Reisolation and NMR characterization of the satratoxins G and H

Hudson Daniel; Singh A. Jonathan; Lewis Andrew R.; Sulyok Michael; Hinkley Simon F.R.

摘要

Abstract >The exquisitely cytotoxic macrolides, satratoxins G and H, have been reisolated from a solvent extract of a rice culture inoculated with Stachybotrys chartarum to be used as high‐purity reference compounds for analytical analyses. Extensive chromatographic separation realized the compounds that were fully recharacterized in two solvents by 1D‐ and 2D‐NMR spectroscopy, revealing some discrepancies in the nuclear magnetic resonance (NMR) data as compared with the previously reported values found in the literature. Detailed spectra are provided in order to aid future identification and dereplication. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >精致的细胞毒性大环内德，淀粉酮G和h已从与STAchyBotrys Chartarum接种的水稻培养物的溶剂提取物中进行再隔离，以用作用于分析分析的高纯度参考化合物。广泛的色谱分离实现了通过1D-和2D-NMR光谱在两种溶剂中完全重新结合的化合物，揭示核磁共振（NMR）数据中的一些差异，与文献中先前报道的值相比。提供了详细的光谱，以帮助未来的识别和无统计。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-24320/'>《Magnetic Resonance in Chemistry: MRC》</a> <b style="margin: 0 2px;">|</b><span>2020年第2期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hudson Daniel&option=202" target="_blank" rel="nofollow">Hudson Daniel;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Singh A. Jonathan&option=202" target="_blank" rel="nofollow">Singh A. Jonathan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lewis Andrew R.&option=202" target="_blank" rel="nofollow">Lewis Andrew R.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sulyok Michael&option=202" target="_blank" rel="nofollow">Sulyok Michael;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hinkley Simon F.R.&option=202" target="_blank" rel="nofollow">Hinkley Simon F.R.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Ferrier Research Institute School of Chemical and Physical SciencesVictoria University of WellingtonNew Zealand;</p> <p>Ferrier Research Institute School of Chemical and Physical SciencesVictoria University of WellingtonNew Zealand;</p> <p>Ferrier Research Institute School of Chemical and Physical SciencesVictoria University of WellingtonNew Zealand;</p> <p>Department for Agrobiotechnology Centre for Analytical ChemistryUniversity of Natural Resources and Life SciencesVienna Austria;</p> <p>Ferrier Research Institute School of Chemical and Physical SciencesVictoria University of WellingtonNew Zealand;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/13344.html" title="磁化学分析法">磁化学分析法;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> </p> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704023546122.html">Reisolation and NMR characterization of the satratoxins G and H</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hudson Daniel&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Hudson Daniel,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Singh A. 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