Synthesis, characterization and X-ray crystal structure of guanidinuim (pyridine-2,6-dicarboxylato)(pyridine-2,6-monocarboxylato) zincate(II) mono pyridine-2,6-dicarboxylic acid tetrahydrate

Aghabozorg H; Sadr-Khanlou E

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Synthesis, characterization and X-ray crystal structure of guanidinuim (pyridine-2,6-dicarboxylato)(pyridine-2,6-monocarboxylato) zincate(II) mono pyridine-2,6-dicarboxylic acid tetrahydrate

机译：胍基亚胺（吡啶-2,6-二羧基）（吡啶-2,6-一羧基）吡啶酸锌（II）一吡啶-2,6-二羧酸四水合物的合成，表征和X射线晶体结构

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A new complex of Zinc(II) and guanidinium pyridine-2,6-dicarboxylate proton transfer compound, (GnH)(2)(pydc), was synthesized and characterized using IR, H-1 NMR and C-13 NMR spectroscopy and single crystal X-ray diffraction. The chemical formula and space group of the resulting complex is (GnH)[Zn(pydc)(pydcH)] center dot (pydcH(2)) center dot 4H(2)O, P (1) over bar Where the final R value is 0.0310 for 13287 reflections collected. The [Zn(pydc)(pydcH)](-) anions and the (GnH)(+) counter-cations form a three-dimensional solid-state structure by a variety of noncovalent interactions such as ion pairing, hydrogen bonding and pi-pi stacking which are going to be discussed. (C) 2008 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

机译：合成了一种新的锌（II）和吡啶吡啶-2,6-二羧酸酯质子转移化合物（GnH）（2）（pydc）的复合物，并使用IR，H-1 NMR和C-13 NMR光谱进行了表征晶体X射线衍射。所得配合物的化学式和空间群为（GnH）[Zn（pydc）（pydcH）]中心点（pydcH（2））中心点4H（2）O，P（1）超过bar，其中最终R值对于收集到的13287个反射，值为0.0310。 [Zn（pydc）（pydcH）]（-）阴离子和（GnH）（+）抗衡阳离子通过各种非共价相互作用，例如离子对，氢键和pi-，形成三维固态结构。 pi堆栈将要讨论。（C）2008 WILEY-VCH Verlag GmbH＆Co.KGaA，Weinheim。

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《Crystal Research and Technology: Journal of Experimental and Industrial Crystallography》 |2008年第3期|共6页
作者
Aghabozorg H; Sadr-Khanlou E;
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正文语种 eng
中图分类晶体学;
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zinc(II) sulphate; pyridine-2; 6-dicarboxylic acid; hydrogen bonds; ion pairs; crystal structure; PROTON-TRANSFER COMPOUND; SELF-ASSEMBLING SYSTEM; 2; 6-PYRIDINEDICARBOXYLIC ACID; ZINC(II) COMPLEX; PYRIDINE;

机译：硫酸锌;吡啶-2;6-二羧酸;氢键;离子对;晶体结构;质子转移化合物;自组装体系;2;6-吡啶二羧酸;锌（II）络合物;吡啶;

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1. Synthesis, characterization and X-ray crystal structure of guanidinuim (pyridine-2,6-dicarboxylato)(pyridine-2,6-monocarboxylato) zincate(II) mono pyridine-2,6-dicarboxylic acid tetrahydrate [J] . Aghabozorg H, Sadr-Khanlou E Crystal Research and Technology: Journal of Experimental and Industrial Crystallography . 2008,第3期

机译：胍基亚胺（吡啶-2,6-二羧基）（吡啶-2,6-一羧基）吡啶酸锌（II）一吡啶-2,6-二羧酸四水合物的合成，表征和X射线晶体结构
2. A proton transfer compound of piperazine with pyridine-2,6-dicarboxylic acid and its palladium(II) and thallium(III) complexes - Synthesis, characterization and crystal structure [J] . Aghabozorg H, Ghadermazi M, Manteghi F, Zeitschrift fur Anorganische und Allgemeine Chemie . 2006,第12a13期

机译：哌嗪与吡啶2,6-二羧酸的质子转移化合物及其钯（II）和th（III）配合物-合成，表征和晶体结构
3. Sonochemical synthesis and characterization of a Zn(II) supramolecule, bis(2,6 diaminopyridinium)bis(pyridine-2,6-dicarboxylato)zincate(II), as a novel precursor for the ZnO-based dye sensitizer solar cell [J] . Ranjbar Maryam, Mozaffari Sayed Ahmad, Kouhestanian Elham, Journal of Photochemistry and Photobiology, A. Chemistry . 2016,第Null期

机译：Zn（II）超分子双（2,6二氨基吡啶）双（吡啶-2,6-二羧基羧基）zincate（II）的声化学合成和表征，作为基于ZnO的染料敏化剂太阳能电池的新型前体
4. The Potential of Pyridine-2,6-Dicarboxylic Acid Based Organolanthanide Complexes for Efficient Near-Infrared Emission [C] . Richard J. Curry, Michael R. George, Martin C. Grossel Organic Light-Emitting Materials and Devices IX . 2005

机译：吡啶-2,6-二羧酸基有机黄嘌呤配合物对高效近红外发射的潜力
5. Genomic analysis of a microbial community by microarray comparative genomic hybridization, and, Genetic characterization of the pdt locus for the production of pyridine-2,6-dithiocarboxylic acid. [D] . Sebat, Jonathan Ladd. 2002

机译：通过微阵列比较基因组杂交对微生物群落进行基因组分析，以及生产2,6-吡啶二硫代吡啶的pdt基因座的遗传特征。
6. Isolation of dipicolinic acid (pyridine-2:6-dicarboxylic acid) from spores of Bacillus megatherium [O] . Joan F. Powell 1953

机译：从巨大芽孢杆菌的孢子中分离二吡啶甲酸（吡啶-2：6-二羧酸）
7. Aqua(1,10-phenanthroline)(pyridine-2,6-dicarboxylato)nickel(II) pyridine-2,6-dicarboxylic acid solvate tetrahydrate [O] . Javad Safaei-Ghomi, Hossein Aghabozorg, Elham Motyeian, 2009

机译：aqua（1,10-phenanthroline）（吡啶-2,6-二羧酸）镍（II）吡啶-2,6-二羧酸溶剂化物四水合物

Synthesis, characterization and X-ray crystal structure of guanidinuim (pyridine-2,6-dicarboxylato)(pyridine-2,6-monocarboxylato) zincate(II) mono pyridine-2,6-dicarboxylic acid tetrahydrate

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