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Characterization of the Structure of Porous Germanium Layers by High-Resolution X-ray Diffractometry

机译:高分辨率X射线衍射法表征多孔锗层的结构

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The surface morphology and the structure of porous germanium layers obtained by chemical etching of n-type single-crystal Ge(111) substrates with their subsequent annealing in hydrogen atmosphere are studied by high-resolution X-ray diffractometry. It is established that upon etching a 1.5 to 2.0-μm-thick porous germanium layer is formed, which contains quasi-ordered microinhomogeneities in the form of elongated pits with characteristic dimensions of 1 μm and an average distance between them of 3-4 μm. The layer bulk has pores with radii ranging within 25-30 nm and nanocrystallites with an average size of 10 nm, with the average porosity being 56%.
机译:通过高分辨率X射线衍射研究了通过化学刻蚀n型单晶Ge(111)衬底并随后在氢气氛中退火获得的多孔锗层的表面形态和结构。已经确定,通过蚀刻形成1.5至2.0μm厚的多孔锗层,该多孔锗层以细长凹坑的形式包含准次序的微不均匀性,其特征尺寸为1μm,并且它们之间的平均距离为3-4μm。该层块具有半径在25-30nm范围内的孔和平均尺寸为10nm的纳米微晶,平均孔隙率为56%。

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