Electrochemical synthesis of Bi _(1-x)Sb _x nanowires with simultaneous control on size, composition, and surface roughness

Müller S.; Sch?tz C.; Picht O.; Sigle W.; Kopold P.; Rauber M.; Alber I.; Neumann R.; Toimil-Molares M.E.

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Electrochemical synthesis of Bi _(1-x)Sb _x nanowires with simultaneous control on size, composition, and surface roughness

机译：Bi _（1-x）Sb _x纳米线的电化学合成，同时控制尺寸，组成和表面粗糙度

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We present the synthesis of Bi _(1-x)Sb _x nanowires with controlled composition between x = 0.05 and x = 0.40 over a wide range of diameters (20-100 nm) interesting for the investigation of the enhancement of thermoelectric efficiency via quantum size effects. We find that the relative concentration of Bi and Sb ions in the electrolyte, together with the deposition potential, determines the resulting nanowire composition. Morphology and composition were analyzed using X-ray diffraction, electron microscopy, and energy dispersive X-ray analysis. Two different templates were fabricated to enable the synthesis of nanowires with smooth and rough contour.

机译：我们提出了Bi_（1-x）Sb _x纳米线的合成，其在宽范围的直径范围（20-100 nm）内，x = 0.05和x = 0.40之间的可控组成对于研究通过量子提高热电效率引起了兴趣尺寸效果。我们发现电解质中Bi和Sb离子的相对浓度以及沉积电位决定了所得纳米线的组成。使用X射线衍射，电子显微镜和能量色散X射线分析法来分析形态和组成。制作了两种不同的模板，以合成具有光滑和粗糙轮廓的纳米线。

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《Crystal growth & design》 |2012年第2期|共7页
作者
Müller S.; Sch?tz C.; Picht O.; Sigle W.; Kopold P.; Rauber M.; Alber I.; Neumann R.; Toimil-Molares M.E.;
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正文语种 eng
中图分类晶体学;
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1. Electrochemical synthesis of Bi _(1-x)Sb _x nanowires with simultaneous control on size, composition, and surface roughness [J] . Müller S., Sch?tz C., Picht O., Crystal growth & design . 2012,第2期

机译：Bi _（1-x）Sb _x纳米线的电化学合成，同时控制尺寸，组成和表面粗糙度
2. Using galvanostatic electroforming of Bi_(1-x)Sb_x nanowires to control composition, crystallinity, and orientation [J] . Steven J. Limmer, Douglas L. Medlin, Michael P. Siegal, Journal of Materials Research . 2015,第2期

机译：使用Bi_（1-x）Sb_x纳米线的恒电流电铸来控制组成，结晶度和方向
3. Flowerlike submicrometer gold particles: Size- and surface roughness-controlled synthesis and electrochemical characterization [J] . Changsheng Shan, Dongxue Han, Jiangfeng Song, Journal of Materials Research . 2010,第9期

机译：花状亚微米级金颗粒：尺寸和表面粗糙度受控的合成和电化学表征
4. Flower-like Sub-micrometer Gold Particles: Size-and Surface Roughness-controlled Synthesis and Electrochemical Characterization [C] . Changsheng SHAN, Dongxue HAN, Jiangfeng SONG, The Twelfth international symposium on electroanalytical chemistry : Program amp; extended abstracts . 2009

机译：花状亚微米金颗粒：尺寸和表面粗糙度控制的合成和电化学表征
5. Fabrication of metallic surfaces with controlled roughness by electrochemical methods. [D] . Liu, Yihua. 2010

机译：通过电化学方法制造具有受控粗糙度的金属表面。
6. Effects of Nanowire Length and Surface Roughness on the Electrochemical Sensor Properties of Nafion-Free Vertically Aligned Pt Nanowire Array Electrodes [O] . Zhiyang Li, Calvin Leung, Fan Gao, 2015

机译：纳米线长度和表面粗糙度对无Nafion垂直排列的Pt纳米线阵列电极的电化学传感器性能的影响
7. Synthesis of Au$_x$Ag$_{1-x}$ nanowire-networks with controlled composition and defined wire diameter [O] . Dyzynski M., Burr L., Trautmann C., 2015

机译：具有受控成分和确定线径的Au $ _x $ Ag $ _ {1-x} $纳米线网络的合成

Electrochemical synthesis of Bi _(1-x)Sb _x nanowires with simultaneous control on size, composition, and surface roughness

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