NH        <sub >2</sub>2        ‐Functionalized Multi Walled Carbon Nanotubes Decorated with ZnO Nanoparticles and Graphene Quantum Dots for Sensitive Assay of Pimozide

Aftab Saima; Kurbanoglu Sevinc; Ozcelikay Goksu; Shah Afzal; Ozkan Sibel A.

摘要

Abstract > In this study, a novel and sensitive electrochemical nanosensor for the determination of antipsychotic drug Pimozide (PZ) is proposed using NH <sub>2</sub> functionalized multi walled carbon nanotubes (NH <sub>2</sub> f MWCNT) decorated with and ZnO nanoparticles (ZnONPs) co‐catalyzed by graphene quantum dots (GQDs). Prior to electrochemical analyses of PZ, the designed nanosensor was well characterized in terms of surface morphology by scanning electron microscopy (SEM) and SEM armed with EDX analysis. Electrochemical impedance spectroscopy (EIS) employed to investigate the electron transfer capability and cyclic voltammetry (CV) technique was used to successfully compare the redox response of PZ on the surface of modified and unmodified electrode. The designed nanosensor response was linear between 6.25×10 ?11 –1.20×10 ?7 ?M concentration range of PZ with a limit of detection value as 1.02×10 ?11 ?M. The influence of interfering agents was further studied to examine the selectivity of the designed sensor. A rapid screening of PZ as is required in pharmaceutical and biological samples underscores the paramount importance of nano based electrochemical sensor for its sensitive and selective detection. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract type =“main”xml：lang =“en”> <标题类型=“main”>摘要</标题> >在本研究中，一种新颖的和敏感的电化学纳米传感器，用于测定抗精神病药pimozide（pz使用NH <sub> 2 </ sub>官能化的多壁碳纳米管（NH <sub> 2 </ sub> f </ i> mwcnt）用ZnO纳米颗粒（ZnOnps）官能化（ZnOnps）催化石墨烯量子点（GQDS）。在PZ的电化学分析之前，通过扫描电子显微镜（SEM）和EDX分析，设计了设计的纳米传感器在表面形态方面具有很好的表征。用于研究电子转移能力和循环伏安法（CV）技术的电化学阻抗光谱（EIS）用于成功地比较改性和未改性电极表面上PZ的氧化还原响应。设计的纳米传感器响应是线性的6.25×10 α11/11-1.20×10 7 </ sup>Δm的pz浓度范围，其检测值限制为1.02×10 <sup >？11 </ sup>？m。进一步研究了干扰剂的影响，以检查设计传感器的选择性。在药物和生物样品中需要的快速筛选PZ，强调了基于纳米电化学传感器的最重要的重要性，以实现其敏感和选择性检测。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2019年第6期</span><b style="margin: 0 2px;">|</b><span>共12页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aftab Saima&option=202" target="_blank" rel="nofollow">Aftab Saima;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kurbanoglu Sevinc&option=202" target="_blank" rel="nofollow">Kurbanoglu Sevinc;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ozcelikay Goksu&option=202" target="_blank" rel="nofollow">Ozcelikay Goksu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shah Afzal&option=202" target="_blank" rel="nofollow">Shah Afzal;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ozkan Sibel A.&option=202" target="_blank" rel="nofollow">Ozkan Sibel A.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Ankara UniversityDepartment of Analytical ChemistryAnkara Turkey;</p> <p>Ankara UniversityDepartment of Analytical ChemistryAnkara Turkey;</p> <p>Ankara UniversityDepartment of Analytical ChemistryAnkara Turkey;</p> <p>University of BahrainDepartment of ChemistrySakhir 32038 Bahrain;</p> <p>Ankara UniversityDepartment of Analytical ChemistryAnkara Turkey;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pimozide&option=203" rel="nofollow">Pimozide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Carbon Nanotubes&option=203" rel="nofollow">Carbon Nanotubes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Quantum Dots&option=203" rel="nofollow">Quantum Dots;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZnO Nanoparticles&option=203" rel="nofollow">ZnO Nanoparticles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Electrochemical Nanosensors&option=203" rel="nofollow">Electrochemical Nanosensors;</a> </p> <div class="translation"> 机译：Pimozide;碳纳米管;量子点;ZnO纳米粒子;电化学纳米调传料; 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Min Zheng</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=郑敏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,郑敏</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yu Chen&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Yu Chen</a> <span> <a href="/conference-cn-7084/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十三届全国有机分子电化学与工业学术会议 </a> <span> <span> . 2012</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020316085428.html">糖敏感型聚磷酯酯基纳米粒子用于胰岛素递释系统</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李红萍&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 李红萍</a> <span> . 2020</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120109538596.html">以超细Au纳米粒子修饰的球形多片层结构ZnO为敏感层的乙炔气体传感器及制备方法</a> <b>[P]</b> . <span> 中国专利： CN107064220A </span> <span> . 2017-08-18</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120109132723.html">一种pH敏感响应的N、S共掺杂石墨烯量子点的制备及脲酶活性的测定</a> <b>[P]</b> . <span> 中国专利： CN106634984A </span> <span> . 2017-05-10</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130401217096.html">Method of producing carbon layers containing graphene on nanoparticles, in particular quantum dots, containing at least one semiconductor material, and reaction vessel for producing carbon layers containing graphene on nanoparticles containing at least one semiconductor material, in particular metal oxides and composite materials</a> <b>[P]</b> . <span> 外国专利：  PL430994A1 </span> <span> . 2020-02-24</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：在包含至少一种半导体材料的纳米颗粒上制备包含石墨烯的碳层的方法，以及在包含至少一种半导体材料，特别是金属氧化物和复合材料的纳米颗粒上制备包含石墨烯的碳层的反应容器 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130416669688.html">FABRICATION OF VISIBLE LIGHT PHOTOCATALYST CONTAINING GRAPHENE QUANTUM DOT AND SILVER NANOPARTICLES DECORATED TITANIA NANOPARTICLES</a> <b>[P]</b> . <span> 外国专利：  KR101420983B1 </span> <span> . 2014-07-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包含石墨烯量子点和银纳米颗粒的二氧化钛纳米微粒的可见光催化剂的制备 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130402819802.html">METAL NANOPARTICLE-DECORATED CARBON NANOTUBES AND METHOD OF PRODUCING METAL NANOPARTICLE-DECORATED CARBON NANOTUBES</a> <b>[P]</b> . <span> 外国专利：  EP3396365B1 </span> <span> . 2020-08-19</span> </div> <p class="zwjiyix 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NH 22 ‐Functionalized Multi Walled Carbon Nanotubes Decorated with ZnO Nanoparticles and Graphene Quantum Dots for Sensitive Assay of Pimozide

摘要

NH ₂2 ‐Functionalized Multi Walled Carbon Nanotubes Decorated with ZnO Nanoparticles and Graphene Quantum Dots for Sensitive Assay of Pimozide