Synthesis crystal growth and properties of the charge transfer complex adduct of 2-nitro aniline with picric acid - An organic non-linear optical material

Bharathikannan R; Chandramohan A; Kandhaswamy MA; Chandrasekaran J; Renganathan R; Kandavelu V

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Synthesis crystal growth and properties of the charge transfer complex adduct of 2-nitro aniline with picric acid - An organic non-linear optical material

机译：2-硝基苯胺与苦味酸的电荷转移复合加合物的合成晶体生长和性质-有机非线性光学材料

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The organic NLO material 2-nitro aniline and picric acid (2NAP) was synthesized, needle shaped single crystals of dimension 10 x 1 x 0.8 mm(3) were grown by slow evaporation solution growth technique from the saturated solution of the title compound in chloroform at ambient temperature. The material was characterized through elemental analysis, powder XRD, H-1 NMR, C-13 NMR and FTIR techniques. The various planes of reflection have been identified from the XRD powder pattern. The formation of the charge transfer complex was confirmed by UV-VIS spectroscopy. The thermal stability of the crystals was investigated using TG/DTA analyses techniques. The second harmonic generation (SHG) efficiency of the material was estimated using Nd: YAG laser as source. (C) 2008 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

机译：合成了有机NLO材料2-硝基苯胺和苦味酸（2NAP），通过缓慢蒸发溶液生长技术从标题化合物在氯仿中的饱和溶液中生长了尺寸为10 x 1 x 0.8 mm（3）的针状单晶。在环境温度下。通过元素分析，粉末XRD，H-1 NMR，C-13 NMR和FTIR技术对材料进行表征。从XRD粉末图案可以识别出各种反射平面。通过UV-VIS光谱法确认了电荷转移络合物的形成。使用TG / DTA分析技术研究了晶体的热稳定性。使用Nd：YAG激光作为光源估算了材料的二次谐波（SHG）效率。（C）2008 WILEY-VCH Verlag GmbH＆Co.KGaA，Weinheim。

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《Crystal Research and Technology: Journal of Experimental and Industrial Crystallography》 |2008年第6期|共6页
作者
Bharathikannan R; Chandramohan A; Kandhaswamy MA; Chandrasekaran J; Renganathan R; Kandavelu V;
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正文语种 eng
中图分类晶体学;
关键词
charge transfer; solution growth; 2-nitroaniline picric acid adduct; nonlinear optical materials; DERIVATIVES; STILBENE;

机译：电荷转移溶液生长2-硝基苯胺苦味酸加合物非线性光学材料衍生物苯乙烯;

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1. Synthesis crystal growth and properties of the charge transfer complex adduct of 2-nitro aniline with picric acid - An organic non-linear optical material [J] . Bharathikannan R, Chandramohan A, Kandhaswamy MA, Crystal Research and Technology: Journal of Experimental and Industrial Crystallography . 2008,第6期

机译：2-硝基苯胺与苦味酸的电荷转移复合加合物的合成晶体生长和性质-有机非线性光学材料
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Synthesis crystal growth and properties of the charge transfer complex adduct of 2-nitro aniline with picric acid - An organic non-linear optical material

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