Curie Temperature Enhancement and Cation Ordering in Titanomagnetites: Evidence From Magnetic Properties, XMCD, and M?ssbauer Spectroscopy

Bowles J. A.; Lappe S.‐C. L. L.; Jackson M. J.; Arenholz E.; Laan G.

摘要

Abstract > Previous work has documented time‐ and temperature‐dependent variations in the Curie temperature ( T <sub> c </sub> ) of natural titanomagnetites, independent of any changes in sample composition. To better understand the atomic‐scale processes responsible for these variations, we have generated a set of synthetic titanomagnetites with a range of Ti, Mg, and Al substitution; a subset of samples was additionally oxidized at low temperature (150?°C). Samples were annealed at temperatures between 325 and 400?°C for up to 1,000?hr and characterized in terms of magnetic properties; Fe valence and site occupancy were constrained by X‐ray magnetic circular dichroism (XMCD) and M?ssbauer spectroscopy. Annealing results in large (up to ~100?°C) changes in T <sub> c </sub> , but M?ssbauer, XMCD, and saturation magnetization data all demonstrate that intersite reordering of Fe 2+ /Fe 3+ does not play a role in the observed T <sub> c </sub> changes. Rather, the data are consistent with vacancy‐enhanced nanoscale chemical clustering within the octahedral sublattice. This clustering may be a precursor to chemical unmixing at temperatures below the titanomagnetite binary solvus. Additionally, the data strongly support a model where cation vacancies are predominantly situated on octahedral sites, Mg substitution is largely accommodated on octahedral sites, and Al substitution is split between the two sites. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 以前的工作在居里温度下记录了时间和温度相关的变化（ t </ i> <sub> c </ i> </ sub> ）天然钛磁石，独立于样品组合物的任何变化。为了更好地理解负责这些变化的原子尺度过程，我们已经产生了一组具有一系列Ti，Mg和Al替代的合成钛镁蛋白;在低温（150℃）下另外氧化样品的子集。在325至400℃的温度下以最高1,000℃的温度退火样品，并以磁性特征为特征; Fe价和位点占用受X射线磁性圆形二色性（XMCD）和M？SSBauer光谱法约束。退火导致大（高达约〜100？°C）变化 t </ i> <sub> c </ i> </ sub> 但是m？ssbauer，xmcd和饱和磁化数据都证明了Fe的交错率重新排序 2 + </ sup> / FE. 3 + </ sup> 在观察到的角色上不起作用 t </ i> <sub> c </ i> </ sub> 变化。相反，数据与八面体子叶内的空位增强的纳米级化学聚类一致。该聚类可以是在钛磁石二元溶解的温度下进行化学解密的前体。另外，数据强烈支持阳离子障碍主要位于八面体位点上的型号，Mg替代在大量地容纳在八面体位点上，并且在两个位点之间分配Al替代。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-23285/'>《Geochemistry, geophysics, geosystems》</a> <b style="margin: 0 2px;">|</b><span>2019年第5期</span><b style="margin: 0 2px;">|</b><span>共18页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bowles J. A.&option=202" target="_blank" rel="nofollow">Bowles J. A.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lappe S.‐C. L. L.&option=202" target="_blank" rel="nofollow">Lappe S.‐C. L. L.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jackson M. J.&option=202" target="_blank" rel="nofollow">Jackson M. J.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Arenholz E.&option=202" target="_blank" rel="nofollow">Arenholz E.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Laan G.&option=202" target="_blank" rel="nofollow">Laan G.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of GeosciencesUniversity of Wisconsin‐MilwaukeeMilwaukee WI USA;</p> <p>Department of GeosciencesUniversity of Wisconsin‐MilwaukeeMilwaukee WI USA;</p> <p>Institute for Rock Magnetism Department of Earth SciencesUniversity of Minnesota Twin CitiesMinneapolis MN USA;</p> <p>Advanced Light SourceLawrence Berkeley National LaboratoryBerkeley CA USA;</p> <p>Magnetic Spectroscopy GroupDiamond Light SourceDidcot UK;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/163.html" title="地球物理学">地球物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=titanomagnetite&option=203" rel="nofollow">titanomagnetite;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Curie temperature&option=203" rel="nofollow">Curie temperature;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=cation ordering&option=203" rel="nofollow">cation ordering;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=XMCD&option=203" rel="nofollow">XMCD;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mossbauer&option=203" rel="nofollow">Mossbauer;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=mineral magnetism&option=203" rel="nofollow">mineral magnetism;</a> </p> <div class="translation"> 机译：泰坦诺弥扑石;居里温度;阳离子排序;XMCD;Mossbauer;矿物质; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704023360799.html">Curie Temperature Enhancement and Cation Ordering in Titanomagnetites: Evidence From Magnetic Properties, XMCD, and M?ssbauer Spectroscopy</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bowles J. 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘璐&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 刘璐</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=闫国利&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,闫国利</a> <span> <a href="/journal-cn-56946/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 心理学报 </a> </span> <span> . 2018</span><span>,第7期</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06130413070692.html">Mössbauer spectroscopy system for applying a magnetic field at cryogenic temperatures using a refrigerator</a> <b>[P]</b> . <span> 外国专利：  JP6024174B2 </span> <span> . 2016-11-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：Mössbauer光谱系统，使用冰箱在低温下施加磁场 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2004-04-02</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过在电磁场中将磁性物质转化为热的磁性物质来产生磁性物质，利用磁性物质的磁性物质的居里温度，利用磁性物质的磁性物质的居里温度，利用磁性物质产生的磁性物质的居里温度，在磁性物质的居里温度范围内通过辐射热来解冻和加热原始材料 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704023360799','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img 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