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首页> 外文期刊>Advanced Powder Technology: The internation Journal of the Society of Powder Technology, Japan >Magnetic and structural properties of amorphousanocrystalline Fe_(42)Ni_(28)Zr8Ta2B_(10)C_(10) soft magnetic alloy produced by mechanical alloying
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Magnetic and structural properties of amorphousanocrystalline Fe_(42)Ni_(28)Zr8Ta2B_(10)C_(10) soft magnetic alloy produced by mechanical alloying

机译:机械合金化制备的非晶/纳米晶Fe_(42)Ni_(28)Zr8Ta2B_(10)C_(10)软磁合金的磁性和结构性能

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摘要

Magnetic behavior, microstructural evolution, and amorphization studies of Fe_(42)Ni_(28)Zr8Ta2B_(10)C_(10)o alloy, synthetized by mechanical alloying, were investigated. The non-equilibrium microstructure originated from a grain size reduction to about 2.5 nm indicated by X-ray diffraction and the introduction of internal strain up to 3.8%. The results showed that as the milling time increased the amorphous phase became dominant and reached about 92 wt.% at 176 h. The magnetic measurements which were obtained by vibrating sample magnetometer, showed an increase in saturation magnetization up to 12 h and then a decrease until 66 h followed by a slow increase. Simultaneously, the coercivity increased, decreased and finally reached a constant level of about 24 Oe. The value of coercivity obtained in the present study is less than the values reported for the widely investigated mechanically alloyed Fe-Ni-Zr-B alloys, which shows this alloy is a very good soft magnet.
机译:研究了通过机械合金化合成的Fe_(42)Ni_(28)Zr8Ta2B_(10)C_(10)o合金的磁行为,微观组织演变和非晶化研究。非平衡微观结构是由X射线衍射表明晶粒尺寸减小到约2.5 nm以及引入高达3.8%的内部应变所致。结果表明,随着研磨时间的增加,非晶相占主导地位,并在176 h达到约92 wt。%。通过振动样品磁力计获得的磁测量结果显示,饱和磁化强度最多增加12小时,然后减小直到66小时,然后缓慢增加。同时,矫顽力增加,降低并最终达到约24 Oe的恒定水平。在本研究中获得的矫顽力值小于广泛研究的机械合金化Fe-Ni-Zr-B合金报道的值,这表明该合金是一种非常好的软磁体。

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