The In Situ Study of the Fe3O4/DMSO Ferrofluid Synthesis

Yakushkin S. S.; Kirillov V. L.; Shalygin A. S.; Martyanov O. N.

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The In Situ Study of the Fe3O4/DMSO Ferrofluid Synthesis

机译：Fe3O4 / DMSO铁物质流体合成的原位研究

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Electron spin resonance in situ was applied to study the initial stages of ferrofluid formation in combination with the X-ray diffraction, high-resolution transmission electron microscopy and Fourier transform infrared spectroscopy studies data. The ultrafine (d = 4 nm) magnetite in dimethylsulfoxide ferrofluid with a narrow size nanoparticles distribution was obtained in a single step at room temperature by admixing butylene oxide to a solution of iron (II) and (III) chlorides in dimethylsulfoxide. It has been shown that at the first step of the ferrofluid synthesis antiferromagnetically ordered iron containing phase is formed, which can be correlated with iron hydroxides.

机译：应用了原位原位的旋转共振，研究了与X射线衍射，高分辨率透射电子显微镜和傅立叶变换红外光谱研究数据组合研究了铁磁流体形成的初始阶段。通过将氧化物与二甲基硫氧化物中的铁（II）和（III）氯化物溶液混合在室温下，在单步比二甲基硫氧化物铁氟甲磺酸盐中的超细（D = 4nm）磁铁矿。已经表明，在铁磁流体合成的第一步，形成反铁晶有序的熨烫相，其可以与铁氢氧化物相关。

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《Applied Magnetic Resonance》 |2019年第10期|共7页
作者
Yakushkin S. S.; Kirillov V. L.; Shalygin A. S.; Martyanov O. N.;
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Russian Acad Sci Boreskov Inst Catalysis Siberian Branch Lavrentieva 5 Novosibirsk 630090 Russia;

Russian Acad Sci Boreskov Inst Catalysis Siberian Branch Lavrentieva 5 Novosibirsk 630090 Russia;

Russian Acad Sci Boreskov Inst Catalysis Siberian Branch Lavrentieva 5 Novosibirsk 630090 Russia;

Russian Acad Sci Boreskov Inst Catalysis Siberian Branch Lavrentieva 5 Novosibirsk 630090 Russia;

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中图分类磁性弛豫及共振现象;
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1. The In Situ Study of the Fe3O4/DMSO Ferrofluid Synthesis [J] . Yakushkin S. S., Kirillov V. L., Shalygin A. S., Applied Magnetic Resonance . 2019,第10期

机译：Fe3O4 / DMSO铁物质流体合成的原位研究
2. Synthesis and application of bilayer-surfactant-enveloped Fe3O4 nanoparticles: water-based bilayer-surfactant-enveloped ferrofluids [J] . Chen Bai-yi, Qiu Jian-hui, Feng Hui-xia International Journal of Minerals,Metallurgy and Materials . 2016,第2期

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3. Synthesis of water-based bilayer surfactants enveloped Fe3O4 nanoparticles used as ferrofluids [J] . Baiyi Chen, Jianhui Qiu, Eiichi Sakai 复合材料シンポシウム讲演要旨集． . 2014,第1期

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The In Situ Study of the Fe3O4/DMSO Ferrofluid Synthesis

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