Highly Sensitive Amperometric Sensor for Eugenol Quantification Based on CeO <sub xmlns='http://www.wiley.com/namespaces/wiley'>2</sub>2 Nanoparticles and Surfactants

Ziyatdinova Guzel; Ziganshina Endzhe; Romashkina Svetlana; Budnikov Herman

摘要

Abstract > Amperometric sensor for eugenol based on glassy carbon electrode (GCE) modified with CeO <sub>2</sub> nanoparticles dispersed in surfactant was fabricated. The effect of surfactant nature (sodium dodecylsulfate, cetylpyridinium bromide (CPB) and Brij? 35) on eugenol voltammetric behaviour was tested. In comparison to CeO <sub>2</sub> ‐H <sub>2</sub> O/GCE, CeO <sub>2</sub> ‐CPB/GCE showed 2.8‐fold increased current and 70 mV cathodic shift of potential in the diffusion‐controlled irreversible electrooxidation. The electrodes were characterized with SEM and EIS. CeO <sub>2</sub> ‐CPB/GCE showed significantly lower charge transfer resistance (2.6±0.3 kΩ vs. 20±1 kΩ for CeO <sub>2</sub> ‐H <sub>2</sub> O/GCE and 173±9 kΩ for GCE). Under conditions of DPV, the sensor linear dynamic range is 0.075‐75.0?μM of eugenol with the limits of detection (LOD) and quantification (LOQ) of 19.1 and 63.8 nM, respectively. The sensor exhibited high sensitivity, selectivity, good reproducibility and fast response and was applied for the real samples analysis (essential oils and clove spices). The results obtained correspond well to the data of spectrophotometric method. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> > amperometric传感器对于基于用CEO <sub> 2的玻璃碳电极（GCE）的丁香酚制造了分散在表面活性剂中的CEO <sub> 2 </ sub>纳米颗粒。测试了表面活性剂性质（十二烷基硫酸钠，十六烷磺酸钠，溴化吡啶鎓（CPB）和Brijα35）对丁醇伏安法的影响进行了测试。与CEO <sub> 2 </ sub> -h <sub> 2 </ sub> o / gce，CEO <sub> 2 </ sub> -cpb / gce显示出2.8倍的电流和70 mV阴极转变扩散控制的不可逆电氧化中的潜力。电极的特征在于SEM和EIS。 CEO <sub> 2 </ sub> -cpb / gce显示出显着较低的电荷传递电阻（CEO <sub> 2 </ sub> -h <sub> 2 </ sub>的2.6±0.3kΩ与20±1kΩ用于GCE的O / GCE和173±9kΩ）。在DPV的条件下，传感器线性动态范围分别为0.075-75.0≤0.075-75.0≤0.075-75.0≤0.075-75.0≤0.075-75.0≤0.075-75.0≤0.075-75.0≤0.075-75.0μm的丁香酚，分别为19.1和63.8 nm的检测（LOD）和定量（LOQ）。传感器表现出高灵敏度，选择性，良好的再现性和快速反应，并应用于真实样品分析（精油和丁香香料）。获得的结果对应于分光光度法的数据。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2017年第4期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ziyatdinova Guzel&option=202" target="_blank" rel="nofollow">Ziyatdinova Guzel;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ziganshina Endzhe&option=202" target="_blank" rel="nofollow">Ziganshina Endzhe;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Romashkina Svetlana&option=202" target="_blank" rel="nofollow">Romashkina Svetlana;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Budnikov Herman&option=202" target="_blank" rel="nofollow">Budnikov Herman;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Analytical Chemistry Department A.M. Butlerov Institute of ChemistryKazan Federal University Kremlyevskaya 18Kazan 420008 Russian Federation tel: +7-843-2337736 fax: +7-843-2387901;</p> <p>Analytical Chemistry Department A.M. Butlerov Institute of ChemistryKazan Federal University Kremlyevskaya 18Kazan 420008 Russian Federation tel: +7-843-2337736 fax: +7-843-2387901;</p> <p>Analytical Chemistry Department A.M. Butlerov Institute of ChemistryKazan Federal University Kremlyevskaya 18Kazan 420008 Russian Federation tel: +7-843-2337736 fax: +7-843-2387901;</p> <p>Analytical Chemistry Department A.M. Butlerov Institute of ChemistryKazan Federal University Kremlyevskaya 18Kazan 420008 Russian Federation tel: +7-843-2337736 fax: +7-843-2387901;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sensors&option=203" rel="nofollow">Sensors;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chemically modified electrodes&option=203" rel="nofollow">Chemically modified electrodes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Metal oxide nanoparticles&option=203" rel="nofollow">Metal oxide nanoparticles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Surfactants&option=203" rel="nofollow">Surfactants;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Eugenol&option=203" rel="nofollow">Eugenol;</a> </p> <div class="translation"> 机译：传感器;化学改性电极;金属氧化物纳米颗粒;表面活性剂;丁香酚; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a 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Highly Sensitive Amperometric Sensor for Eugenol Quantification Based on CeO 22 Nanoparticles and Surfactants

摘要

Highly Sensitive Amperometric Sensor for Eugenol Quantification Based on CeO ₂2 Nanoparticles and Surfactants