Hydrothermal synthesis of uniform cuprous oxide microcrystals with controlled morphology

Zhao HY; Wang YF; Zeng JH

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Hydrothermal synthesis of uniform cuprous oxide microcrystals with controlled morphology

机译：水热法合成形态可控的均匀氧化亚铜微晶

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Cuprous oxide (Cu2O) with controlled morphology was synthesized via a hydrothermal method by reducing copper nitrate with formic acid. Reactant concentration, reaction temperature, and time show strong effects on the phase formation and morphology of the products. The products were characterized by X-ray power diffraction (XRD), scanning electron microscope (SEM), and UV-vis diffuse reflectance spectroscopy. The possible crystal growth processes have been proposed. The band gap versus different morphology was also studied.

机译：通过水热法，用甲酸还原硝酸铜，合成了形态可控的氧化亚铜（Cu2O）。反应物浓度，反应温度和时间对产物的相形成和形态显示强烈影响。产品通过X射线功率衍射（XRD），扫描电子显微镜（SEM）和紫外可见漫反射光谱进行表征。已经提出了可能的晶体生长过程。还研究了带隙对不同形态的影响。

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《Crystal growth & design》 |2008年第10期|共4页
作者
Zhao HY; Wang YF; Zeng JH;
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正文语种 eng
中图分类晶体学;
关键词
CU2O MICROCRYSTALS; SHAPE EVOLUTION; ARYL HALIDES; NANOCRYSTALS; NANOSPHERES; NANOCUBES; TEMPERATURE; NANOWIRES; GROWTH; ROUTE;

机译：CU2O微晶体;形状演变;ARYL卤化物;纳米晶体;纳米球;纳米球;温度;纳米线;生长;路线;

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专利

1. Hydrothermal synthesis of uniform cuprous oxide microcrystals with controlled morphology [J] . Zhao HY, Wang YF, Zeng JH Crystal growth & design . 2008,第10期

机译：水热法合成形态可控的均匀氧化亚铜微晶
2. Simultaneous Phase- And Morphology-controlled Synthesis Of Mno_2 Crystals Through Controlled Release Of Cuprous Ions In Hydrothermal Condition [J] . Yange Zhang, Zhi Zheng, Ka Wai Wong, Journal of Materials Research . 2009,第1期

机译：水热条件下亚铜离子的受控释放同时合成和形貌控制的Mno_2晶体
3. Shaped-Controlled Synthesis of Nanosized Cuprous Oxides by Hydrothermal Oxidation Method [J] . Nguyen Tien Thao, Mai Quang Tuong Asian Journal of Chemistry: An International Quarterly Research Journal of Chemistry . 2014,第22期

机译：水热氧化法形变控制合成纳米氧化亚铜
4. Hydrothermal synthesis of SrSO_4:Eu~(2+) microcrystals with different morphologies and its luminescence properties [C] . Jiayue Sun, Qiumei Di, Liu Han, International Conference on Advanced Design and Manufacturing Engineering . 2014

机译：SRSO_4的水热合成：Eu〜（2+）微晶，具有不同形态及其发光性能
5. Morphological Control of Copper and Cuprous Oxide Nanoparticles via Synthesis and Oxidation/Reduction Reactions. [D] . Mowbray, Ryan. 2013

机译：通过合成和氧化/还原反应控制铜和氧化亚铜纳米粒子的形态。
6. Controlled synthesis and visible light photocatalytic activity of Bi12GeO20 uniform microcrystals [O] . Zhen Wan, Gaoke Zhang -1

机译：Bi12GeO20均匀微晶的受控合成及可见光光催化活性
7. Shaped-Controlled Synthesis of Nanosized Cuprous Oxides by Hydrothermal Oxidation Method [O] . Nguyen Tien Thao, Mai Quang Tuong 2014

机译：水热氧化法成型控制纳米亚铜氧化物的合成

Hydrothermal synthesis of uniform cuprous oxide microcrystals with controlled morphology

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