From Self-Assembled Cu(II) Coordination Polymer to Shape-Controlled CuS Nanocrystals

Nagarathinam M; Chen JL; Vittal JJ

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From Self-Assembled Cu(II) Coordination Polymer to Shape-Controlled CuS Nanocrystals

机译：从自组装的Cu（II）配位聚合物到形状控制的CuS纳米晶体

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A hydrogen-bonded 1D coordination polymer, {[Cu(HSglu)(H2O)] center dot H2O}(n), 1, has been used as a precursor as well its a sacrificial template to synthesize covellite CuS nanomaterials. A remarkable correlation between the repeating patterns of the metal atoms in the coordination polymer with the preliminary shape of the obtained CuS is revealed from a detailed investigation of the effect of experimental conditions on the final products. The formation mechanism of the final mesostructured product has been explained oil the basis of the role of the chelating ligand and solvents in the self-assembly process.

机译：氢键键合的一维配位聚合物{[Cu（HSglu）（H2O）]中心点H2O}（n），1已被用作前驱体及其牺牲模板来合成贝壳铜CuS纳米材料。通过对实验条件对最终产物的影响的详细研究，揭示了配位聚合物中金属原子的重复图案与所得CuS的初始形状之间的显着相关性。最终的介孔结构产物的形成机理已经说明，这是螯合配体和溶剂在自组装过程中的作用基础。

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《Crystal growth & design》 |2009年第5期|共7页
作者
Nagarathinam M; Chen JL; Vittal JJ;
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正文语种 eng
中图分类晶体学;
关键词
COPPER SULFIDE NANORODS; SOLID-STATE TRANSFORMATION; SONOCHEMICAL SYNTHESIS; SELECTIVE SYNTHESIS; NANOWIRES; ROUTE; HOLLOW; PRECURSOR; MORPHOLOGIES; GROWTH;

机译：硫化铜纳米颗粒;固相转变;化学合成;选择性合成;纳米级;路线;空心;前驱体;发光;生长;

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1. From Self-Assembled Cu(II) Coordination Polymer to Shape-Controlled CuS Nanocrystals [J] . Nagarathinam M, Chen JL, Vittal JJ Crystal growth & design . 2009,第5期

机译：从自组装的Cu（II）配位聚合物到形状控制的CuS纳米晶体
2. Self-assembled 3D heterometallic Cu~(II)/Fe~(II) coordination polymers with octahedral net skeletons: Structural features, molecular magnetism, thermal and oxidation catalytic properties [J] . Karabach Y.Y., Guedes Da Silva M.F.C., Kopylovich M.N., Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2010,第23期

机译：具有八面体净骨架的自组装3D杂金属Cu〜（II）/ Fe〜（II）配位聚合物：结构特征，分子磁性，热和氧化催化性能
3. Topologically unique heterometallic Cu ~(II)/Li coordination polymers self-assembled from N, N-bis(2-hydroxyethyl)-2-aminoethanesulfonic acid biobuffer: Versatile catalyst precursors for mild hydrocarboxylation of alkanes to carboxylic acids [J] . Kirillova M.V., Kirillov A.M., Martins A.N.C., Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2012,第9期

机译：由N，N-双（2-羟乙基）-2-氨基乙烷磺酸生物缓冲剂自行组装的拓扑独特的杂金属Cu〜（II）/ Li配位聚合物：用于烷烃轻度加氢羧化为羧酸的多功能催化剂前体
4. Synthesis and Electrochemistry of Pt~(II) 2Cu~(II) 2Zn~(II) Coordination Polymers with D-Penicillaminate [C] . Naoto Kuwamura, Yoshinari Kurioka, Takumi Konno 日本化学会春季年会講演予稿集 . 2018

机译：Pt〜（II）2Cu〜（II）2ZN〜（II）配位聚合物与D-霉素的合成和电化学
5. Optical and structural studies of shape-controlled semiconductor nanocrystals and their self-assembled solids [D] . Diroll, Benjamin Tavenner 2015

机译：形状受控的半导体纳米晶体及其自组装固体的光学和结构研究
6. Catalytic Performance of a New 1D Cu(II) Coordination Polymer {Cu(NO3)(H2O)}(HTae)(44′-Bpy) for Knoevenagel Condensation [O] . Edurne S. Larrea, Roberto Fernández de Luis, María I. Arriortua 2016

机译：新型一维Cu（II）配位聚合物{Cu（NO3）（H2O）}（HTae）（44-Bpy）催化Knoevenagel缩合的性能
7. Bis(μ-chloro) bridged 1D Cu I and Cu II coordination polymer complex and mononuclear Cu II complex: Synthesis, crystal structure and biological properties [O] . Thangavel Thirunavukkarasu, Hazel A. Sparkes, C. Balachandran, 2018

机译：双（μ-氯）桥接1d Cu I和Cu II和Cu II配位聚合物复合物和单核Cu II复合物：合成，晶体结构和生物特性

From Self-Assembled Cu(II) Coordination Polymer to Shape-Controlled CuS Nanocrystals

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