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New synthetic route and characterization of magnesium borate nanorods

机译：硼酸镁纳米棒的新合成路线和表征

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摘要

In the current research, we have successfully fabricated single-crystalline triclinic MgB2O5 and orthorhombic Mg3B2O6 nanorods by a solvothermal method under supercritical conditions. Detailed microstructures of as-synthesized products were characterized by X-ray diffraction, scanning electron microscopy (SEM), transmission electron microscopy, and X-ray photoelectron spectroscopy. It was found that the morphology and phase of the products were strongly dependent on the reaction conditions, such as the ratio of Mg/B, temperature, reaction time, and solvent media. The formation process Of Mg2B2O5 nanorods was illustrated based on SEM observations of the different reaction stages. This technique may also have great potential in realizing other nanostructured materials.
机译：在当前的研究中，我们已经通过溶剂热法在超临界条件下成功地制备了单晶三斜晶MgB2O5和正交晶Mg3B2O6纳米棒。通过X射线衍射，扫描电子显微镜（SEM），透射电子显微镜和X射线光电子能谱表征了所合成产品的详细微观结构。发现产物的形态和相在很大程度上取决于反应条件，例如Mg / B的比例，温度，反应时间和溶剂介质。基于不同反应阶段的SEM观察结果，阐明了Mg2B2O5纳米棒的形成过程。该技术在实现其他纳米结构材料方面也可能具有巨大潜力。

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