Synthesis and Structural Characterization of a Nickel Coordination Polymer Based on 4-(1H-Imidazol-1-yl)phenyl)methanone with Phthalic Acid

Sun Shu-Wen; Wang Gao-Feng; Zhang Xiao

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Synthesis and Structural Characterization of a Nickel Coordination Polymer Based on 4-(1H-Imidazol-1-yl)phenyl)methanone with Phthalic Acid

机译：基于4-（1H-咪唑-1-基）苯基用邻苯二甲酸甲酮的镍配位聚合物的合成与结构表征

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A nickel coordination polymer with V-shaped ligands, {[(L-1)(2)Ni(H2O)(2)] 2(C8H5O4)}(n), (L-1 = 4-(1H-imidazol-1-yl)phenyl)methanone) has been synthesized under the solvothermal conditions. The structure has been determined by the single-crystal X-ray diffraction analysis and characterized by the infrared spectroscopy and elemental analysis. The crystal is crystallized in the monoclinic sp. gr. P2(1)/c with the unit cell parameters a = 15.6387(3) angstrom, b = 8.0526(2) angstrom, c = 24.4791(6) angstrom, and = 129.2350(10)degrees, Z = 2. The adjacent [Ni(H2O)(2)] units are linked by two bridging L-1 ligands to form 1D looped chains, which are extended by the hydrogen bonds to yield a 3D framework.

机译：具有V形配体的镍配位聚合物，{[（1-1）（2）Ni（H 2 O）] 2（C8H5O4）}（N），（L-1 = 4-（1H-咪唑-1） - 苯基）甲酮）已在溶剂热条件下合成。该结构已经通过单晶X射线衍射分析确定，其特征在于红外光谱和元素分析。晶体在单斜晶型中结晶。 GR。 P2（1）/ c具有单位电池参数A = 15.6387（3）埃，B = 8.0526（2）埃，C = 24.4791（6）埃，= 129.2350（10）度，Z = 2.相邻的[ Ni（H2O）（2）]单元通过两个桥接L-1配体连接，形成1D环链链，其被氢键延伸以产生3D框架。

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《Crystallography reports》 |2018年第7期|共4页
作者
Sun Shu-Wen; Wang Gao-Feng; Zhang Xiao;
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Yuncheng Univ Dept Appl Chem Yuncheng 044000 Peoples R China;

Yuncheng Univ Dept Appl Chem Yuncheng 044000 Peoples R China;

Harbin Inst Technol Sch Chem &

Chem Engn MIIT Key Lab Crit Mat Technol New Energy Convers Harbin 150080 Heilongjiang Peoples R China;

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正文语种 eng
中图分类晶体学;
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机译：基于4-（1H-咪唑-1-基）苯基用邻苯二甲酸甲酮的镍配位聚合物的合成与结构表征
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Synthesis and Structural Characterization of a Nickel Coordination Polymer Based on 4-(1H-Imidazol-1-yl)phenyl)methanone with Phthalic Acid

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