Synthesis of Bi2Se3 nanosheets by microwave heating using an ionic liquid

Jiang Y; Zhu YJ; Cheng GF

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Synthesis of Bi2Se3 nanosheets by microwave heating using an ionic liquid

机译：离子液体微波加热合成Bi2Se3纳米片

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Bi2Se3 nanosheets with thicknesses of 50-100 nm have been successfully synthesized by a simple microwave heating method using selenium powder, Bi(NO3)(3)center dot 5H(2)O, HNO3 aqueous solution, ethylenediamine or ethylene glycol, and an ionic liquid 1-n-butyl-3-methylimidazolium tetrafluoroborate. The effects of experimental parameters on the formation of the products were investigated. The products were characterized by X-ray powder diffraction, scanning electron microscopy, and transmission electron microscopy.

机译：通过简单的微波加热方法，使用硒粉，Bi（NO3）（3）中心点5H（2）O，HNO3水溶液，乙二胺或乙二醇和离子离子，通过简单的微波加热方法成功合成了厚度为50-100 nm的Bi2Se3纳米片液体1-正丁基-3-甲基咪唑鎓四氟硼酸盐。研究了实验参数对产物形成的影响。通过X射线粉末衍射，扫描电子显微镜和透射电子显微镜对产物进行表征。

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来源
《Crystal growth & design》 |2006年第9期|共3页
作者
Jiang Y; Zhu YJ; Cheng GF;
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正文语种 eng
中图分类晶体学;
关键词
ASSISTED SYNTHESIS; BISMUTH SELENIDE; SONOCHEMICAL SYNTHESIS; THIN-FILMS; NANORODS; TEMPERATURE; NANOWIRES;

机译：辅助合成;硒化铋;化学合成;薄膜;纳米;温度;纳米;

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1. Synthesis of Bi2Se3 nanosheets by microwave heating using an ionic liquid [J] . Jiang Y, Zhu YJ, Cheng GF Crystal growth & design . 2006,第9期

机译：离子液体微波加热合成Bi2Se3纳米片
2. Intensification of the Capillary-Based Kolbe-Schmitt Synthesis from Resorcinol by Reactive Ionic Liquids, Microwave Heating, or a Combination Thereof [J] . Faysal Benaskar, Volker Hessel, Ulrich Krtschil Organic process research & development . 2009,第5期

机译：反应性离子液体，微波加热或两者结合可增强间苯二酚从毛细管中合成的Kolbe-Schmitt
3. Microwave heating coupled with ionic liquids: Synthesis and properties of novel optically active polyamides, thermal degradation and electrochemical stability on multi-walled carbon nanotubes electrode [J] . Mallakpour S, Taghavi M Polymer: The International Journal for the Science and Technology of Polymers . 2008,第15期

机译：微波加热与离子液体耦合：新型光学活性聚酰胺的合成与性能，在多壁碳纳米管电极上的热降解和电化学稳定性
4. Intensified Kolbe-Schmitt Synthesis using Continuous Microreactor Processing, Reactive Ionic Liquids and Microwave Heating [C] . Ullrich Krtschil, Faysal Benaskar, Volker Hessel, SynTOP Conference on Smart Synthesis and Technologies for Organic Processes . 2008

机译：使用连续微反应器加工，反应离子液体和微波加热增强Kolbe-Schmitt合成
5. Synthesis of Ionic Liquids and Magnetic Ionic Liquids and Their Application in Dispersive Liquid-liquid Microextraction [D] . Pierson, Stephen A. 2018

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6. Ionic Liquids and Ohmic Heating in Combination for Pd-Catalyzed Cross-Coupling Reactions: Sustainable Synthesis of Flavonoids [O] . Vera L. M. Silva, Raquel G. Soengas, Artur M. S. Silva 2020

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Synthesis of Bi2Se3 nanosheets by microwave heating using an ionic liquid

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