Non‐enzymatic Glucose Sensor Based on Nickel/Carbon Composite

Marini Silvia; Ben?Mansour Nabil; Hjiri Mokhtar; Dhahri Ramzi; El?Mir Lassaad; Espro Claudia; Bonavita Anna; Galvagno Signorino; Neri Giovanni; Leonardi Salvatore Gianluca

摘要

Abstract > Nickel/carbon composites (Ni?C) have been synthesized by a pyrolysis treatment carried out at the temperature of 675?°C, of NiO incorporated into a pyrogallol‐formaldehyde organic wet gel. Structural and morphological characterizations of the Ni?C samples were performed by XRD and SEM analysis, respectively. Electrochemical non‐enzymatic glucose sensors were fabricated modifying the working electrode surface of screen printed carbon electrodes. Cyclic voltammetry and amperometric tests were performed in order to investigate the electrocatalytic activity of differently Ni loaded carbon towards the oxidation of glucose in alkaline 0.1?M KOH solution. The sensor based on 30?% Ni/carbon showed the best sensing performance towards glucose monitoring with a sensitivity of 670?μA/mM?cm ?1 in the a liner range from 20 to 500?μM, and a detection limit lower than 8?μM at S/N=3. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘录</标题> >镍/碳复合材料（Niβc）已通过在NiO的温度为675℃，掺入过吡糖醇 - 甲醛有机湿凝胶中。通过XRD和SEM分析进行Niβc样品的结构和形态学特性。制造电化学非酶促葡萄糖传感器修改丝网印刷碳电极的工作电极表面。进行循环伏安法和安培检测，以研究不同Ni负载碳的电催化活性朝向碱性0.1μkOH溶液中葡萄糖的氧化。基于30μl％的Ni /碳的传感器显示出葡萄糖监测的最佳感测性能，灵敏度为670ΩΩ/ mm？cm 1 / sup>在衬里范围为20至500Ωμm，在S / N = 3处的检测极限低于8？μm。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2018年第4期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Marini Silvia&option=202" target="_blank" rel="nofollow">Marini Silvia;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ben?Mansour Nabil&option=202" target="_blank" rel="nofollow">Ben?Mansour Nabil;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hjiri Mokhtar&option=202" target="_blank" rel="nofollow">Hjiri Mokhtar;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Dhahri Ramzi&option=202" target="_blank" rel="nofollow">Dhahri Ramzi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=El?Mir Lassaad&option=202" target="_blank" rel="nofollow">El?Mir Lassaad;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Espro Claudia&option=202" target="_blank" rel="nofollow">Espro Claudia;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bonavita Anna&option=202" target="_blank" rel="nofollow">Bonavita Anna;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Galvagno Signorino&option=202" target="_blank" rel="nofollow">Galvagno Signorino;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Neri Giovanni&option=202" target="_blank" rel="nofollow">Neri Giovanni;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Leonardi Salvatore Gianluca&option=202" target="_blank" rel="nofollow">Leonardi Salvatore Gianluca;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of EngineeringUniversity of Messina98166 Messina Italy;</p> <p>Laboratory of Physics of Materials and Nanomaterials Applied at EnvironmentUniversity of Gabes6072 Gabes Tunisia;</p> <p>Laboratory of Physics of Materials and Nanomaterials Applied at EnvironmentUniversity of Gabes6072 Gabes Tunisia;</p> <p>Laboratory of Physics of Materials and Nanomaterials Applied at EnvironmentUniversity of Gabes6072 Gabes Tunisia;</p> <p>Laboratory of Physics of Materials and Nanomaterials Applied at EnvironmentUniversity of Gabes6072 Gabes Tunisia;</p> <p>Department of EngineeringUniversity of Messina98166 Messina Italy;</p> <p>Department of EngineeringUniversity of Messina98166 Messina Italy;</p> <p>Department of EngineeringUniversity of Messina98166 Messina Italy;</p> <p>Department of EngineeringUniversity of Messina98166 Messina Italy;</p> <p>Department of EngineeringUniversity of Messina98166 Messina Italy;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Non-enzymatic sensor&option=203" rel="nofollow">Non-enzymatic sensor;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Glucose&option=203" rel="nofollow">Glucose;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nickel nanoparticles&option=203" rel="nofollow">Nickel nanoparticles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Porous carbon&option=203" rel="nofollow">Porous carbon;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pyrolysis&option=203" rel="nofollow">Pyrolysis;</a> </p> <div class="translation"> 机译：非酶传感器;葡萄糖;镍纳米粒子;多孔碳;热解; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-foreign_materials-science-engineering-biomimetic-supramolecular-systems_thesis/0204112885497.html">High-performance non-enzymatic glucose sensor by 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