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首页> 外文期刊>Macromolecular theory and simulations >Synthesis of Micrometer‐Size Poly(Methyl Methacrylate) Particles by Utilizing Microsuspension Iodine Transfer Polymerization ( msms ITP): Kinetic Approach
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Synthesis of Micrometer‐Size Poly(Methyl Methacrylate) Particles by Utilizing Microsuspension Iodine Transfer Polymerization ( msms ITP): Kinetic Approach

机译：利用微肺碘转移聚合来合成微米尺寸聚（甲基丙烯酸甲酯）颗粒（ ms ms ITP）：动力学方法

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Abstract > In a previous work, microsuspension ITP ( ms ITP) of methyl methacrylate (MMA) using iodoform (CHI <sub>3</sub> ) as a chain transfer agent and benzoyl peroxide (BPO) as an initiator could be successfully carried out at 80 °C for the synthesis of micrometer‐size poly(MMA) (PMMA) particles without the byproduct of submicrometer‐size particles. Whereas, in microsuspension conventional radical polymerization ( ms CRP) at the same conditions except for non‐use of CHI <sub>3</sub> , about half amount of PMMA was formed as submicrometer‐size byproduct particles by accompanying emulsion polymerization. In this article, kinetic simulations of ITP and CRP in bulk systems, which, respectively, correspond to those within MMA droplets in ms ITP and ms CRP, are performed using PREDICI software from CiTGmbH to understand the successful reason of the ms ITP of MMA. The simulation results of the ITP indicate that the concentrations of MMA oligomer radicals having BPO initiator fragment and vinyl group as end‐group, which seem to exit from MMA droplets and accompany emulsion polymerization in the aqueous medium in the ms CRP, remarkably decreased in the presence of CHI <sub>3</sub> . This strongly supports the idea “RED effect” proposed in the previous article to explain the success of the ms ITP of MMA. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 在以前的工作中，microSpension ITP（ ms </ i> 使用Iodoform的甲基丙烯酸甲酯（MMA）的ITP（CHI <sub> 3 </ sub> 作为引发剂的链转移剂和过氧化苯甲酰（BPO）可以在80℃下成功地在80℃下成功地进行微米尺寸的聚（MMA）（PMMA）颗粒而没有亚微米尺寸粒子的副产物。虽然，在microSpension中，常规自由基聚合（ ms </ i> CRP）在相同的条件外，除了不使用Chi <sub> 3 </ sub> ，大约半量的PMMA通过伴随乳液聚合形成亚模尺副产物颗粒。在本文中，分别对应于MMA液滴中的ITP和CRP的ITP和CRP动力学模拟 ms </ i> ITP和 ms </ i> CRP，使用来自CITGMBH的Predici软件来了解的成功原因 ms </ i> MMA的ITP。 ITP的仿真结果表明，具有BPO引发剂片段和乙烯基的MMA低聚物自由基作为末端基团，其似乎从MMA液滴中出来并伴随水性介质中的乳液聚合 ms </ i> CRP在Chi存在下显着下降 <sub> 3 </ sub> 。这强烈支持在前一篇文章中提出的“红色效果”的想法，以解释MMA的ITP MS的成功。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-24304/'>《Macromolecular theory and simulations》</a> <b style="margin: 0 2px;">|</b><span>2018年第5期</span><b style="margin: 0 2px;">|</b><span>共5页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Okubo Masayoshi&option=202" target="_blank" rel="nofollow">Okubo Masayoshi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kitayama Yukiya&option=202" target="_blank" rel="nofollow">Kitayama Yukiya;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yamashita Nobuko&option=202" target="_blank" rel="nofollow">Yamashita Nobuko;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Xiang&option=202" target="_blank" rel="nofollow">Liu Xiang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Huang Chujuan&option=202" target="_blank" rel="nofollow">Huang Chujuan;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Energy Science and EngineeringNanjing Tech University30 Puzhu South Road Nanjing 211816 China;</p> <p>Graduate School of EngineeringKobe UniversityKobe 657‐8501 Japan;</p> <p>Graduate School of EngineeringKobe UniversityKobe 657‐8501 Japan;</p> <p>School of Energy Science and EngineeringNanjing Tech University30 Puzhu South Road Nanjing 211816 China;</p> <p>Institute of Advanced MaterialsNanjing Tech University5 Xinmofan Road Nanjing 210009 China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=emulsion polymerization&option=203" rel="nofollow">emulsion polymerization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=iodine transfer polymerization&option=203" rel="nofollow">iodine transfer polymerization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=microsuspension polymerization&option=203" rel="nofollow">microsuspension polymerization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ms ITP&option=203" rel="nofollow">ms ITP;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=radical exit depression (RED) effect&option=203" rel="nofollow">radical exit depression (RED) effect;</a> </p> <div class="translation"> 机译：乳液聚合;碘转移聚合;微肺部聚合;MS ITP;自由基出口抑郁（红色）效果; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" 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<span>机译：逆向碘转移聚合（RITP）和无皂乳液聚合的颗粒具有优异的单分散分布的聚合物颗粒的制备方法，以及使用化学聚合调色剂的化学方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130479809541.html">SIZES FOR GLASS FIBERS COMPRISING EMULSIFIED CLAD PARTICLES OF POLY(METHYL METHACRYLATE)</a> <b>[P]</b> . <span> 外国专利： <!-- --> CA1043027A </span> <span> . 1978-11-21</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包含甲基丙烯酸甲酯乳化包覆颗粒的玻璃纤维尺寸 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130442510189.html">Ternary polymer blends not netted base of poly (methyl methacrylate), process of preparation of ternary polymer blends not netted base of poly (methyl methacrylate), and,Plastic article manufactured</a> <b>[P]</b> . <span> 外国专利： <!-- --> BR0205004A </span> <span> . 2004-07-20</span> </div> <p class="zwjiyix translation" style="max-width: 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