Application of Carbon Paste Electrode Modified with Carbon Nanofibres/Polyaniline/Platinum Nanoparticles as an Electrochemical Sensor for the Determination of Bezafibrate

Rajpurohit Anuja S.; Punde Ninad S.; Rawool Chaitali R.; Srivastava Ashwini K.

摘要

Abstract > The present study deals with the development of an electrochemical sensor for quantitative determination of Bezafibrate (BZF) based on carbon nanofibers/polyaniline/platinum nanoparticles modified carbon paste electrode (CNF/PANI/Pt/CPE). BZF is a fibric acid derivative and is used largely in the treatment of lipid disorders. The nanocomposite was synthesized by in?situ polymerization of aniline using ammonium persulphate and platinum nanoparticles were uniformly decorated on the CNF/PANI surface by reducing hexachloroplatinic acid using sodium borohydride. The electrochemical response of BZF at CNF/PANI/Pt/CPE was studied using cyclic voltammetry (CV), differential pulse voltammetry (DPV) and electrochemical impedance spectroscopy (EIS). The above study resulted into significant improvement of the electrochemical signal towards the oxidation of BZF, revealing that the oxidation process is highly favorable at the surface of modified electrode. The anodic peak current I <sub>p</sub> (μA) is found to be linearly dependent on BZF concentration in the range of 0.025?μM to 100?μM with a detection limit of 2.46?nM. The practical analytical utilities of the sensor were investigated by performing the experiments on synthetic pharmaceutical formulations, human blood serum and urine samples which offered good recovery, suggesting the high efficacy and authenticity of CNF/PANI/Pt/CPE sensor for BZF determination. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</标题> >本研究涉及开发电化学传感器，用于定量测定Bezafbribate（BZF）基于碳纳米纤维/聚苯胺/铂纳米颗粒改性碳浆电极（CNF / PANI / PT / CPE）。 BZF是一种纤维酸衍生物，主要用于治疗脂质疾病。通过使用硼酸氢钠还原六氯铂含有铵脱脂，铂纳米颗粒在CNF / PANI表面上均匀地装饰在CNF / PANI表面上的苯胺聚合的纳米复合材料。使用循环伏安法（CV），差分脉冲伏安法（DPV）和电化学阻抗光谱（EIS）研究了BZF在CNF / PANI / PT / PT / CPE处的电化学响应。上述研究导致电化学信号朝向BZF氧化的显着改善，揭示了氧化过程在改性电极表面的高处。发现阳极峰值电流I <Sub> P </ sub>（μA）是线性取决于0.025Ωμm至100Ωμm的BZF浓度，检测限为2.46Ω·Nm。通过在提供良好的恢复的合成药物制剂，人血清和尿液样本的实验来研究传感器的实际分析公用事业，这表明BZF测定的CNF / PANI / PT / CPE传感器的高疗效和真实性。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2018年第3期</span><b style="margin: 0 2px;">|</b><span>共12页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rajpurohit Anuja S.&option=202" target="_blank" rel="nofollow">Rajpurohit Anuja S.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Punde Ninad S.&option=202" target="_blank" rel="nofollow">Punde Ninad S.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rawool Chaitali R.&option=202" target="_blank" rel="nofollow">Rawool Chaitali R.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Srivastava Ashwini K.&option=202" target="_blank" rel="nofollow">Srivastava Ashwini K.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Chemistry University of Mumbai Vidyanagari Santacruz (East)Mumbai – 400 098 India;</p> <p>Department of Chemistry University of Mumbai Vidyanagari Santacruz (East)Mumbai – 400 098 India;</p> <p>Department of Chemistry University of Mumbai Vidyanagari Santacruz (East)Mumbai – 400 098 India;</p> <p>Department of Chemistry University of Mumbai Vidyanagari Santacruz (East)Mumbai – 400 098 India;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bezafibrate&option=203" rel="nofollow">Bezafibrate;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Carbon nanofibers/Polyaniline/Platinum nanocomposite&option=203" rel="nofollow">Carbon nanofibers/Polyaniline/Platinum nanocomposite;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Carbon paste electrode&option=203" rel="nofollow">Carbon paste electrode;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=human serum and urine samples&option=203" rel="nofollow">human serum and urine samples;</a> </p> <div class="translation"> 机译：Bezafiblate;碳纳米纤维/聚苯胺/铂纳米复合材料;碳浆料电极;人血清和尿液样本; 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<b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130408594473.html">MANUFACTURING HYBRID PASTE OF POLYANILINE OR CAMPHORSULFONIC ACID CONTAINING PLATINUM-ATTACHED CARBON NANOPARTICLE AND METHOD FOR MANUFACTURING FLEXIBLE DIPOLE TAG ANTENNA USING SAME</a> <b>[P]</b> . <span> 外国专利：  KR101740849B1 </span> <span> . 2017-06-08</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：制造含铂连接的碳纳米粒子的聚苯胺或聚草酸的混合浆料以及使用相同方法制造柔性双偶极天线的方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130408736073.html">PRINTED CARBON ELECTRODE-BASED ELECTROCHEMICAL SENSOR FUNCTIONALIZED WITH PLATINUM NANOPARTICLE FOR MEASURING PENICILLIN RESIDUAL ANTIBIOTIC</a> <b>[P]</b> . <span> 外国专利：  KR20170032107A </span> <span> . 2017-03-22</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：铂纳米粒子作用的印染碳基电化学传感器测定青霉素残留量 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130411649926.html">METHOD FOR MODIFYING CARBON MATERIAL ELECTRODE SURFACE BY CURRENT CARRYING, SURFACE-MODIFIED CARBON MATERIAL ELECTRODE, AND ELECTROCHEMICAL CAPACITOR COMPRISING SURFACE-MODIFIED CARBON MATERIAL ELECTRODE</a> <b>[P]</b> . <span> 外国专利：  WO2016122070A1 </span> <span> . 2016-08-04</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过电流输送，表面改性的碳材料电极和包括表面改性的碳材料电极的电化学电容器对碳材料电极表面进行改性的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img 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