Surface crystallization of cordierite from glass studied by high-temperature X-ray diffraction and electron backscatter diffraction (EBSD)

Wisniewski W.; Baptista C.A.; Müller M.; V?lksch G.; Rüssel C.

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Surface crystallization of cordierite from glass studied by high-temperature X-ray diffraction and electron backscatter diffraction (EBSD)

机译：通过高温X射线衍射和电子背散射衍射（EBSD）研究了堇青石在玻璃中的表面结晶

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A glass with the composition of stoichiometric cordierite (2Al _2O_3?2MgO?5SiO_2) shows surface crystallization during thermal annealing. High temperature X-ray diffraction (HT-XRD) was performed on a compact sample. The surface crystallization is further studied using scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD). The formation of an oriented layer at the immediate surface is not observed. This is in disagreement with previous reports in the literature. Topographical effects during crystallization and EBSD pattern acquisition are analyzed by atomic force microscopy.

机译：具有化学计量的堇青石（2Al _2O_3→2MgO·5SiO_2）组成的玻璃在热退火期间显示出表面结晶。在紧凑的样品上进行了高温X射线衍射（HT-XRD）。使用扫描电子显微镜（SEM）和电子背散射衍射（EBSD）进一步研究了表面结晶。没有观察到在直接表面上形成取向层。这与文献中先前的报道不同。通过原子力显微镜分析结晶过程中的形貌效应和EBSD图案。

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《Crystal growth & design》 |2011年第10期|共7页
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Wisniewski W.; Baptista C.A.; Müller M.; V?lksch G.; Rüssel C.;
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1. Surface crystallization of cordierite from glass studied by high-temperature X-ray diffraction and electron backscatter diffraction (EBSD) [J] . Wisniewski W., Baptista C.A., Müller M., Crystal growth & design . 2011,第10期

机译：通过高温X射线衍射和电子背散射衍射（EBSD）研究了堇青石在玻璃中的表面结晶
2. Analysis of the cordierite X-phase and phase transformation by electron backscatter diffraction (EBSD) [J] . Wolfgang Wisniewski, Christian Rüssel Journal of Non-Crystalline Solids: A Journal Devoted to Oxide, Halide, Chalcogenide and Metallic Glasses, Amorphous Semiconductors, Non-Crystalline Films, Glass-Ceramics and Glassy Composites . 2014,第Null期

机译：电子反散射衍射（EBSD）分析堇青石的X相和相变
3. Oriented Nucleation of both Ge-Fresnoite and Benitoite/BaGe4O9 during the Surface Crystallisation of Glass Studied by Electron Backscatter Diffraction [J] . Wolfgang Wisniewski, Marek Patschger, Steliana Murdzheva, Scientific reports. . 2016,第1期

机译：电子背向散射研究玻璃表面结晶过程中锗钙镁铁矿和贝氏体/ BaGe4O9的定向成核
4. Textural Analysis of a Microcrystalline Quartz using X-Ray and Electron Backscatter Diffraction (EBSD) Techniques [C] . Daniel Chateigner, Gianfranco Camana, Patrick Trimby 13th International Conference on Textures of Materials Pt.2 Aug 26-30, 2002 Seoul, Korea . 2002

机译：使用X射线和电子背散射衍射（EBSD）技术对微晶石英进行纹理分析
5. The growth of epitaxial iron oxides on platinum (111) as studied by x-ray photoelectron diffraction, scanning tunneling microscopy, and low-energy electron diffraction. [D] . Kim, Yong-Joo. 1995

机译：通过X射线光电子衍射，扫描隧道显微镜和低能电子衍射研究了外延氧化铁在铂（111）上的生长。
6. Oriented Nucleation of both Ge-Fresnoite and Benitoite/BaGe4O9 during the Surface Crystallisation of Glass Studied by Electron Backscatter Diffraction [O] . Wolfgang Wisniewski, Marek Patschger, Steliana Murdzheva, -1

机译：电子背向散射研究玻璃表面结晶过程中锗钙镁铁矿和贝氏体/ BaGe4O9的定向成核
7. Oriented Nucleation of both Ge-Fresnoite and Benitoite/BaGe4O9 during the Surface Crystallisation of Glass Studied by Electron Backscatter Diffraction [O] . Wolfgang Wisniewski, Marek Patschger, Steliana Murdzheva, 2016

机译：在通过电子反向散射衍射研究的玻璃表面结晶期间导向Ge-Fresnoite和Benitoite / Bage4O9的成核

Surface crystallization of cordierite from glass studied by high-temperature X-ray diffraction and electron backscatter diffraction (EBSD)

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