期</span><b style="margin: 0 2px;">|</b><span>共1页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qian Kun&option=202" target="_blank" rel="nofollow">Qian Kun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tang Linkai&option=202" target="_blank" rel="nofollow">Tang Linkai;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wagemaker Marnix&option=202" target="_blank" rel="nofollow">Wagemaker Marnix;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=He Yan‐Bing&option=202" target="_blank" rel="nofollow">He Yan‐Bing;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Dongqing&option=202" target="_blank" rel="nofollow">Liu Dongqing;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Hai&option=202" target="_blank" rel="nofollow">Li Hai;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shi Ruiying&option=202" target="_blank" rel="nofollow">Shi Ruiying;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Baohua&option=202" target="_blank" rel="nofollow">Li Baohua;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kang Feiyu&option=202" target="_blank" rel="nofollow">Kang Feiyu;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Nano Energy Materials Laboratory (NEM)Tsinghua UniversityShenzhen 518055 P. R. China;</p> <p>Laboratory of Advanced MaterialsTsinghua UniversityBeijing 100086 P. R. China;</p> <p>Department of Radiation Science and TechnologyDelft University of TechnologyMekelweg 15 Delft 2629JB The Netherlands;</p> <p>Engineering Laboratory for the Next Generation Power and Energy Storage BatteriesTsinghua UniversityShenzhen 518055 P. R. China;</p> <p>Engineering Laboratory for the Next Generation Power and Energy Storage BatteriesTsinghua UniversityShenzhen 518055 P. R. China;</p> <p>Laboratory of Advanced MaterialsTsinghua UniversityBeijing 100086 P. R. China;</p> <p>Laboratory of Advanced MaterialsTsinghua UniversityBeijing 100086 P. R. China;</p> <p>Engineering Laboratory for the Next Generation Power and Energy Storage BatteriesTsinghua UniversityShenzhen 518055 P. R. China;</p> <p>Nano Energy Materials Laboratory (NEM)Tsinghua UniversityShenzhen 518055 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hydrothermal method&option=203" rel="nofollow">hydrothermal method;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li 4 Ti 5 O 12&option=203" rel="nofollow">Li 4 Ti 5 O 12;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=lithium‐ion batteries&option=203" rel="nofollow">lithium‐ion batteries;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Na 2 S&option=203" rel="nofollow">Na 2 S;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=surface modifications&option=203" rel="nofollow">surface modifications;</a> </p> <div class="translation"> 机译：水热法;Li 4 Ti 5 O 12;锂离子电池;NA 2 S;表面修改; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022434837.html">A Facile Surface Reconstruction Mechanism toward Better Electrochemical Performance of Li <sub xmlns="http://www.wiley.com/namespaces/wiley">4</sub>4 Ti <sub xmlns="http://www.wiley.com/namespaces/wiley">5</sub>5 O <sub xmlns="http://www.wiley.com/namespaces/wiley">12</sub>12 in Lithium‐Ion Battery</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qian Kun&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Qian Kun,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tang Linkai&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Tang Linkai,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wagemaker Marnix&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Wagemaker Marnix,</a> <a href="/journal-foreign-18063/" target="_blank" rel="nofollow" class="tuijian_authcolor">Advanced materials interfaces .</a> <span>2017</span><span>,第11期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: 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target="_blank" rel="nofollow" class="tuijian_authcolor">Advanced materials interfaces .</a> <span>2017</span><span>,第12期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：多级李 <sub xmlns =“http://www.wiley.com/namespaces/wiley”> 1.2 </ sub> 1.2 你 <sub xmlns =“http://www.wiley.com/namespaces/wiley”> 0.2 </ sub> 0.2 m <sub xmlns =“http://www.wiley.com/namespaces/wiley”> 0.6 </ sub> 0.6 O. <sub xmlns =“http://www.wiley.com/namespaces/wiley”> 2 </ sub> 2 用于锂离子电池的高性能阴极材料的微型架构</span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-conference-foreign_meeting-287971_thesis/0705015365478.html">Comparison of Structural Analysis and Electrochemical Studies of C-Li_4Ti_5O_(12) and CNT- Li_4Ti_5O_(12) Nanocomposites particles used as Anode for Lithium Ion Battery</a> <b>[C]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xiangcheng Sun&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Xiangcheng Sun,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xuedong Bai&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Xuedong Bai,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yongqing Wang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Yongqing Wang,</a> <a href="/conference-foreign-287971/" target="_blank" rel="nofollow" class="tuijian_authcolor">Materials Research Society Symposium on Materials for Vehicular and Grid Energy Storage .</a> <span>2013</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：C-Li_4Ti_5O_（12）和CNT-LI_4TI_5O_（12）纳米复合材料用作锂离子电池阳极的C-LI_4TI_5O_（12）和CNT-LI_4TI_5O_（12）纳米复合材料的比较</span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-degree-foreign_mphd_thesis/02061812965.html">Electrochemical performance of lithium-ion hybrid supercapacitors based on activated carbon and Li4Ti5O12 insertion electrodes</a> <b>[D] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Singh, Sandeep.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Singh, Sandeep. </a> <span>2014</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：基于活性炭和Li4Ti5O12插入电极的锂离子杂交超级电容器的电化学性能</span> </p> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-journal-foreign-pmc_detail_thesis/040001773414.html">Catalytic Asymmetric Synthesis 2nd Edition. By Iwao Ojima (Editor)Wiley-VCH: New York (http://www.wiley.com/). 2000. Pages: XIV 864 Pages Hardcover. Price: 169.- Euro / 330.54 DM / 294.- SFR. ISBN: 0-471-29805-0</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> </a> <span>2001</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：催化不对称合成第二版。奥利马（Iwao Ojima）（编辑）Wiley-VCH：纽约（http://www.wiley.com/）。 2000。页数：XIV864页精装。价格：169.-欧元/330.54 DM / 294.- SFR。国际标准书号（ISBN）：0-471-29805-0</span> </p> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/open-access_resources_thesis/01000125377833.html">Growth kinetics of <mml:math altimg="si18.gif" overflow="scroll" xmlns:xocs="http://www.elsevier.com/xml/xocs/dtd" xmlns:xs="http://www.w3.org/2001/XMLSchema" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns="http://www.elsevier.com/xml/ja/dtd" xmlns:ja="http://www.elsevier.com/xml/ja/dtd" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:tb="http://www.elsevier.com/xml/common/table/dtd" xmlns:sb="http://www.elsevier.com/xml/common/struct-bib/dtd" xmlns:ce="http://www.elsevier.com/xml/common/dtd" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:cals="http://www.elsevier.com/xml/common/cals/dtd" xmlns:sa="http://www.elsevier.com/xml/common/struct-aff/dtd"><mml:mrow><mml:mi>ω</mml:mi></mml:mrow></mml:math> particles in <mml:math altimg="si16.gif" overflow="scroll" xmlns:xocs="http://www.elsevier.com/xml/xocs/dtd" xmlns:xs="http://www.w3.org/2001/XMLSchema" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns="http://www.elsevier.com/xml/ja/dtd" xmlns:ja="http://www.elsevier.com/xml/ja/dtd" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:tb="http://www.elsevier.com/xml/common/table/dtd" xmlns:sb="http://www.elsevier.com/xml/common/struct-bib/dtd" xmlns:ce="http://www.elsevier.com/xml/common/dtd" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:cals="http://www.elsevier.com/xml/common/cals/dtd" xmlns:sa="http://www.elsevier.com/xml/common/struct-aff/dtd"><mml:mrow><mml:mi>β</mml:mi></mml:mrow></mml:math>-Ti matrix studied by in situ small-angle X-ray scattering</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=J. Šmilauerová&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">J. Šmilauerová,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=P. Harcuba&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">P. Harcuba,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=D. Kriegner&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">D. Kriegner,</a> <span>2015</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：<mml：math altimg =“si18.gif”overflow =“滚动”xmlns：xocs =“http://www.elsevier.com/xml/xocs/dtd”xmlns：xs =“http：// www .w3.org / 2001 / xmlschema“xmlns：xsi =”http://www.w3.org/2001/xmlschema-instance“xmlns =”http://www.elsevier.com/xml/ja/dtd“xmlns ：JA =“http://www.elsevier.com/xml/ja/dtd”XMLNS：MML =“http://www.w3.org/1998/math/mathml”xmlns：tb =“http：// www.elsevier.com/xml/common/table/dtd“xmlns：sb =”http://www.elsevier.com/xml/common/struct-bib/dtd“xmlns：ce =”http：// www。 elessvier.com/xml/common/dtd“xmlns：xlink =”http://www.w3.org/1999/xlink“xmlns：cals =”http://www.elsevier.com/xml/common/cals/ DTD“XMLNS：SA =”http://www.elsevier.com/xml/common/struction-aff / dd“> <mml：mrow> <mml：mi> mi>ω</ mml：mi> </ mml：mrow > </ mml：math> math> math> math altimg =“si16.gif”overflow 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A Facile Surface Reconstruction Mechanism toward Better Electrochemical Performance of Li 44 Ti 55 O 1212 in Lithium‐Ion Battery

摘要

A Facile Surface Reconstruction Mechanism toward Better Electrochemical Performance of Li ₄4 Ti ₅5 O ₁₂12 in Lithium‐Ion Battery