Facile Synthesis of Ni(OH)        <sub >2</sub>2        Modified Disposable Pencil Graphite Electrode and its Application for Highly Sensitive Non‐enzymatic Glucose Sensor

Chelaghmia Mohamed Lyamine; Nacef Mouna; Affoune Abed Mohamed; Pontié Maxime; Derabla Tahar

摘要

Abstract > In this study, a low‐cost, disposable, sensitive and selective electrochemical sensor was developed for glucose determination, which is based on a pencil graphite electrode (PGE) modified with nickel hydroxide. Cyclic voltammetry was used to deposit nickel on PGE. The morphology and composition of the unmodified and modified PGE electrodes were characterized by field‐emission scanning electron microscopy (FE‐SEM), atomic force microscopy (AFM) and energy‐dispersive X‐ray spectroscopy (EDX). The performance of the as modified electrode towards the electrooxidation of glucose in alkaline media was evaluated with cyclic voltammetry and amperometry techniques. A linear relationship between the concentration of glucose and oxidation peak currents was observed in two concentration ranges of 0.004–3.5?mM and 3.5–9.0?mM. The detection limit was 2?μM at signal‐to‐noise ratio of 3. In addition to a fast response time (2?s), the proposed sensor preserved 93?% of its original response towards glucose after 28?days. Also, the sensor showed a good reproducibility and high selectivity for glucose oxidation in the presence of common interfering species. The use of Ni(OH) <sub>2</sub> /PGE sensor was successfully tested in the determination of glucose in human blood serum for the first time in the literature. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >在本研究中，开发了低成本，一次性，敏感和选择性的电化学传感器葡萄糖测定，基于用氢氧化镍改性的铅笔石墨电极（PGE）。使用循环伏安法在PGE上沉积镍。通过现场发射扫描电子显微镜（Fe-SEM），原子力显微镜（AFM）和能量分散X射线光谱（EDX）的形态和改性PGE电极的形态和组成特征。用循环伏安法和电流测定技术评价作为碱介质中葡萄糖电氧化的作为改性电极的性能。在0.004-3.5Ωmm和3.5-9.0Ωmm的两个浓度范围内观察到葡萄糖浓度与氧化峰值电流之间的线性关系。除了快速响应时间（＆lt 2秒）之外，检测极限为2≤μm，响应时间为3.除了快速响应时间（＆lt 2秒），所提出的传感器在28例后保留了其对葡萄糖的原始响应的93.％。而且，传感器在共同干扰物种存在下，对葡萄糖氧化显示出良好的再现性和高选择性。在文献中首次，在确定人血清中的葡萄糖中成功地测试了Ni（OH）<sub> 2 / PGE传感器的使用。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2018年第6期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chelaghmia Mohamed Lyamine&option=202" target="_blank" rel="nofollow">Chelaghmia Mohamed Lyamine;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nacef Mouna&option=202" target="_blank" rel="nofollow">Nacef Mouna;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Affoune Abed Mohamed&option=202" target="_blank" rel="nofollow">Affoune Abed Mohamed;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pontié Maxime&option=202" target="_blank" rel="nofollow">Pontié Maxime;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Derabla Tahar&option=202" target="_blank" rel="nofollow">Derabla Tahar;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Département de Génie des Procédés Laboratoire d'Analyses Industrielles et Génie des MatériauxUniversité 8 Mai 1945 Guelma24000 BP 401 Guelma Algeria;</p> <p>Département de Génie des Procédés Laboratoire d'Analyses Industrielles et Génie des MatériauxUniversité 8 Mai 1945 Guelma24000 BP 401 Guelma Algeria;</p> <p>Département de Génie des Procédés Laboratoire d'Analyses Industrielles et Génie des MatériauxUniversité 8 Mai 1945 Guelma24000 BP 401 Guelma Algeria;</p> <p>Univ. d'Angers SFR Santé Laboratoire GEIHP EA 31424 Rue Larrey 49933 Angers Cedex 9 Angers France;</p> <p>Département de Génie des Procédés Laboratoire d'Analyses Industrielles et Génie des MatériauxUniversité 8 Mai 1945 Guelma24000 BP 401 Guelma Algeria;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nanostructures&option=203" rel="nofollow">Nanostructures;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nickel hydroxide&option=203" rel="nofollow">Nickel hydroxide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pencil graphite electrode&option=203" rel="nofollow">Pencil graphite electrode;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Glucose Non-enzymatic sensor&option=203" rel="nofollow">Glucose Non-enzymatic sensor;</a> </p> <div class="translation"> 机译：纳米结构;氢氧化镍;铅笔石墨电极;葡萄糖非酶促传感器; 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Facile Synthesis of Ni(OH) 22 Modified Disposable Pencil Graphite Electrode and its Application for Highly Sensitive Non‐enzymatic Glucose Sensor

摘要

Facile Synthesis of Ni(OH) ₂2 Modified Disposable Pencil Graphite Electrode and its Application for Highly Sensitive Non‐enzymatic Glucose Sensor